Mechanical Engineering Commons^™

The Role Of Electron Irradiation History In Liquid Cell Transmission Electron Microscopy., Trevor H Moser, Hardeep Mehta, Chiwoo Park, Ryan T Kelly, Tolou Shokuhfar, James E Evans

Michigan Tech Publications

In situ liquid cell transmission electron microscopy (LC-TEM) allows dynamic nanoscale characterization of systems in a hydrated state. Although powerful, this technique remains impaired by issues of repeatability that limit experimental fidelity and hinder the identification and control of some variables underlying observed dynamics. We detail new LC-TEM devices that improve experimental reproducibility by expanding available imaging area and providing a platform for investigating electron flux history on the sample. Irradiation history is an important factor influencing LC-TEM results that has, to this point, been largely qualitatively and not quantitatively described. We use these devices to highlight the role of …