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Chemical Engineering

2015

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Articles 1 - 30 of 66

Full-Text Articles in Mechanical Engineering

Independency Of Elasticity On Residual Stress Of Room Temperature Rolled Stainless Steel 304 Plates For Structure Materials, Parikin Parikin, David Allen Dec 2015

Independency Of Elasticity On Residual Stress Of Room Temperature Rolled Stainless Steel 304 Plates For Structure Materials, Parikin Parikin, David Allen

Makara Journal of Technology

Mechanical strengths of materials are widely expected in general constructions of any building. These properties depend on its formation (cold/hot forming) during fabrication. This research was carried out on cold-rolled stainless steel (SS) 304 plates, which were deformed to 0, 34, 84, and 152% reduction in thickness. The tests were conducted using Vickers method. Ultra micro indentation system (UMIS) 2000 was used to determine the mechanical properties of the material, i.e.: hardness, modulus elasticity, and residual stresses. The microstructures showed lengthening outcropping due to stress corrosion cracking for all specimens. It was found that the tensile residual stress in a …


Effect Of Fly Ash Fortification In The Manufacture Process Of Making Concrete Towards Characteristics Of Concrete In Sulfuric Acid Solution, Asep Handaya Saputra, Muhammad Shohibi, Masatoshi Kubouchi Dec 2015

Effect Of Fly Ash Fortification In The Manufacture Process Of Making Concrete Towards Characteristics Of Concrete In Sulfuric Acid Solution, Asep Handaya Saputra, Muhammad Shohibi, Masatoshi Kubouchi

Makara Journal of Technology

Fly ash is a silica or alumino silica material that can be used as a constituent of cement in the concrete manufacturing process. Utilization of fly ash aims to improve durability and minimize the reduction of concrete’s compressive strength exposed to an acidic environment, which can be achieved through the pozzolanic reaction of fly ash with Ca(OH)2 within concrete. The reduced content of Ca(OH)2 through pozzolanic reaction will minimize the tendency of ettringite formation (compounds that cause deterioration and decrease the compressive strength of concrete). In order to determine the relation between fly ash replenishment into concrete with concrete’s characteristics …


Improvement Of Quality Of Carica Papaya L. With Clove Oil As Preservative In Edible Coating Technology, Eny Kusrini, Anwar Usman, Chrispine Deksita Wisakanti, Rita Arbianti, Dedy Alharis Nasution Dec 2015

Improvement Of Quality Of Carica Papaya L. With Clove Oil As Preservative In Edible Coating Technology, Eny Kusrini, Anwar Usman, Chrispine Deksita Wisakanti, Rita Arbianti, Dedy Alharis Nasution

Makara Journal of Technology

We have studied utilization of essential clove oil, extracted from clove buds by hydrodistillation, as preservative in edible packaging technology. Preservative of essential clove oil was applied on chopped papaya fruits by using two methods, namely spray and brush. The effects of concentration of clove oil from 0.05 to 0.20% on the preservation of papaya fruits (Carica papaya L.) at room temperature (25 °C) were also evaluated. Physicochemical and in vitro microbiological activities on the papaya fruits that were stored at 25 oC and 85-90% relative humidity were investigated in details. The results indicate that the clove oil at concentration …


Oxidation Process Of H 2 O /Uv For Cod Reduction Of Wastewater From Soybean Tofu Production, Komala Pontas, Abrar Muslim Dec 2015

Oxidation Process Of H 2 O /Uv For Cod Reduction Of Wastewater From Soybean Tofu Production, Komala Pontas, Abrar Muslim

Makara Journal of Technology

Chemical Oxygen Demand (COD) reduction of wastewater from soybean tofu production was studied by conducting advanced oxidation process (AOP) using hydrogen peroxide with UV radiation catalysts in a closed cylindrical glass reactor. The hydroxyl radical (*OH) concentration from H2O2 decomposition was modeled, and exponential trends were found for the *OH concentration over radiation time and operation temperature. As a result, it was found that the maximal *OH concentration was 0.209 mol L-1 at 240 minutes and 50 °C. The *OH concentration exponentially increased following rise in operation temperature. The H2O2/UV AOP application reduced COD concentration to approximately 42.41% from 10,545 …


Improving Renewable Energy Transition Acceptance: A Simulation Gaming Approach On A Multi Actor Setting In The Netherlands, Aziiz Sutrisno, Jac A. M. Vennix, Noor Syaifudin Dec 2015

Improving Renewable Energy Transition Acceptance: A Simulation Gaming Approach On A Multi Actor Setting In The Netherlands, Aziiz Sutrisno, Jac A. M. Vennix, Noor Syaifudin

Makara Journal of Technology

The Netherlands have tried very hard to increase their renewable energy sources (RES) shares to fulfill the European Union target in 2050. However, RES performance did not show the expected result as the performance declined in 2009 producing even wider gap compare to the target. The Dutch government’s tried to incorporate all interested stakeholders by forming the Dutch energy transition task force. Nevertheless, the task force’s result is also not showing a desirable trend. Key reasons behind the Dutch low RES performance are the lack of shared understanding and positive attitude toward RES development among interested actors. This research uses …


Calibration Of Numerical Model For Shoreline Change Prediction Using Satellite Imagery Data, Sigit Sutikno, Keisuke Murakami, Dwi Puspo Handoyo, Manyuk Fauzi Dec 2015

Calibration Of Numerical Model For Shoreline Change Prediction Using Satellite Imagery Data, Sigit Sutikno, Keisuke Murakami, Dwi Puspo Handoyo, Manyuk Fauzi

Makara Journal of Technology

This paper presents a method for calibration of numerical model for shoreline change prediction using satellite imagery data in muddy beach. Tanjung Motong beach, a muddy beach that is suffered high abrasion in Rangsang Island, Riau province, Indonesia was picked as study area. The primary numerical modeling tool used in this research was GENESIS (GENEralized Model for Simulating Shoreline change), which has been successfully applied in many case studies of shoreline change phenomena on a sandy beach.The model was calibrated using two extracted coastlines satellite imagery data, such as Landsat-5 TM and Landsat-8 OLI/TIRS. The extracted coastline data were analyzed …


Dual-Band Singly-Fed Proximity-Coupled Tip-Truncated Triangular Patch Array For Land Vehicle Mobile System, Basari Basari, Josaphat Tetuko Sri Sumantyo Dec 2015

Dual-Band Singly-Fed Proximity-Coupled Tip-Truncated Triangular Patch Array For Land Vehicle Mobile System, Basari Basari, Josaphat Tetuko Sri Sumantyo

Makara Journal of Technology

This paper proposes a dual-band left-handed circularly polarized triangular-patch array that is developed for land vehicle mobile system aimed at mobile satellite communications. The array consists of six tip-truncated triangular patches, which the first three patches are used for reception and the second three patches are used for transmission purpose. Each of three-patches has a beam pattern that can be switched in three different 120°-coverage beam in azimuth-cut plane at a minimum targeted gain at a desired elevation angle. The targeted minimum gain of the array is 5 dBic, in order for data communications with a large geostationary satellite can …


Uplift Of Shoreline Regions On Pagai Island Due To The September 12, 2007 Mw 8.4 Earthquake Captured By Sar Image, Ashar Muda Lubis Dec 2015

Uplift Of Shoreline Regions On Pagai Island Due To The September 12, 2007 Mw 8.4 Earthquake Captured By Sar Image, Ashar Muda Lubis

Makara Journal of Technology

At least 25 people were killed by the September 12, 2007 Mw 8.4 Bengkulu earthquake, and many buildings were destroyed in Bengkulu and West Sumatra provinces. It is very important to estimate the earth surface deformation due to the earthquake to understand the rupture size and its process. The aim of this research is to estimate the shoreline change and vertical displacement on Pagai Island associated with the September 12, 2007 Mw 8.4 Bengkulu earthquake. The intensity of ALOS-PALSAR satellite images is used to access the pattern of displacement. The result shows that Pagai Island demonstrated huge uplift due to …


Computational Simulation Of Mass Transport And Energy Transfer In The Microbial Fuel Cell System, Shiqi Ou Dec 2015

Computational Simulation Of Mass Transport And Energy Transfer In The Microbial Fuel Cell System, Shiqi Ou

Doctoral Dissertations

This doctoral dissertation introduces the research in the computational modeling and simulation for the microbial fuel cell (MFC) system which is a bio-electrochemical system that drives a current by using bacteria and mimicking bacterial interactions found in nature. The numerical methods, research approaches and simulation comparison with the experiments in the microbial fuel cells are described; the analysis and evaluation for the model methods and results that I have achieved are presented in this dissertation.

The development of the renewable energy has been a hot topic, and scientists have been focusing on the microbial fuel cell, which is an environmentally-friendly …


Size-Controlled Large-Diameter And Few-Walled Carbon Nanotube Catalysts For Oxygen Reduction, Xianliang Wang, Qing Li, Hengyu Pan, Ye Lin, Yujie Ke, Haiyang Sheng, Mark T. Swihart, Gang Wu Nov 2015

Size-Controlled Large-Diameter And Few-Walled Carbon Nanotube Catalysts For Oxygen Reduction, Xianliang Wang, Qing Li, Hengyu Pan, Ye Lin, Yujie Ke, Haiyang Sheng, Mark T. Swihart, Gang Wu

Faculty Publications

We demonstrate a new strategy for tuning the size of large-diameter and few-walled nitrogen-doped carbon nanotubes (N-CNTs) from 50 to 150 nm by varying the transition metal (TM = Fe, Co, Ni or Mn) used to catalyze graphitization of dicyandiamide. Fe yielded the largest tubes, followed by Co and Ni, while Mn produced a clot-like carbon morphology. We show that morphology is correlated with electrocatalytic activity for the oxygen reduction reaction (ORR). A clear trend of Fe > Co > Ni > Mn for the ORR catalytic activity was observed, in both alkaline media and more demanding acidic media. The Fe-derived N-CNTs exhibited …


Narrow-Linewidth Megahertz-Repetition-Rate Optical Parametric Oscillator For High-Speed Flow And Combustion Diagnostics, Naibo Jiang, Walter R. Lempert, Gary L. Switzer, Terrence R. Meyer, James R. Gord Nov 2015

Narrow-Linewidth Megahertz-Repetition-Rate Optical Parametric Oscillator For High-Speed Flow And Combustion Diagnostics, Naibo Jiang, Walter R. Lempert, Gary L. Switzer, Terrence R. Meyer, James R. Gord

Terrence R Meyer

We demonstrate the ability to generate ultra-high-frequency sequences of broadly wavelength-tunable, high-intensity laser pulses using a custom-built optical parametric oscillator pumped by the thirdharmonic output of a "burst-mode" Nd:YAG laser. Burst sequences consisting of 6-10 pulses separated in time by 6-10 Îs are obtained, with average total conversion efficiency from the 355 nm pump to the near-IR signal and idler wavelengths of 33%. Typical individual pulse output energy for the signal and idler beams is in the range of 4-6 mJ, limited by the available pump energy. Line narrowing is demonstrated by means of injection seeding the idler wave using …


Gasification Of Coal And Heat Integration Modification For Igcc - Integrated Gasification Combined Cycle, Dalia A. Ali Eng, Mamdouh A. Gadalla Prof., Fatma H. Ashour Prof. Oct 2015

Gasification Of Coal And Heat Integration Modification For Igcc - Integrated Gasification Combined Cycle, Dalia A. Ali Eng, Mamdouh A. Gadalla Prof., Fatma H. Ashour Prof.

Chemical Engineering

Use of energy is closely related to the development of an economy. The most useful form of energy in the modern world is electricity. IGCC has higher fuel flexibility (biomass, refinery residues, petroleum coke, etc.) and generates multiple products (electricity, hydrogen and chemicals like methanol and higher alcohols) and by-products - sulphur, sulphuric acid, slag, etc. IGCC plants include coal preparation unit, air separation unit (ASU) to separate oxygen from air to use it in the gasification process, gasification unit where an incomplete combustion for coal is made to produce Syngas, cleaning unit to remove acid gases and CO2 from …


Three-Dimensional Confocal Microscopy Indentation Method For Hydrogel Elasticity Measurement, Donghee Lee, Md Mahmudur Rahman, You Zhou, Sangjin Ryu Aug 2015

Three-Dimensional Confocal Microscopy Indentation Method For Hydrogel Elasticity Measurement, Donghee Lee, Md Mahmudur Rahman, You Zhou, Sangjin Ryu

Md Mahmudur Rahman

No abstract provided.


A New Method For Simulating Power Flow Density Focused By A Silicon Lens Antenna Irradiated With Linearly Polarized Thz Wave, Catur Apriono, Eko Tjipto Rahardjo, Norihisa Hiromoto Aug 2015

A New Method For Simulating Power Flow Density Focused By A Silicon Lens Antenna Irradiated With Linearly Polarized Thz Wave, Catur Apriono, Eko Tjipto Rahardjo, Norihisa Hiromoto

Makara Journal of Technology

A terahertz system uses dielectric lens antennas for focusing and collimating beams of terahertz wave radiation. Linearly polarized terahertz wave radiation has been widely applied in the terahertz system. Therefore, an accurate method for analyzing the power flow density in the dielectric lens antenna irradiated with the linearly polarized terahertz wave radiation is important to design the terahertz systems. In optics, ray-tracing method has been used to calculate the power flow density by a number density of rays. In this study, we propose a method of ray-tracing combined with Fresnel’s transmission, including transmittance and polarization of the terahertz wave radiation …


Application Of Fiscal Incentives For Development Of East Natuna Gas Field For Long-Term National Natural Gas Demand, Marwan Batubara, Widodo Wahyu Purwanto, Akhmad Fauzi Aug 2015

Application Of Fiscal Incentives For Development Of East Natuna Gas Field For Long-Term National Natural Gas Demand, Marwan Batubara, Widodo Wahyu Purwanto, Akhmad Fauzi

Makara Journal of Technology

East Natuna gas field, which has proven reserves of 46 trillion cubic feet, is projected to meet long-term natural gas needs. However, CO2-content of the gas reserves reaches 71%, leading to expensive development costs. This research investigates the feasibility of the field based on several fiscal incentives. Firstly, gas supply-demand until year 2040 was analyzed. Then, based on the analysis, the field was developed using high CO2 gas separation technology to produce gas of 1300 MMSCFD in 2023, 2600 MMSCFD in 2031, and 3900 MMSCFD in 2039. Finally, the economic feasibility was assessed using cash flow analysis in accordance with …


Stochastic Optimization Of Supply Chain Risk Measures –A Methodology For Improving Supply Security Of Subsidized Fuel Oil In Indonesia, Adinda Yuanita, Andi Noorsaman Sommeng, Anondho Wijonarko Aug 2015

Stochastic Optimization Of Supply Chain Risk Measures –A Methodology For Improving Supply Security Of Subsidized Fuel Oil In Indonesia, Adinda Yuanita, Andi Noorsaman Sommeng, Anondho Wijonarko

Makara Journal of Technology

Monte Carlo simulation-based methods for stochastic optimization of risk measures is required to solve complex problems in supply security of subsidized fuel oil in Indonesia. In order to overcome constraints in distribution of subsidized fuel in Indonesia, which has the fourth largest population in the world—more than 250,000,000 people with 66.5% of productive population, and has more than 17,000 islands with its population centered around the nation's capital only—it is necessary to have a measurable and integrated risk analysis with monitoring system for the purpose of supply security of subsidized fuel. In consideration of this complex issue, uncertainty and probability …


Thermodynamic Analysis Of Irreversible Heat-Transformers, Niccolo` Giannetti, Arnas Arnas, Andrea Rocchetti, Kiyoshi Saito Aug 2015

Thermodynamic Analysis Of Irreversible Heat-Transformers, Niccolo` Giannetti, Arnas Arnas, Andrea Rocchetti, Kiyoshi Saito

Makara Journal of Technology

Absorption heat transformers extend the possibilities for efficient and environment-friendly energy conversion processes. Based on a general thermodynamic model of three-thermal cycles with finite thermal capacity of the heat sources, this paper is intent upon analyzing and optimizing the performance of absorption heat transformers, by including the influence of irreversibility in the analytical expression of the system efficiency. Dimensionless parameters for an overall optimization are defined and a first screening is performed to clarify their influence. Dependence on the main factors is highlighted to suggest how to change them in order to enhance the whole system performance. Under this point …


Effects Of Supplier-Manufacturer Relationships On Supply-Chain Performance Of Manufacturing Industries In Indonesia, Rachmad Hidayat, Khisbullah Hudha, Sabarudin Akhmad Aug 2015

Effects Of Supplier-Manufacturer Relationships On Supply-Chain Performance Of Manufacturing Industries In Indonesia, Rachmad Hidayat, Khisbullah Hudha, Sabarudin Akhmad

Makara Journal of Technology

The present study describes the relationships between commitment, communication, satisfaction, trust, relationship quality with suppliers, and supply-chain performance. The population of the study was manufacturing companies in Indonesia. Respondents were the chief executive officers or corporate secretaries or the designated managers involved in strategic decision making. Samples were taken by using a proportional area random sampling technique. Structural Equation Modeling (SEM) was used for analysis. Results of both direct and indirect testing of hypothesis indicated two hypotheses of positive and significant effects and nine hypotheses of positive but insignificant effects. Those hypotheses of positive and significant effects were the direct …


Transmission Electron Microscopy Characterization Of High-Temperatur Oxidation Of Fe-20cr-5al Alloy Prepared By Focused Ion Beam Technique, Mohammad Dani, Pudji Untoro, Teguh Yulius Surya Panca Putra, Parikin Parikin, Joachim Mayer, Arbi Dimyati Aug 2015

Transmission Electron Microscopy Characterization Of High-Temperatur Oxidation Of Fe-20cr-5al Alloy Prepared By Focused Ion Beam Technique, Mohammad Dani, Pudji Untoro, Teguh Yulius Surya Panca Putra, Parikin Parikin, Joachim Mayer, Arbi Dimyati

Makara Journal of Technology

The Focused Ion Beam (FIB) technique was applied for cross section preparation of the oxidized alloy for Transmission Electron Microscopy (TEM) study. Prior to preparation, the specimens of Fe-20Cr-5Al alloy sheet were oxidized in air at 1200 oC for 2 minutes, 10 minutes, 2 hours, and 100 hours. The microstructure and elemental composition of the samples were characterized using TEM equipped with an Energy Dispersive X-Ray Spectroscopy (EDX). The Electron Energy Loss Spectroscopy (EELS) was used to determine of the light elements. The TEM investigation reveals remarkable microstructure evolution of the specimens during oxidation which generally exhibit a typical multi-layer …


High Temperature Corrosion Of Aluminized Aisi 4130 Steel With The Different Composition Of Nacl/Na2so4 Deposits, Mohammad Badaruddin, Chaur Jeng Wang, Yudhistyra Saputra, Abu Khalid Rivai Aug 2015

High Temperature Corrosion Of Aluminized Aisi 4130 Steel With The Different Composition Of Nacl/Na2so4 Deposits, Mohammad Badaruddin, Chaur Jeng Wang, Yudhistyra Saputra, Abu Khalid Rivai

Makara Journal of Technology

The high temperature corrosion of AISI 4130 steel can be increased by hot-dip aluminizing coating. The aluminized steel specimens with the deposit composition of 100/0, 30/70, 50/50, 70/30, and 0/100 (wt.%) NaCl/Na2SO4 were oxidized at 750 °C for 1-49 h periods. According to a parabolic rate constant (kp) value, the aluminized steel with deposit composition of 70/30 NaCl/Na2SO4 shows the highest kp value (3.71 × 10-11 g2cm- 4s-1), later followed by the kp value of 3.35 × 10-11 g2cm-4s-1 for 100/0 and the lowest kp value is 7.731 × 10-12 g2cm-4s-1 for 0/100. Whereas, the kp value for the aluminized …


Swelling-Etching Characterization Of Copper (I) Oxide - Pdms For The Development Of Micro/Nano - Particles Composite Mems Corrosion Sensor, Abdoul Kader Maiga Jul 2015

Swelling-Etching Characterization Of Copper (I) Oxide - Pdms For The Development Of Micro/Nano - Particles Composite Mems Corrosion Sensor, Abdoul Kader Maiga

Graduate Theses and Dissertations

The primary objective for this thesis is to contribute to the understanding of the oxide removal process for a corrosion sensing device. The goal for designing such a device is for monitoring corrosion on metallic structures. The sensing material (6.35mm x 1mm discs) of the device is composed of copper (I) oxide particles mixed in some polydimethylsiloxane (PDMS). The PDMS, “housing,” is meant for controlling the oxidation rate through the sensing material. A solvent was used to facilitate the etchant diffusion through the PDMS matrix. Toluene and acetic acid were the ideal solvent and etchant, respectively, for carrying out the …


Design & Analysis Of Ø40” X 80” Conventional Sugar Mill Head Stock., Santosh Y. Salunkhe Jul 2015

Design & Analysis Of Ø40” X 80” Conventional Sugar Mill Head Stock., Santosh Y. Salunkhe

Innovative Research Publications IRP India

Sugar mill head stock play a significant role in the sugar plant as they have to sustain the forces experienced by the rollers while extracting juice from the cane. The present analysis related to modification in sugar mill head stock Ø40”X80”. This paper describes the advantages of using Ø40”X80” mill head stocks by designing & analysis by ANSYS software. In this study theoretical study has been done considering the Bending moment & force polygon diagrams. Bending moment factor which helps in finding actual results. By changing various parameters the performance of mill head stocks is studies using static structural analysis …


Mechanism Of Sulfur Poisoning Of Sr2Fe1.5Mo0.5O6-Δ Perovskite Anode Under Solid Oxide Fuel Cell Conditions, Eric Walker, Salai Ammal, Suwit Suthirakun, Fanglin Chen, Gabriel Terejanu, Andreas Heyden May 2015

Mechanism Of Sulfur Poisoning Of Sr2Fe1.5Mo0.5O6-Δ Perovskite Anode Under Solid Oxide Fuel Cell Conditions, Eric Walker, Salai Ammal, Suwit Suthirakun, Fanglin Chen, Gabriel Terejanu, Andreas Heyden

Salai C. Ammal

No abstract provided.


Significantly Improved Photocurrent Response Of Zns-Reduced Graphene Oxide Composites May 2015

Significantly Improved Photocurrent Response Of Zns-Reduced Graphene Oxide Composites

Faculty of Engineering University of Malaya

ZnS-nanoparticles (NPs) reduced graphene oxide (rGO) composites with a high degree of crystallinity and high dispersity were successfully synthesized via a facile solvothermal method in the gelatin medium, during which the formation of ZnS NPs, reduction of graphene oxide and loading of ZnS NPs into the rGO surface occur simultaneously. Gelatin, as a natural capping agent, plays a significant role in controlling the degree of dispersion and coverage of ZnS NPs. The effect of rGO on the crystalline structure and optical properties of ZnS NPs were determined via X-ray diffraction, UV-visible diffused reflectance spectroscopy and photoluminescence spectroscopy. The ZnS-rGO composites …


Effects Of Biomass Moisture Content On Volatile Flame Length During Cofiring With Coal, Matthew Pollard May 2015

Effects Of Biomass Moisture Content On Volatile Flame Length During Cofiring With Coal, Matthew Pollard

McKelvey School of Engineering Theses & Dissertations

Cofiring biomass with coal can contribute to meeting Renewable Portfolio Standards (RPS) and reduce pollutant emissions. The physical characteristics and composition of biomass can vary significantly, which can affect the combustion characteristics. When cofiring biomass with coal, these differences can impact the structure of the volatile flame, the region where combustion of volatiles dominates. The length and location of the volatile flame is important to flame stability and determines the location and extent of volatile release. This has an effect on pollutant emissions, such as NOx (nitrogen oxides). Previously, the effects of parameters such as cofiring ratio, particle size, and …


Experimental And Numerical Investigation Of Heat Transfer In Cnt Nanofluids May 2015

Experimental And Numerical Investigation Of Heat Transfer In Cnt Nanofluids

Faculty of Engineering University of Malaya

Nanofluids with their enhanced thermal conductivity are believed to be a promising coolant in heat transfer applications. In this study, carbon nanotube (CNT) nanofluids of 0.01wt%, stabilised by 1.0wt% gum arabic were used as a cooling liquid in a concentric tube laminar flow heat exchanger. The flow rate of cold fluid varied from 10 to 50g/s. Both experimental and numerical simulations were carried out to determine the heat transfer enhancement using CNT nanofluids. Computational fluid dynamics (CFD) simulations were carried out using Fluent v 6.3 by assuming single-phase approximation. Thermal conductivity, density and rheology of the nanofluid were also measured …


Characterization Of Nano-Porous Si-Cu Composites To Enhance Lubricant Retention Impacting The Tribological Properties Of Sliding Surfaces, Julius Sheldon Morehead May 2015

Characterization Of Nano-Porous Si-Cu Composites To Enhance Lubricant Retention Impacting The Tribological Properties Of Sliding Surfaces, Julius Sheldon Morehead

Graduate Theses and Dissertations

As the expectations for modern machinery's tribological and thermal performances continue to rise, the retention of lubricant on the contact surfaces of their sliding components becomes an increasingly important issue. Friction and wear cause heat-related failures which lead to catastrophic damage to machinery. Evaporation of a lubricant's volatile constituents as well as lubricant migration leads not only to a reduction in lubricant quantity but also in its quality, thus facilitating component failures. In order to enhance component reliability, the surface should incorporate features that actively retain lubricants. The unique properties of nano-porous topographies such as their high surface area-to-volume ratio …


The Tribological And Electrochemical Behavior Of Hvof-Sprayed Cr3c2-Nicr Ceramic Coating On Carbon Steel May 2015

The Tribological And Electrochemical Behavior Of Hvof-Sprayed Cr3c2-Nicr Ceramic Coating On Carbon Steel

Faculty of Engineering University of Malaya

High Velocity Oxygen Fuel (HVOF) is an excellent approach to prepare a good, wear-resistant lamella of Chromium Carbide-Nickel Chrome (Cr3C2-NiCr) on carbon steel for high temperature application. This research investigates the effect of a thin, deposited layer of Cr3C2-NiCr on carbon steel in terms of wear and corrosion properties. The microstructure of the HVOF-sprayed Cr3C2-NiCr coating was characterized at each step by scanning electron microscopy. Wear testing was performed with a pin-on-disk tester. Wear weight loss was examined by applying different loads over a 9048.96 m sliding distance. Experimental results show that the wear resistance of the coated sample reduced …


A Label-Free High Throughput Resistive-Pulse Sensor For Simultaneous Differentiation And Measurement Of Multiple Particle-Laden Analytes, Ashish Jagtiani, Rupesh Sawant, Jiang Zhe Apr 2015

A Label-Free High Throughput Resistive-Pulse Sensor For Simultaneous Differentiation And Measurement Of Multiple Particle-Laden Analytes, Ashish Jagtiani, Rupesh Sawant, Jiang Zhe

Dr. Jiang Zhe

We describe an all-electronic, label-free, resistive-pulse sensor that utilizes multiple microchannels for parallel detection, counting and differentiation of multiple biological particles simultaneously. Four particle solutions, including 20 µm and 40 µm polymethacrylate particles, Juniper Scopulorum (Rocky Mountain Juniper) pollen and Populus deltidoes (Eastern Cottonwood) pollen, were loaded to the four peripheral reservoirs, respectively, and were driven to the central reservoir through four microchannels, all operating simultaneously for particle detection and counting. Experiments demonstrated that this sensor was able to differentiate and count multiple particle solutions simultaneously through its four microchannels fabricated on polymer membranes. Thus the sensing throughput has been …


Effect Of Processing Conditions On The Development Of Morphology In Clay Nanoparticle Filled Nylon 6 Fibers, Zeynep Ergungor, Mukerrem Cakmak, Celal Batur Apr 2015

Effect Of Processing Conditions On The Development Of Morphology In Clay Nanoparticle Filled Nylon 6 Fibers, Zeynep Ergungor, Mukerrem Cakmak, Celal Batur

Dr. Celal Batur

The effect of melt temperature on the phase behavior and preferential orientation development in Nylon 6/montmorillonite nanocomposites were investigated at melt spinning temperatures ranging from 230° to 250°C. The fibers were found to exhibit mostly γ crystalline form that is typical of Nylon 6 filled with montmorillonite nanoparticles. At higher take-up speeds α-crystals begin to appear in the crystalline phase. The presence of nanoparticles was found to impart substantial chain orientation levels even at low to moderate take up speeds reaching a plateau at moderate take up speeds. This was attributed to the increased spin line stress in the presence …