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Full-Text Articles in Nuclear Engineering
Impact Of The Synthesis Process On Structure Properties For Afci Fuel Candidates, Kenneth Czerwinski
Impact Of The Synthesis Process On Structure Properties For Afci Fuel Candidates, Kenneth Czerwinski
Fuels Campaign (TRP)
The research objectives are:
• To explore a low-temperature fluoride route to synthesize actinide nitrides. • To characterize actinide nitrides structurally and thermally.
• To use high resolution TEM techniques to explore the microstructure of the radioactive samples.
Solution-Based Synthesis Of Nitride Fuels, Kenneth Czerwinski, Tyler A. Sullens
Solution-Based Synthesis Of Nitride Fuels, Kenneth Czerwinski, Tyler A. Sullens
Fuels Campaign (TRP)
One of the original synthetic routes devised for the synthesis of U (III)N involved the entire reaction taking place in liquid ammonia. Several experimental reactions were conducted in an attempt to synthesize the UI3(NH3)x and U(NH2)3(NH3)x precursors of U(III) N. Each attempt involved cleaning of the uranium metal to remove the oxide coating of the metal reagent with 3 washes of concentrated nitric acid, each followed by a rinse with liquid ammonia. Success of this cleaning procedure was varied, with a majority of cleaned metal oxidizing rapidly once …