Open Access. Powered by Scholars. Published by Universities.®

Mechanical Engineering Commons

Open Access. Powered by Scholars. Published by Universities.®

Articles 1 - 3 of 3

Full-Text Articles in Mechanical Engineering

On The Nature Of The Electrochemically Synthesized Hard Fe-0.96 Mass Pct C Alloy Film Dec 2002

On The Nature Of The Electrochemically Synthesized Hard Fe-0.96 Mass Pct C Alloy Film

A.S. Md Abdul Haseeb

A hard Fe-0.96 mass pet C alloy with a hardness value of 810 HV has been electrochemically synthesized from a ferrous sulfate bath containing a small amount of citric acid and L-ascorbic acid. The nature of the alloy has been investigated by a number of techniques, including X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), scanning electron microscopy (SEM), transmission electron microscopy (TEM), Mössbauer spectroscopy, differential scanning calorimetry (DSC), and magnetic measurements. The decomposition behavior of the alloy is also studied and compared with that of thermally prepared martensite. It has been found that the electrochemically deposited Fe-C alloy exists in …


On The Nature Of The Electrochemically Synthesized Hard Fe-0.96 Mass Pct C Alloy Film Nov 2002

On The Nature Of The Electrochemically Synthesized Hard Fe-0.96 Mass Pct C Alloy Film

A.S. Md Abdul Haseeb

A hard Fe-0.96 mass pet C alloy with a hardness value of 810 HV has been electrochemically synthesized from a ferrous sulfate bath containing a small amount of citric acid and L-ascorbic acid. The nature of the alloy has been investigated by a number of techniques, including X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), scanning electron microscopy (SEM), transmission electron microscopy (TEM), Mössbauer spectroscopy, differential scanning calorimetry (DSC), and magnetic measurements. The decomposition behavior of the alloy is also studied and compared with that of thermally prepared martensite. It has been found that the electrochemically deposited Fe-C alloy exists in …


Piezoelectric In Situ Transmission Electron Microscopy Technique For Direct Observations Of Fatigue Damage Accumulation In Constrained Metallic Thin Films, Xiaoli Tan, T. Du, J.K. Shang Jan 2002

Piezoelectric In Situ Transmission Electron Microscopy Technique For Direct Observations Of Fatigue Damage Accumulation In Constrained Metallic Thin Films, Xiaoli Tan, T. Du, J.K. Shang

Xiaoli Tan

A piezoelectricin situtransmission electron microscopy(TEM) technique has been developed to observe the damage mechanism in constrained metallic thin films under cyclic loading. The technique was based on the piezoelectric actuation of a multilayered structure in which a metallic thin film was sandwiched between a piezoelectric actuator and a silicon substrate. An alternating electric field with a static offset was applied on the piezoelectric actuator to drive the crack growth in the thin metallic layer while the sample was imaged in TEM. The technique was demonstrated on solder thin films where cavitation was found to be the dominant fatigue damage mechanism.