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Graduate Theses and Dissertations

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Full-Text Articles in Mechanical Engineering

Capabilities Of Sintered Silver As A High Temperature Packaging Material, Bakhtiyar Mohammad Nafis Dec 2023

Capabilities Of Sintered Silver As A High Temperature Packaging Material, Bakhtiyar Mohammad Nafis

Graduate Theses and Dissertations

With electrification progressing across many sectors including industry, automotive and aerospace, the power density requirements are changing. The increased power density results in higher and higher ambient temperatures that electronics are exposed to. The response has been to move towards wide bandgap (WBG) semiconductor devices that can withstand much greater temperatures and can operate at much higher voltages than silicon. Additionally, these WBG devices deliver low drain-source on resistance (RDS_on) capabilities, enabling high current power modules that increase power density even further. This also requires the packaging to evolve in order to withstand the new requirements. As a result, researchers …


Development Of A Prototype Satellite-Tracking Telescope For Ground-Based Spectroscopy, Charles Smith Dec 2023

Development Of A Prototype Satellite-Tracking Telescope For Ground-Based Spectroscopy, Charles Smith

Graduate Theses and Dissertations

Spectroscopy is the practice of determining the chemical composition of a gas through analyzing the light that is filtered by the gas. Spectroscopy is commonly used by astronomers to deduce the atmospheric composition of planets. This process is done by initially measuring the spectrum of light from the star that the planet orbits, and then measuring it again once the planet is in between the observer and the star. The spectrum light that is filtered out is dependent on the chemical composition of the gas, and so this information can be used to determine the chemical composition of the atmosphere …


Partial Discharge Mitigation In Power Modules Using An Automation-Driven Design Rule Development Method, Shilpi Mukherjee Sep 2023

Partial Discharge Mitigation In Power Modules Using An Automation-Driven Design Rule Development Method, Shilpi Mukherjee

Graduate Theses and Dissertations

Power modules used for the conversion and conditioning of electrical power for applications like electric vehicles, more-electric aircraft, the power grid, etc., are largely designed manually by engineers. Design automation of power modules is starting to gain recognition as a timely and necessary alternative to intuitive manual design and fabrication. With increasing need for wide bandgap materials that can operate at higher voltages, and the need to make modules more compact, hazards like electrical breakdown are more likely. Partial discharge (PD) is a silent and invisible precursor to electrical breakdown. It is compounded with compaction, creating a potential for electrical …


Improving Tribological Properties Of Polydopamine/Polytetrafluoroethylene Coatings Through Incorporating Core-Shell Nanoparticles And Laser Surface Texturing, Firuze Soltani-Kordshuli May 2023

Improving Tribological Properties Of Polydopamine/Polytetrafluoroethylene Coatings Through Incorporating Core-Shell Nanoparticles And Laser Surface Texturing, Firuze Soltani-Kordshuli

Graduate Theses and Dissertations

Polytetrafluoroethylene (PTFE) is a widely used polymer that has unique properties such as chemical and temperature resistance, corrosion resistance, low maintenance cost, and a very low coefficient of friction (COF). These distinctive properties have made PTFE a promising candidate for industrial applications where surfaces are in relative motion. PTFE can be utilized as a thin film solid lubricant to significantly reduce the friction between moving surfaces. However, PTFE coatings have low cohesion and poor adhesion to the substrate resulting in its low wear resistance. This fact limits the application of PTFE coatings in load-bearing situations. To address these limitations, an …


Pda/Ptfe Solid Lubricant Coating For 60niti Applications, Charles Richey Miller May 2023

Pda/Ptfe Solid Lubricant Coating For 60niti Applications, Charles Richey Miller

Graduate Theses and Dissertations

The intermetallic alloy 60NiTi has a unique combination of high hardness and low elastic modulus, which makes it highly resistant to dents. Additionally, 60NiTi is extremely corrosion resistant and chemically inert. These properties make 60NiTi a desirable material for challenging mechanical component applications with high contact stresses and in harsh environments. However, lubrication issues have hindered the use of 60NiTi because it has poor tribological performance if it is not properly lubricated. The mechanical properties of hardened 60NiTi and its microconstituents were studied by nanoindentation. This study showed that the bulk properties of 60NiTi are driven by the properties of …


Advanced Cmos Process For Submicron Silicon Carbide (Sic) Device, Niloy Saha May 2023

Advanced Cmos Process For Submicron Silicon Carbide (Sic) Device, Niloy Saha

Graduate Theses and Dissertations

Silicon carbide (SiC) is a wide semiconductor material with superior material properties compared to other rival materials. Due to its fewer dislocation defects than gallium nitride and its ability to form native oxides, this material possesses an advantage among wide band gap materials. Despite having several superior properties its low voltage application is less explored. CMOS is extremely important in low voltage areas and silicon is the dominant player in it for the last 50 years where scaling has contributed a major role in this flourishment. The channel length of silicon devices has reached 3 nm whereas SiC is still …


Interfacial Engineering Of Nickel-Rich Layered Oxide Cathodes Via Atomic Layer Deposition (Ald), Xin Wang Dec 2022

Interfacial Engineering Of Nickel-Rich Layered Oxide Cathodes Via Atomic Layer Deposition (Ald), Xin Wang

Graduate Theses and Dissertations

Layered nickel-rich cathodes LiNixMnyCozO2 (NMCs, x + y + z =1, x ≥ 0.6) are regarded as one of the most promising cathode materials for next-generation lithium-ion batteries (LIBs), given their remarkably reduced cost and increased capacity compared to the conventional LiCoO2 cathode. However, the deployment of these Ni-rich cathodes has been hindered by the continuous loss of practical capacity and reduction in average working voltage, inherently due to their interfacial, structural, and thermodynamic instability. To address these issues, interfacial engineering via surface modification has been well-recognized as an effective strategy and a large number of coating materials have been …


Data-Driven Research On Engineering Design Thinking And Behaviors In Computer-Aided Systems Design: Analysis, Modeling, And Prediction, Molla Hafizur Rahman Aug 2022

Data-Driven Research On Engineering Design Thinking And Behaviors In Computer-Aided Systems Design: Analysis, Modeling, And Prediction, Molla Hafizur Rahman

Graduate Theses and Dissertations

Research on design thinking and design decision-making is vital for discovering and utilizing beneficial design patterns, strategies, and heuristics of human designers in solving engineering design problems. It is also essential for the development of new algorithms embedded with human intelligence and can facilitate human-computer interactions. However, modeling design thinking is challenging because it takes place in the designer’s mind, which is intricate, implicit, and tacit. For an in-depth understanding of design thinking, fine-grained design behavioral data are important because they are the critical link in studying the relationship between design thinking, design decisions, design actions, and design performance. Therefore, …


Constraint-Aware, Scalable, And Efficient Algorithms For Multi-Chip Power Module Layout Optimization, Imam Al Razi Aug 2022

Constraint-Aware, Scalable, And Efficient Algorithms For Multi-Chip Power Module Layout Optimization, Imam Al Razi

Graduate Theses and Dissertations

Moving towards an electrified world requires ultra high-density power converters. Electric vehicles, electrified aerospace, data centers, etc. are just a few fields among wide application areas of power electronic systems, where high-density power converters are essential. As a critical part of these power converters, power semiconductor modules and their layout optimization has been identified as a crucial step in achieving the maximum performance and density for wide bandgap technologies (i.e., GaN and SiC). New packaging technologies are also introduced to produce reliable and efficient multichip power module (MCPM) designs to push the current limits. The complexity of the emerging MCPM …


Understanding Thermal Comfort Impact And Air Movement Around Open Stairs Through The Use Of Cfd Modeling, Ethan Davidson May 2022

Understanding Thermal Comfort Impact And Air Movement Around Open Stairs Through The Use Of Cfd Modeling, Ethan Davidson

Graduate Theses and Dissertations

The air exchange between two floors of a building has an impact on thermal comfort. The present research attempts to quantify this impact and identify the contributing factors disrupting the thermal comfort on and around stairs. Various heating and cooling scenarios were analyzed, using CFD modeling, in a simple two-story building separated by a single staircase. The research examines a single building layout with a fixed inlet and outlet configuration. In addition, the study investigated the short-term impact on thermal comfort. As a result, the duration of the simulations varies from two and half minutes to ten minutes, consistent with …


Hobby Grade Lithium-Ion Batteries For Spacecraft Applications: Establishing An Automated Electrical Characteristics Testing Procedure For Flight Acceptance Of Non-Space-Grade Small Secondary Batteries, Braidon Hughes Dec 2021

Hobby Grade Lithium-Ion Batteries For Spacecraft Applications: Establishing An Automated Electrical Characteristics Testing Procedure For Flight Acceptance Of Non-Space-Grade Small Secondary Batteries, Braidon Hughes

Graduate Theses and Dissertations

Li-ion batteries are widely used due to the large amount of rechargeable energy they pack into a small, light package. This higher energy density makes Li-ion batteries ideal for small satellite applications, specifically CubeSats. CubeSats have grown in popularity in higher level education due to the National Aeronautics and Space Administration’s implementation of the Cube Satellite Launch Initiative, making it easier and cheaper to conduct small, low orbit missions. Because these CubeSats are occupying the same space as a crewed spacecraft, it is imperative that they are safe. There are numerous reports of Li-ion batteries creating fires that result in …


Deep Learning Strategies For Pool Boiling Heat Flux Prediction Using Image Sequences, Connor Heo Dec 2021

Deep Learning Strategies For Pool Boiling Heat Flux Prediction Using Image Sequences, Connor Heo

Graduate Theses and Dissertations

The understanding of bubble dynamics during boiling is critical to the design of advanced heater surfaces to improve the boiling heat transfer. The stochastic bubble nucleation, growth, and coalescence processes have made it challenging to obtain mechanistic models that can predict boiling heat flux based on the bubble dynamics. Traditional boiling image analysis relies on the extraction of the dominant physical quantities from the images and is thus limited to the existing knowledge of these quantities. Recently, machine-learning-aided analysis has shown success in boiling crisis detection, heat flux prediction, real-time image analysis, etc., whereas most of the existing studies are …


Respiratory Compensated Robot For Liver Cancer Treatment: Design, Fabrication, And Benchtop Characterization, Mishek Jair Musa Dec 2021

Respiratory Compensated Robot For Liver Cancer Treatment: Design, Fabrication, And Benchtop Characterization, Mishek Jair Musa

Graduate Theses and Dissertations

Hepatocellular carcinoma (HCC) is one of the leading causes of cancer-related death in the world. Radiofrequency ablation (RFA) is an effective method for treating tumors less than 5 cm. However, manually placing the RFA needle at the site of the tumor is challenging due to the complicated respiratory induced motion of the liver. This paper presents the design, fabrication, and benchtop characterization of a patient mounted, respiratory compensated robotic needle insertion platform to perform percutaneous needle interventions. The robotic platform consists of a 4-DoF dual-stage cartesian platform used to control the pose of a 1-DoF needle insertion module. The active …


Thermometry Via Diffusion In Ferrous Core-Shell Nanoparticles For Induction Heating Applications, Hayden Carlton Dec 2021

Thermometry Via Diffusion In Ferrous Core-Shell Nanoparticles For Induction Heating Applications, Hayden Carlton

Graduate Theses and Dissertations

Induction heating causes the release of enormous amounts of heat from dispersed magnetic nanoparticles. While the rate of heat transfer can be easily quantified calorimetrically, measuring the temperature of the nanoparticles on the nanoscale presents experimental challenges. Fully characterizing the temperature and thermal output of these magnetic particles is necessary to gauge overall heating efficiency and to provide a more holistic understanding of heat transfer on the nanoscale. Herein, this dissertation seeks to develop a novel nanoparticle thermometry technique, which correlates diffusion behavior in core-shell nanoparticles to local temperature. Initial measurements suggested that heating silica capped ferrous nanoparticles (SCNPs) via …


Nonmetallic Jet Impingement Thermal Management For Power Electronics Via Additive Manufacturing, Reece Whitt Dec 2021

Nonmetallic Jet Impingement Thermal Management For Power Electronics Via Additive Manufacturing, Reece Whitt

Graduate Theses and Dissertations

The increase in energy demanded by transportation and energy sectors has necessitated highly efficient thermal management for reliable power electronics operations. Conventional cooling techniques are limited by their inability to target switching location hot spot temperatures, leading to non-uniform thermal gradients. These devices, such as cold plates and heat sinks, also utilize heavy metallic structures that can accentuate electromagnetic interferences generated by high voltage switching processes. This work proposes a non-metallic jet impingement cooler for more customized thermal management, while simultaneously reducing the harmful effects of electromagnetic interferences. Additive manufacturing is utilized to enable jet impingement zones to target individual …


Combined Stressors In Reliability Failure Modes In Flip-Chip Electronic Packaging, Mahsa Montazeri Dec 2021

Combined Stressors In Reliability Failure Modes In Flip-Chip Electronic Packaging, Mahsa Montazeri

Graduate Theses and Dissertations

The trend toward miniaturization of electronic devices to fulfill Moore’s law introduces new reliability concerns to the electronic packaging process while worsening existing primary challenges. In solder interconnect specifically, temperature cycling is one of the prominent failure threats. However, with further downscaling of the flip-chip solder connections, electromigration also present a precarious failure mode in these interconnects. On the other hand, understanding the degradation mechanism in solders is crucial for the power electronic products' reliability considering the industrial tendency to replace wirebonds with solder attachment while improving the current carry capacity. This dissertation utilizes FEA simulation and an experimental approach …


Mission Profile Effects On Automotive Drivetrain Electronics Reliability: Modeling And Mitigation, Bakhtiyar Mohammad Nafis Dec 2021

Mission Profile Effects On Automotive Drivetrain Electronics Reliability: Modeling And Mitigation, Bakhtiyar Mohammad Nafis

Graduate Theses and Dissertations

The reliability of electronic devices is dependent upon the conditions to which they are subject. Temperature variations coupled with differences in thermal expansion between bonded materials results in thermomechanical stresses to build up, which can instigate failure in the interconnects or other critical regions. With the move towards electrification in the automotive industry, there is the increasingly important consideration of powertrain electronics reliability, the pertinent conditions being governed by the drive cycle or mission profile of the vehicle. The mission profile determines the power dissipated by the electronic devices, which determines the peak and mean temperature, temperature swing and the …


Tribological Studies Of Thick Polytetrafluoroethylene Coatings Enhanced By Polydopamine And Nanoparticles, Sujan Kumar Ghosh Jul 2021

Tribological Studies Of Thick Polytetrafluoroethylene Coatings Enhanced By Polydopamine And Nanoparticles, Sujan Kumar Ghosh

Graduate Theses and Dissertations

Polytetrafluoroethylene (PTFE) is a popular low friction solid lubricant with high chemical and thermal stability. Thick PTFE coatings have the potential for many tribological applications, such as replacing Tin-based Babbitt materials in journal bearings. However, the weak bonding strength to the substrate and the high wear rate of PTFE coatings are current limiting factors. The lack of understanding of their tribological properties and wear mechanisms in oil-lubricated conditions and how coating thickness affects the tribological performance further hindered the use of PTFE coatings. In this dissertation, polydopamine (PDA), a bio-inspired adhesive, is used as an underlayer for or as a …


Development Of Novel Battery Materials For Lithium-Ion Batteries And Beyond, Jiyu Cai Jul 2021

Development Of Novel Battery Materials For Lithium-Ion Batteries And Beyond, Jiyu Cai

Graduate Theses and Dissertations

As fossil fuels are depleting and causing environmental issues, it becomes imperative to widely implement renewable energies (e.g., solar and wind power). In this context, electrical energy storage (EES) systems are essential to accommodate the intermittent supply and uneven distribution of renewable energies. To this end, high-energy-density EES devices are highly demanded, such as rechargeable batteries. This dissertation presents my efforts in developing novel battery materials for lithium-ion batteries (LIBs), sodium-ion batteries (SIBs), and solidstate lithium batteries (SSLBs). These efforts include electrochemical evaluations of battery materials, surface modifications of electrodes via atomic layer deposition (ALD), and advanced characterizations of batteries …


Phase-Field Modeling Of The Polymer Membrane Formation Process For Micro- And Ultra-Filtration, Michael Rosario Cervellere Jul 2021

Phase-Field Modeling Of The Polymer Membrane Formation Process For Micro- And Ultra-Filtration, Michael Rosario Cervellere

Graduate Theses and Dissertations

Porous polymer membrane filters are widely used in separation and filtration process. Micro- and ultra-filtration membranes are commonly used in biopharmaceutical applications such as filtering viruses and separating proteins from a carrier solution. The formation of these membrane filters via phase inversion is a complex and interconnected process where varying casting conditions can have a wide variety of effects on the final membrane morphol- ogy. Tailoring membrane filters for specific performance characteristics is a tedious and time consuming process. The time and length scales of membrane formation make it extremely difficult to experimentally observe membrane formation. Modeling the membrane formation …


Influence Of Extracellular Matrix Stiffness And Topography On Neuronal Cell Behavior And Neurite Outgrowth, Mohan Yasodharababu Jul 2021

Influence Of Extracellular Matrix Stiffness And Topography On Neuronal Cell Behavior And Neurite Outgrowth, Mohan Yasodharababu

Graduate Theses and Dissertations

The focus of regeneration therapy for traumatic brain injuries and Alzheimer's disease is on the promotion and growth of neuronal cells. In vitro research attempts to improve this by modifying the stiffness and topography of the extracellular matrix (ECM). However, the limitations of in vitro experiments make it difficult to control the individual factors influencing neuronal cell growth. A computational model can be used to decouple individual factors and study them individually to gain a better understanding of the mechanics between the neuronal cell and ECM, which will aid in the design of in vitro experimental studies.

This study develops …


Material Detection With Thermal Imaging And Computer Vision: Potentials And Limitations, Jared Poe Jul 2021

Material Detection With Thermal Imaging And Computer Vision: Potentials And Limitations, Jared Poe

Graduate Theses and Dissertations

The goal of my masters thesis research is to develop an affordable and mobile infraredbased environmental sensoring system for the control of a servo motor based on material identification. While this sensing could be oriented towards different applications, my thesis is particularly interested in material detection due to the wide range of possible applications in mechanical engineering. Material detection using a thermal mobile camera could be used in manufacturing, recycling or autonomous robotics. For my research, the application that will be focused on is using this material detection to control a servo motor by identifying and sending control inputs based …


Computational Frameworks For Multi-Robot Cooperative 3d Printing And Planning, Laxmi Prasad Poudel Jul 2021

Computational Frameworks For Multi-Robot Cooperative 3d Printing And Planning, Laxmi Prasad Poudel

Graduate Theses and Dissertations

This dissertation proposes a novel cooperative 3D printing (C3DP) approach for multi-robot additive manufacturing (AM) and presents scheduling and planning strategies that enable multi-robot cooperation in the manufacturing environment. C3DP is the first step towards achieving the overarching goal of swarm manufacturing (SM). SM is a paradigm for distributed manufacturing that envisions networks of micro-factories, each of which employs thousands of mobile robots that can manufacture different products on demand. SM breaks down the complicated supply chain used to deliver a product from a large production facility from one part of the world to another. Instead, it establishes a network …


High Temperature Degradation In Gan-Based Hall Effect Sensors, Alexis Anne Krone Jul 2021

High Temperature Degradation In Gan-Based Hall Effect Sensors, Alexis Anne Krone

Graduate Theses and Dissertations

This research focuses on understanding the effects of accelerated aging through temperature and environment on novel gallium nitride-based Hall effect magnetic field sensors and determining device reliability under electric vehicle operating conditions. The device reliability was modeled using accelerated aging for the temperatures of 200 °C, 350 °C, 450 °C, and 600 °C under various time steps unique to each temperature and either air, which is identical to operating circumstances, or argon, which would model the hermetic packaging environment. Using a high temperature furnace and oven, devices underwent high temperature storage tests at a chosen temperature and time step. Afterwards, …


An Investigation Of Testing Parameters On The Frictional Properties Of Patterned Core-Shell Nanostructures, Colin Phelan May 2021

An Investigation Of Testing Parameters On The Frictional Properties Of Patterned Core-Shell Nanostructures, Colin Phelan

Graduate Theses and Dissertations

Friction tests are a beneficial means to analyze the tribological characteristics and advantages of materials and textured surfaces. However, the selected test parameters can significantly influence the results. This work explores the significance of the friction testing parameters on the frictional performances of core-shell nanostructure-textured surfaces (CSNTSs). Several applied normal loads (10 μN, 100 μN, and 500 μN) and diamond counterface indenter tip radii (1 μm, 5 μm, and 20 μm) were selected for the testing of Al/diamond-like-carbon (DLC) and Al/amorphous silicon (a-Si) CSNTSs. The measured friction values of the CSNTSs were then compared to a matching Al/DLC film and …


Numerical Simulations Of Directed Self-Assembly Methods In Di-Block Copolymer Films For Efficient Manufacturing Of Nanoscale Patterns With Long-Range Order, Joseph Hill Dec 2020

Numerical Simulations Of Directed Self-Assembly Methods In Di-Block Copolymer Films For Efficient Manufacturing Of Nanoscale Patterns With Long-Range Order, Joseph Hill

Graduate Theses and Dissertations

Directed self-assembly (DSA) of block copolymers (BCPs) has been shown as a viable method to achieve bulk fabrication of surface patterns with feature sizes smaller than those available through traditional photolithography. Under appropriate thermodynamic conditions, BCPs will self-assemble into ordered micro-domain morphologies, a desirable feature for many applications. One of the primary interests in this field of research is the application of thin-film BCPs to existing photolithography techniques. This “bottom-up” approach utilizes the self-assembled BCP nanostructures as a sacrificial templating layer in the lithographic process.

While self-assembly occurs spontaneously, extending orientational uniformity over centimeter-length scales remains a critical challenge. A …


Mechanical And Frictional Behavior Of Textured And Non-Textured Surfaces, Raghuram R. Santhapuram Dec 2020

Mechanical And Frictional Behavior Of Textured And Non-Textured Surfaces, Raghuram R. Santhapuram

Graduate Theses and Dissertations

Tribology is the study of surfaces where two objects are sliding against another. Significant energy is lost due to friction between the sliding surfaces. Therefore, developing or designing surfaces to minimize friction is critical for the durability and reliability of the mechanical components. Several researchers have identified that surface texturing at the nanoscale (nanotexture) would reduce the friction between the contacting surfaces. The nanotextured surfaces have several applications in microelectromechanical systems and nanoelectromechanical systems. This dissertation employs molecular dynamics simulations to investigate the frictional and mechanical response of nanotextured aluminum (Al) and Al/amorphous silicon (a-Si) composite surfaces.

This study determines …


Adhesion And Deformation Mechanisms Of Polydopamine And Polytetrafluoroethylene: A Multiscale Computational Study, Matthew Brownell Dec 2020

Adhesion And Deformation Mechanisms Of Polydopamine And Polytetrafluoroethylene: A Multiscale Computational Study, Matthew Brownell

Graduate Theses and Dissertations

Polydopamine (PDA) has been shown to bond via covalent bonding, van der Waals forces, and hydrogen bonding and is known to adhere strongly to almost any material. The application of PDA between a substrate and a PTFE surface coating has resulted in low friction and a greatly reduced wear rate. Previous research probing the capabilities and limitations of PDA/PTFE films have studied the wear and mechanical properties of the film, but the overall adhesive and deformation mechanisms remain unclear.

In this research, we investigate the tribological properties of PDA and PTFE molecules and composites from the atomic to the microscale …


Design, Fabrication, And Reliability Effects Of Additively Manufactured First Level Compliant Interconnects For Microelectronics Application, Tumininu David Olatunji Dec 2020

Design, Fabrication, And Reliability Effects Of Additively Manufactured First Level Compliant Interconnects For Microelectronics Application, Tumininu David Olatunji

Graduate Theses and Dissertations

Semiconductor packaging and development is greatly dependent on the magnitude of interconnect and on-chip stress that ultimately limits the reliability of electronic components. Thermomechanical related strains occur because of the coefficient of thermal expansion mismatch from different conjoined materials being assembled to manufacture a device. To curb the effect of thermal expansion mismatch between conjoined parts, studies have been done in integrating compliant structures between dies, solder balls, and substrates. Initial studies have enabled the design and manufacturing of these structures using a photolithography approach which involves a high number of fabrication steps depending on the complexity of the structures …


The Varied Thermal Response Of Magnetic Iron-Oxide Nanoparticles During Induction Heating In Liquid And Solid-Liquid Phase Change Mediums, Joshua Tompkins Dec 2020

The Varied Thermal Response Of Magnetic Iron-Oxide Nanoparticles During Induction Heating In Liquid And Solid-Liquid Phase Change Mediums, Joshua Tompkins

Graduate Theses and Dissertations

This study investigates the induction heating response of uncapped iron oxide nanoparticles sonically dispersed as a nanofluid and mechanically distributed in solid phase change materials. The nanoparticles examined have a mean diameter of 14.42 nm and are magnetically heated in an alternating magnetic field at an amplitude of 72.6 kA/m at frequencies of 217, 303, and 397 kHz. Nanoparticle characterization was undertaken through transition electron microscopy, x-ray diffraction, and dynamic light scattering when in suspension. Carrier fluids were characterized through viscosity, heat capacity, and density measurements which were used in the calorimetric calculation of the specific absorption rate (SAR) of …