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Open Access. Powered by Scholars. Published by Universities.®

2017

The University of Akron

High-Energy Ball Milling

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Effect Of Sintering Temperature On Microstructure, Corrosion Behavior, And Hardness Of Nanocrystalline Al-5at.%Ni And Al-5at.%V Alloys, Matthew G. Wachowiak Jan 2017

Effect Of Sintering Temperature On Microstructure, Corrosion Behavior, And Hardness Of Nanocrystalline Al-5at.%Ni And Al-5at.%V Alloys, Matthew G. Wachowiak

Williams Honors College, Honors Research Projects

The purpose of this project was to investigate thermal stability of high energy ball milled Al-5at.%Ni and Al-5at.%V alloys. Characterization was done by analyzing grain size and solid solubility. Samples were created using high energy ball milling, cold compaction to 3 GPa, and sintering from 100 °C to 500 °C at 100 °C increments, as well 450 °C and 614 °C. Microstructure, mechanical properties, and corrosion properties were determined using scanning electron microscopy, energy dispersive x-ray spectroscopy, x-ray diffraction, hardness testing, and cyclic potentiodynamic polarization. Vickers hardness of Al-5at.%Ni decreased with increasing temperature. For Al-at.%V, hardness increased with sintering temperature …