Nanoscience and Nanotechnology Commons^™

High Speed Atomic Force Microscopy Techniques For The Efficient Study Of Nanotribology, James L. Bosse

Master's Theses

As mechanical devices scale down to micro/nano length scales, it is crucial to understand friction and wear at the nanoscale (nanotribology) especially at technically relevant sliding velocities. Accordingly, three novel techniques have been developed to study nanotribology, leveraging recent advances in high speed AFM. The first method utilizes high line-scanning rates coupled with sinusoidal scanning along the AFM fast scan axis, enabling rapid friction measurements as a function of velocity up to 20 mm/sec. The second method rapidly acquires friction versus force curves through disabling the feedback loop during scanning and relating the resulting lateral data with the correspondingly varying …

Nanocharacterization Of Porous Materials With Atomic Force Microscopy, Yasemin Kutes

Master's Theses

Scanning Probe Microscopy techniques have proven very useful in the investigation of porous nanostructured surfaces. Especially, Atomic Force Microscopy (AFM) has been widely used due to its compatibility with non-conducting surfaces. In particular, AFM often complements other techniques like scanning and transmission electron microscopy by providing quantitative surface information coupled with nanoscale spatial resolution. Its ability to operate in fluid is also important, as this allows researchers to mimic the physiological environment of biological materials and systems. In this work, two main types of porous materials are studied with AFM, including Phosphoric Acid Fuel Cell (PAFC) electrode catalyst layers, and …

Electrochemical Synthesis Of Single Crystal Metal Nanowires, Nan Li

Master's Theses

Electrodeposition is an efficient and economical approach for template synthesis of one-dimensional (1D) nanostructured materials. Based on the porous membranes as templates during electrodeposition, metallic nanowires, nanorods, and nanotubes can overcome the geometrical restrictions to be inserted into the nanometric recesses with both diameter and length well controlled by tuning the size and thickness of the templates.

In this work, the morphology, growth rate and texture of copper nanowires prepared with templates were investigated by the controlled parameters in various experiments. Cu nanowire arrays with preferential orientations can be successfully synthesized into the Anodic Aluminum Oxide (AAO) templates with optimized …