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Full-Text Articles in Engineering Science and Materials
Microstructure Of Electrodeposited Copper Foil: Discussion On The Mechanism Model Of Three-Dimensional Electrocrystallization, Ren-Zhi Liu, Ping-Ling Xie, Chong Wang
Microstructure Of Electrodeposited Copper Foil: Discussion On The Mechanism Model Of Three-Dimensional Electrocrystallization, Ren-Zhi Liu, Ping-Ling Xie, Chong Wang
Journal of Electrochemistry
The manufacturing of electrolytic copper foil has attracted more and more attention with the extensive applications of printed circuit board and lithium battery. The industrial scale is still extending. Compared with the developments of electroplating equipment and electroplating process, there is limited research on the mechanism of electrodeposition. This paper summarizes the manufacturing process of electrodeposited copper foil and analyzes the differences of various electroplating parameters in different electrodeposited copper technologies, and points out the important role of electrodeposition current density in the formation of copper foil. By showing and comparing the microstructures of different electrodeposited copper foils, the influences …
Electrode Of Metallic Oxides Coated Titanium With Interlayer, Yi Tang, Li-Kun Xu, Yong-Lei Xin, Jun-Tao Wang, Ping Long
Electrode Of Metallic Oxides Coated Titanium With Interlayer, Yi Tang, Li-Kun Xu, Yong-Lei Xin, Jun-Tao Wang, Ping Long
Journal of Electrochemistry
Various Ti/IrRuSn,Ti/IrTa/IrRuSn and Ti/IrTaSn/IrRuSn oxide electrodes were prepared by sol-gel method.The surface morphology and microstructure were analysed with FESEM and XRD.The electrochemical activity and stability were investigated using electrochemical technologies including chlorine and oxygen evolving potential measurements,cyclic voltammetry,accelerated life test,and alternative electrolysis.The results indicate that the electrodes with interlayers present more cracks on the surface and a little bigger average grain size,with particles of different shapes precipitated in the cracks.The electroactive sites are increased and the selectivity for the chlorine evolving reaction is enhanced,but the current efficiency for the chlorine production is somewhat lowered by the addition of different interlayers.The …
Study On The Microstructure Of Pb-Sn Alloy Obtained From Quasi-Two-Dimensional Electrodeposition, Bin Sun
Study On The Microstructure Of Pb-Sn Alloy Obtained From Quasi-Two-Dimensional Electrodeposition, Bin Sun
Journal of Electrochemistry
A two-layered structure of eutectic-solid sulotion is formed in the microstructure of Pb-Sn alloy obtained from quasi-two-dimensional electrodeposition.It is showed that this unique structure is caused by the variation of the current density on the growth interface.When the interface is located in the front of the whole deposits,the current density is high.So the Pb and Sn can deposit together and the eutectic texture forms.When the interface is in the rear of the whole deposits,the current density is low.At this moment the electrodeposition of Pb is the dominant reaction,and the Pb-based solid solution appears.
On Misorientation Distribution Evolution During Anisotropic Grain Growth, Elizabeth A. Holm, Gregory N. Hassold, Mark A. Miodownik
On Misorientation Distribution Evolution During Anisotropic Grain Growth, Elizabeth A. Holm, Gregory N. Hassold, Mark A. Miodownik
Physics Publications
In order to study the development of texture and boundary character during annealing, three-dimensional grain crystallography and crystallographically mediated grain boundary properties were incorporated into a finite temperature Monte Carlo model for grain growth. Randomly textured microstructures evolve normally, with growth exponent n=0.96. While texture remains random, the steady-state boundary misorientation distribution favors low-angle boundaries. To first order, low-angle boundaries increase by lengthening, not by proliferating. In contrast, microstructures with a strong single-component texture develop four-grain junctions and highly curved grain boundaries, which alter evolution. The boundary misorientation distribution narrows and shifts to low angles, and no steady state …
An Analysis On The Microstructure Of Electrodeposited Zro 2 Ni Functionally Graded Materials, Chengjun Quan, Xinghua Xiang, Jingchuan Zhu, Zhongda Yin
An Analysis On The Microstructure Of Electrodeposited Zro 2 Ni Functionally Graded Materials, Chengjun Quan, Xinghua Xiang, Jingchuan Zhu, Zhongda Yin
Journal of Electrochemistry
The electrodeposited ZrO 2 Ni functionally graded coating was fabricated by controlling the ZrO 2 concentration in the bath, and the microstructure was analyzed by X Ray Diffraction (XRD) and Electron Probe Microanalysis (EPMA). The results show that the functionally graded coating has excellent compositional gradient distribution from the substrate to the surface. The content of ZrO 2 is up to 14.4 vol% in the surface layer and the coating consists of the t ZrO 2, m ZrO 2 and Ni phases. Owing to the ZrO 2 particles pressed by Ni atoms during electrodepositing, t→m transformation has occurred.