Mechanical Engineering Commons^™

The Effect Of Parameters In Cryogenic Treatment On Mechanical Properties Of Tool Steel: A Review, Ronaldus Caesariano Ekaputra, Myrna Ariati Mochtar

Journal of Materials Exploration and Findings (JMEF)

Tool steel is classified as special alloy steel which proposed as dies or mold materials as their high mechanical properties and dimensional stability. In order to improve tool steel’s mechanical properties, heat treatment process, especially, cryogenic treatment is conducted. Cryogenic treatment is done by exposing tool steel material at sub-zero liquid/gas media after heated at austenite temperature. This process significantly affects the martensite phase transformation increase and avoids retained austenite emersion. In particular, the higher martensite volume fraction, the higher hardness and wear resistance value of tool steel. It had been proven that adjusting critical process parameters of cryogenic treatment …

Sae 8620 Pspp Map - Infographic, John F. Mitchener

ME 4133/6133 Mechanical Metallurgy

This infographic summarizes a Processing-Structure-Property-Performance (PSPP) Map for SAE 8620 alloy steel, with an emphasis on the gas carburization process. This PSPP map allows researchers and material scientists to better understand the processes that drive the microstructures, material properties, and ultimate performance parameters.

Direct Energy Deposition Of Mo Powder Prepared By Electrode Induction Melting Gas Atomization, Goo Won Roh, Eun Soo Park, Jaeyun Moon, Hojun Lee, Jongmin Byun

Mechanical Engineering Faculty Research

Molybdenum (Mo) is used to form a barrier layer for metal wiring in displays or semiconductor devices. Recently, researches have been continuously attempted to fabricate Mo sputtering targets through additive manufacturing. in this study, spherical Mo powders with an average particle size of about 37 um were manufactured by electrode induction melting gas atomization. Subsequently, Mo layer with a thickness of 0.25 mm was formed by direct energy deposition in which the scan speed was set as a variable. According to the change of the scan speed, pores or cracks were found in the Mo deposition layer. Mo layer deposited …

The Effect Of Flinak Molten Salt Corrosion On The Hardness Of Hastelloy N, David Kok

Scholar Week 2016 - present

The Molten Salt Reactor (MSR) has been identified as a promising candidate to replace aging nuclear reactors around the world. However, a suitable combination of molten salt and container material needs to be found in order to reduce the potential for corrosion in the MSR before it can be considered commercially viable. FLiNaK molten salt and the nickel-based alloy Hastelloy N have been identified as prime candidates for this function, but the severity of FLiNaK corrosion in Hastelloy N requires additional study before this combination can be used in the operation of a MSR. In this study, Hastelloy N samples …

Custom Foot Prosthetic: Diabetic Care, Chandler Streuli

All Undergraduate Projects

Across the United States there are people every day who lose their toes to diabetes or to loss of circulation within their legs. The problem becomes building a more cost effective and efficient prosthetic for these individuals. The prosthetics that are used for medical purposes are often costly, especially without the help of insurance. The new prosthetic was designed to be taken in and out of shoes so that it is fast and easy for the user to move the device from shoe to shoe. The manufacturing method for this project was using a 3D printer to build the initial …

Bending Nanoindentation And Plasticity Noise In Fcc Single And Polycrystals, Ryder Bolin, Hakan Yavas, Hengxu Song, Kevin J. Hemker, Stefanos Papanikolaou

Faculty & Staff Scholarship

Abstract: We present a high-throughput nanoindentation study of in situ bending effects on incipient plastic deformation behavior of polycrystalline and single-crystalline pure aluminum and pure copper at ultranano depths (< 200 nm). We find that hardness displays a statistically inverse dependence on in-plane stress for indentation depths smaller than 10 nm, and the dependence disappears for larger indentation depths. In contrast, plastic noise in the nanoindentation force and displacement displays statistically robust noise features, independently of applied stresses. Our experimental results suggest the existence of a regime in Face Centered Cubic (FCC) crystals where ultranano hardness is sensitive to residual applied stresses, but plasticity pop-in noise is insensitive to it.

The Effect Of Flinak Molten Salt Corrosion On The Hardness Of Hastelloy N, David Kok

Honors Program Projects

The desire to reduce pollution caused by electricity production has led to a call for the replacement of conventional fossil fuel power plants. In order to fulfill this goal, a large amount of new nuclear reactors is required, and this provides the opportunity to put new and innovative reactor designs into production. The Molten Salt Reactor (MSR) is one of the most promising concepts, but a suitable combination of molten salt and container material needs to be found to reduce the potential for corrosion before the concept can be put into production. FLiNaK molten salt and the nickel-based alloy Hastelloy …

Microstructures And Hardness Of Tig Welded Experimental 57fe15cr25ni Steel, Parikin Parikin, Mohammad Dani, Abu Khalid Rivai, Agus Hadi Ismoyo, Riza Iskandar, Arbi Dimyati

Makara Journal of Technology

The microstructures and hardness of tungsten inert gas (TIG) welded experimental 57Fe15Cr25Ni steel were investigated through optical–scanning electron microscopy analyses and with a hardness tester, respectively. The welding process restructured the constituent atoms into regular and irregular crystal lattices. Rapid cooling of the weld metal allowed the formation of a dendritic (columnar) structure, with porous grains. By contrast, slow cooling influenced HAZ and led to the formation of grain structures. The crystal lattice became more organized and larger than other zones. Meanwhile, the base metal formed circular nets that covered large area inside thick and thin grain boundaries. The diffraction …

Direct Metal Laser-Sintered Stainless Steel: Comparison Of Microstructure And Hardness Between Different Planes, M. Ghasri-Khouzani, H. Peng, R. Attardo, P. Ostiguy, J. Neidig, R. Billo, D. Hoelzle, M. R. Shankar

Mechanical and Aerospace Engineering Faculty Research & Creative Works

Microstructural analysis and micro-hardness measurements were performed on different planes of 316L stainless steel fabricated by direct metal laser sintering (DMLS) technique. A fine cellular network was observed within the steel microstructure, where morphology of most cells changed from columnar on XZ-plane (vertical section) to equiaxed on XY-plane (horizontal section). Correspondingly, morphology of most grains was found to alter from columnar for the XZ-plane to equiaxed in the case of the XY-plane. Moreover, X-ray diffraction (XRD) analysis revealed a fully austenitic structure for both the planes. The average micro-hardness value for the XZ-plane and XY-plane was insignificantly (≈ 3%) different, …

Analysis Of Ni And Fe-Based Alloys For Turbine Seal Ring Applications, Dawei She

USF Tampa Graduate Theses and Dissertations

Metal sealing rings have been used widely in compressors, turbines and hydraulic devices. Such rings can extend out due to elasticity, and keep close contact with the valve wall, resulting in the formation of a functional seal under pressure. In this project, the failure of metal sealing rings is considered. Sealing component failure due to stress relaxation can threaten the safety of the whole steam turbine. The object of this study was to examine the stress relaxation response and corresponding changes in microstructure of metal sealing rings used in nuclear steam turbine under high temperature and applied stress. The two …

Raman Spectroscopy Of The Skeleton Of The Coral Acropora Cervicornis, Zachary C. Shepard

Honors Undergraduate Theses

Coral reefs are an important element of marine ecosystem that are critical to maintain a healthy environment. Unfortunately, in recent years coral reefs are doing poorly and many in parts of the ocean are simply dying. Therefore, study of coral’s structural response to external loads could answer what will happen with their structures, while they exhibit different types of loading. Therefore, the proposition of using in-situ micro-Raman spectroscopy to study skeletons of Acropora cervicornis was used. Coral skeleton samples I subjected to mechanical loading studied their vibrational properties by exciting the material with 532nm visible light. A uniaxial compressive load …

Effect Of Ultrasonic Treatment On The Microstructure And Mechanical Properties Of Al6061 And Composite, Ana S. Exime

FIU Electronic Theses and Dissertations

In this study, the effect of ultrasonic treatment (UST) parameters such as amplitude, sonication time, and melt temperature on microstructure and microhardness of Al 6061 alloy is evaluated. The effect of UST on the dispersion of tungsten disulfide (WS₂) and carbon nanotubes (CNT) as reinforcement particles in Al 6061 during casting is also studied. The cast Al 6061 with UST demonstrated 32% grain size reduction and 8% increase in the microhardness for optimum processing conditions. The cavitation process induced by UST is responsible for the refinement in microstructure and increase of hardness by enhancing the degassing and nucleation …

Design And Fabrication Of Functionally Graded Material From Ti To Γ-Tial By Laser Metal Deposition, Xueyang Chen, Lei Yan, Joseph William Newkirk, Frank W. Liou

Materials Science and Engineering Faculty Research & Creative Works

Functionally graded material (FGM) is one kind of advanced material characterized by a gradual change in properties as the position varies. The spatial variation of compositional and microstructure over volume is aimed to control corresponding functional properties. In this research, when 100% γ-TiAl was directly deposited on pure Ti substrate, cracks were formed within the γ-TiAl layer. Then a six-layer crack-free functionally graded material of Ti/TiAl was designed and fabricated by laser metal deposition (LMD) method, with composition changing from pure Ti on one side to 100% γ-TiAl on the other side. The fabricated FGM was characterized for material properties …

Cryogenic Processing Of Al 7050-T7451 Alloy For Improved Surface Integrity, Bo Huang

Theses and Dissertations--Mechanical Engineering

Al 7050-T7451 alloy with good combinations of strength, stress corrosion cracking resistance and toughness, is used broadly in the aerospace/aviation industry for fatigue-critical airframe structural components. However, it is also considered as a highly anisotropic alloy as the crack growth behavior along the short transverse direction is very different from the one in the long transverse direction, due to the inhomogeneous microstructure with the elongated grains distributed in the work material used in the sheet/plate applications. Further processes on these materials are needed to improve its mechanical and material properties and broaden its applications.

The material with ultra-fine or nano …

An Investigation Of Nanoparticles Addition On Solidification Kinetics And Microstructure Development Of Tin–Lead Solder, D. Lin, S. Liu, T. Guo, Guo-Xiang Wang, T. Srivatsan, M. Petraroli

Dr. Guo-Xiang Wang

High strength solders can be engineered by adding trace amounts of nanopowders into solder paste. An experimental study was conducted for a better understanding of the solidification kinetics and microstructure development of such nano-composite tin–lead solders. The composite solder pastes were prepared by mechanically mixing nanopowders of either copper or TiO₂ with tin–lead powders (tens of microns in size). Solidification experiments of the composite solders were performed in an aluminum crucible with temperature variation during cooling and solidification being measured. For the titanium dioxide (TiO₂) nanopowders-reinforced composite solders, the test data reveals the occurrence of melt undercooling …

Synthesis And Characterization Of Nano-Composite Lead-Free Solder, D. Lin, C. Kuo, T. Srivatsan, M. Petraroli, Guo-Xiang Wang

Dr. Guo-Xiang Wang

A series of experiments conducted on a lead-free eutectic solder (Sn-3.5%Ag) have shown that addition of trace amounts of nanometer-sized particles does have an influence on mechanical properties of materials. In this study, three different types of nanoparticles (copper, nickel and iron) were chosen as the reinforcing candidate. For each particulate reinforcement the reflow process was performed under identical cooling conditions. Addition of trace amounts of nano-particles alters the kinetics governing solidification of the composite solder paste while concurrently exerting an influence on microstructural development, particularly the formation and presence of second phases in the solidified end product. The nano-sized …

An Investigation Of Friction Stir Welding Parameter Effects On Post Weld Mechanical Properties In 7075 Aa, Steven B. Dickson

Theses and Dissertations

The effects of weld temperature, travel speed, and backing plate thermal diffusivity on themechanical properties of a weld have been studied. A face centered cubic experiment of designwas completed in which the response variables were yield strength, minimum hardness in the HAZ, and charpy impact toughness. Three models were created from the data gathered usinga stepwise regression in order to see the effects of each parameter. For the yield strength andminimum hardness it was found that only travel speed and backing plate thermal diffusivities werestatistically significant to the properties. The charpy impact toughness saw that all three parameterswere statistically significant …

Alternative Methods To Determine The Elastoplastic Properties Of Sintered Hydroxyapatite From Nanoindentation Testing

Faculty of Engineering University of Malaya

This study introduces alternative methods to determine the elastoplastic properties of bovine-derived Hydroxyapatite (HA) porous bone graft through a set of nanoindentation tests with a Berkovich indenter. Generally, experimental data obtained from nanoindentation tests are force displacement, hardness and elastic modulus. However, to determine plastic properties such as strength coefficient and work hardening exponent of bovine HA, analytical or inverse finite element models are required. In this paper, the effect of sintering temperature on these properties of HA is studied for the range of 1000-1400 degrees C. The direct and inverse Finite Element (FE) simulation models for nanoindentation tests were …

Nanomechanical Characterization Of Cavity Growth And Rupture In Hydrogen-Implanted Single-Crystal Batio3., Young-Bae Park, Patrick Nardi, Xiaodong Li, Harry A. Atwater

Xiaodong Li

A thermodynamic model of cavitynucleation and growth in ion-implanted single-crystal BaTiO3 layer is proposed, and cavity formation is related to the measured mechanical properties to better understand hydrogen implantation-induced layer transfer processes for ferroelectric thin films. The critical radius for cavitynucleation was determined experimentally from blistering experiments performed under isochronal anneal conditions and was calculated using continuum mechanical models for deformation and fracture, together with thermodynamic models. Based on thermodynamic modeling, we suggest that cavitiesgrow toward the cracking criteria at a critical blister size whereupon gas is emitted from ruptured cavities. The main driving force for layer splitting is the …

Investigating The Surface Tribology Of Roller-Burnished Polymer Using The Fuzzy Rule-Based Approach

Faculty of Engineering University of Malaya

Burnishing is specified as the plastic deformation cold working process applied as surface treatment and smoothing following machining to obtain a superior surface roughness finish. The present experimental study was carried out on roller-burnished polyurethane using a roller burnishing tool. An analysis was done to investigate the effect of burnishing depth, speed, feed rate, and roller width on the surface roughness of the polymer workpiece. Roughness (R-a) prediction was achieved with a fuzzy rule-based system. The results indicate 95% accuracy between the fuzzy predicted roughness values and experimental results. Link to Full-Text Articles : www.tandfonline.com/doi/abs/10.1080/10402004.2014.962205

The Mechanical And Tribology Properties Of Sputtered Titanium Aluminum Nitride Coating On The Tungsten Carbide Insert Tool In The Dry Turning Of Tool Steel, Esmar Budi, Mohd. Razali Bin Muhamad, Md. Nizam Bin Abdul Rahman

Makara Journal of Technology

The effect of the sputtering parameters on the mechanical tribology properties of Titanium Aluminum Nitride coating on the tungsten cabide insert tool in the dry turning of tool steel has been investigated. The coating was deposited using a Direct Current magnetron sputtering system with various substrate biases (-79 to -221 V) and nitrogen flow rates (30 to 72 sccm). The dry turning test was carried out on a Computer Numeric Code machine using an optimum cutting parameter setting. The results show that the lowest flank wear (~0.4 mm) was achieved using a Titanium Aluminum Nitride-coated tool that was deposited at …

Surface Hardness Of Friction Stir Welded Aa6063 Pipe, Azman Ismail, Mokhtar Awang

Azman Ismail

The external surface hardness of friction stir welded aluminum alloy 6063 pipe joint was investigated in this paper. The 89mm of outside diameter pipe with 5mm of wall thickness was used as test pipe piece for this experiment on closed butt joint configuration by utilising Bridgeport 2216 CNC milling machine and orbital clamping unit specially designed to cater for this task and function. Several welded samples were produced on varying process parameters which were successfully joined by using a non-consumable tool with a flat shoulder and a cylindrical pin.

Gadolinia Doped Hafnia (Gd2o3- Hfo2) Thermal Barrier Coatings For Gas Turbine Applications, Satya Kiran Gullapalli

Open Access Theses & Dissertations

Thermal efficiency of the gas turbines is influenced by the operating temperature of the hot gas path components. The material used for the hot gas path components can only withstand temperature up to a certain limit. Thermal barrier coatings (TBC) provide the additional thermal protection for these components and help the gas turbine achieve higher firing temperatures. Traditionally available yttria stabilized zirconia (YSZ) TBCs have a limitation up to 1200 C due to their phase transformation. The present work focuses on gadolinia based hafnia (GSH) TBCs to study their potential to replace the YSZ coatings. Different compositions of gadolinia doped …

Study On The Fracture Toughness Of Friction Stir Welded Api X80, Allan M. Tribe

Theses and Dissertations

High strength low alloy (HSLA) steels have been developed to simultaneously have high yield strength and high fracture toughness. However, in practical applications steel must be welded. Traditional arc welding has proven detrimental to the fracture toughness of HSLA steels. Friction stir welding has recently shown mixed results in welding HSLA steels. The range of welding parameters used in these recent studies however has been very limited. With only a few welding parameters tested, the effect of spindle speed, travel speed, and heat input on the fracture toughness of friction stir welded HSLA steel remains unknown. To understand how the …

Degradation Of Physical Properties Of Different Elastomers Upon Exposure To Palm Biodiesel

A.S. Md Abdul Haseeb

Biodiesel, as an alternative fuel, is gradually receiving more popularity for use in internal combustion engines. However questions continue to arise with regard to its compatibility with elastomeric materials. The present work aims to investigate the comparative degradation of physical properties for different elastomers [e.g. ethylene propylene diene monomer (EPDM), silicone rubber (SR), polychloroprene (CR), polytetrafluroethylene (PTFE) and nitrile rubber (NBR)] upon exposure to diesel and palm biodiesel. Static immersion tests in B0(diesel), B10 (10% biodiesel in diesel), B20, B50 and B100(biodiesel) were carried out at room temperature (25 °C) for 1000 h. Different physical properties like, changes in weight …

Addition Of Cobalt Nanoparticles Into Sn-3.8ag-0.7cu Lead-Free Solder By Paste Mixing

A.S. Md Abdul Haseeb

Purpose - The purpose of this paper is to investigate the effects of addition Co nanoparticles on the characteristic properties of Sn-3.8Ag-0.7Cu solder. Design/methodology/approach - Cobalt (Co) nanoparticles were added to Sn-Ag-Cu solders by thoroughly blending various weight percentages (0-2.0 wt%) of Co nanoparticles with near eutectic SAC387 solder paste. Blending was done mechanically for 30 min to ensure a homogeneous mixture. The paste mixture was then reflowed on a hot plate at 250°C for 45 s. The melting points of nanocomposite solder were determined by differential scanning calorimetry. Spreading rate of nanocomposite was calculated following the JIS Z3198-3 standard. …

Structural And Mechanical Properties Of Nanostructured Tio2 Thin Films Deposited By Rf Sputtering

A.S. Md Abdul Haseeb

This study mainly aims to evaluate the effects of substrate temperatures on the mechanical properties of TiO2 thin films deposited on glass substrates by radio-frequency (RF) magnetron sputtering. All titania films possess anatase structure having a nodular morphology. AES results reveal that Si and Na ions from glass diffuse into TiO2 films at higher substrate temperatures. Micro-scratch and wear tests were conducted to evaluate their mechanical and tribological properties. The adhesion critical loads of TiO2 films deposited at room temperature, 200 and 300°C are found to be 1.51, 1.54 and 1.08N, respectively. Scratch hardness also increases from 11.5 to 13.6GPa …

Compatibility Of Elastomers In Palm Biodiesel

A.S. Md Abdul Haseeb

In recent time, environmental awareness and concern over the rapid exhaustion of fossil fuels have led to an increased popularity of biodiesel as an alternative fuel for automobiles. However, there are concerns over enhanced degradation of automotive materials in biodiesel. The present study aims to investigate the impact of palm biodiesel on the degradation behavior of elastomers such as nitrile rubber (NBR), polychloroprene, and fluoro-viton A. Static immersion tests in B0 (diesel), B10 (10% biodiesel in diesel), B100 (biodiesel) were carried out at room temperature (25 °C) and at 50 °C for 500 h. At the end of immersion test, …

Thermal Stability Of Electrodeposited Liga Ni-W Alloys For High Temperature Mems Applications

A.S. Md Abdul Haseeb

For thermally stable LIGA materials for high temperature MEMS applications LIGA Ni-W layers and micro testing samples with different compositions (15 and 5 at% W) were electrodeposited. In order to investigate the thermal stability the Ni-W layers were annealed at different temperatures (300-700°C) and for different durations (1, 4, 16 h). Their microstructure and micro-hardness were than analysed after annealing and compared with those of as-deposited states. The observed microstructures show, in comparison to pure LIGA nickel, a small grain growth and a relatively stable structure up to 700°C. The micro-hardness values of the LIGA Ni-W layers are higher than …

Nanoindentation Of The A And C Domains In A Tetragonal Batio3 Single Crystal, Young-Bae Park, Matthew J. Dicken, Zhi-Hui Xu, Xiaodong Li

Faculty Publications

Nanoindentation in conjunction with piezoresponse force microscopy was used to study domain switching and to measure the mechanical properties of individual ferroelectric domains in a tetragonal BaTiO₃ single crystal. It was found that nanoindentation has induced local domain switching; the a and c domains of BaTiO₃ have different elastic moduli but similar hardness.Nanoindentationmodulus mapping on the a and c domains further confirmed such difference in elasticity. Finite element modeling was used to simulate the von Mises stress and plastic strain profiles of the indentations on both a and c domains, which introduces a much higher stress level than …