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Nanoscience and Nanotechnology

Nanocrystalline Fe

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Full-Text Articles in Engineering Science and Materials

Resistance To Helium Bubble Formation In Amorphous Sioc/Crystalline Fe Nanocomposite, Qing Su, Tianyao Wang, Jonathan Gigax, Lin Shao, Michael Nastasi Jan 2019

Resistance To Helium Bubble Formation In Amorphous Sioc/Crystalline Fe Nanocomposite, Qing Su, Tianyao Wang, Jonathan Gigax, Lin Shao, Michael Nastasi

Department of Mechanical and Materials Engineering: Faculty Publications

The management of radiation defects and insoluble He atoms represent key challenges for structural materials in existing fission reactors and advanced reactor systems. To examine how crystalline/amorphous interface, together with the amorphous constituents affects radiation tolerance and He management, we studied helium bubble formation in helium ion implanted amorphous silicon oxycarbide (SiOC) and crystalline Fe composites by transmission electron microscopy (TEM). The SiOC/Fe composites were grown via magnetron sputtering with controlled length scale on a surface oxidized Si (100) substrate. These composites were subjected to 50 keV He+ implantation with ion doses chosen to produce a 5 at% peak He …


Dose Dependence Of Radiation Damage In Nano-Structured Amorphous Sioc/Crystalline Fe Composite, Qing Su, Lloyd Price, Lin Shao, Michael Nastasi Jan 2016

Dose Dependence Of Radiation Damage In Nano-Structured Amorphous Sioc/Crystalline Fe Composite, Qing Su, Lloyd Price, Lin Shao, Michael Nastasi

Department of Mechanical and Materials Engineering: Faculty Publications

Through examination of radiation tolerance properties of amorphous silicon oxycarbide (SiOC) and crystalline Fe composite to averaged damage levels, from approximately 8 to 30 displacements per atom (dpa), we demonstrated that the Fe/SiOC interface and the Fe/amorphous FexSiyOz interface act as efficient defect sinks and promote the recombination of vacancies and interstitials. For thick Fe/SiOC multilayers, a clear Fe/SiOC interface remained and no irradiation-induced mixing was observed even after 32 dpa. For thin Fe/SiOC multilayers, an amorphous FexSiyOz intermixed layer was observed to form at 8 dpa, but no further …


Temperature-Dependent Helium Ion-Beam Mixing In An Amorphous Sioc/Crystalline Fe Composite, Qing Su, Lloyd Price, Lin Shao, Michael Nastasi Jan 2016

Temperature-Dependent Helium Ion-Beam Mixing In An Amorphous Sioc/Crystalline Fe Composite, Qing Su, Lloyd Price, Lin Shao, Michael Nastasi

Department of Mechanical and Materials Engineering: Faculty Publications

Temperature dependent He-irradiation-induced ion-beam mixing between amorphous silicon oxycarbide (SiOC) and crystalline Fe was examined with a transmission electron microscope (TEM) and via Rutherford backscattering spectrometry (RBS). The Fe marker layer (7.2 ± 0.8 nm) was placed in between two amorphous SiOC layers (200 nm). The amount of ion-beam mixing after 298, 473, 673, 873, and 1073 K irradiation was investigated. Both TEM and RBS results showed no ion-beam mixing between Fe and SiOC after 473 and 673 K irradiation and a very trivial amount of ion-beam mixing (~2 nm) after 298 K irradiation. At irradiation temperatures higher than 873 …