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Biomedical Engineering and Bioengineering Commons

Open Access. Powered by Scholars. Published by Universities.®

1999

Scanning electron microscopy

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Full-Text Articles in Biomedical Engineering and Bioengineering

Mechanical Properties Of Dendritic Pd-Cu-Ga Dental Alloys, Efstratios Papazoglou, Qiang Wu, William A. Brantley, John C. Mitchell, Glyn Meyrick Jan 1999

Mechanical Properties Of Dendritic Pd-Cu-Ga Dental Alloys, Efstratios Papazoglou, Qiang Wu, William A. Brantley, John C. Mitchell, Glyn Meyrick

Cells and Materials

Three Pd-Cu-Ga dental alloys with very similar nominal compositions and dendritic as-cast microstructures were selected for study: Option (Ney Dental) and Spartan (Williams/lvoclar) contain a small amount of boron, while Spartan Plus (Williams/Ivoclar) is boron-free. Bars of each alloy were tested in tension for the as-cast and simulated porcelain-firing conditions, and values of mechanical properties were measured. Fracture surfaces and microstructures of axially sectioned and etched fracture specimens were observed with the scanning electron microscope (SEM). Except for the elastic modulus, significant differences were typically found in alloy properties. Heat treatment eliminated the dendritic microstructure, decreased strength and increased ductility. …


X-Ray Diffraction And Scanning Electron Microscopy Analyses Of A Gallium-Based Dental Restorative Alloy, Randa E. Shaker, William A. Brantley, Qiang Wu, John C. Mitchell Jan 1999

X-Ray Diffraction And Scanning Electron Microscopy Analyses Of A Gallium-Based Dental Restorative Alloy, Randa E. Shaker, William A. Brantley, Qiang Wu, John C. Mitchell

Cells and Materials

Specimens of a gallium-based dental alloy were prepared with different condensation techniques, with and without the removal of a surface layer, and after aging for 2 hours at 50°, 100° and 150°C. X-ray diffraction at times ranging from 10 minutes to 1 day showed the development of the four matrix phases (ß-Sn, CuGa2, Ga28Ag72, and In4Ag9) during the setting reaction. Scanning electron microscope (SEM) examination of specimens loaded to failure revealed brittle fracture, with greater porosity for hand-condensed specimens, and provided insight into crack propagation processes. Aging increased …


Effects Of Casting Conditions And Annealing On Microstructures And Vickers Hardness Of Dendritic Pd-Cu-Ga Dental Alloys, William A. Brantley, Qiang Wu, Zhuo Cai, Stanley G. Vermilyea, John C. Mitchell, Michael C. Comerford Jan 1999

Effects Of Casting Conditions And Annealing On Microstructures And Vickers Hardness Of Dendritic Pd-Cu-Ga Dental Alloys, William A. Brantley, Qiang Wu, Zhuo Cai, Stanley G. Vermilyea, John C. Mitchell, Michael C. Comerford

Cells and Materials

Three Pd-Cu-Ga alloys with as-cast dendritic microstructures and very similar compositions, two containing less than 1 wt% boron and the third boron-free, were cast with normal bench-cooling or rapid-quenching into water. Quenched specimens were also heat treated at temperatures of 1000°, 1200°, 1500° and 1800°F that span the firing cycles for dental porcelain. Similar values of Vickers hardness were observed for all three alloys, suggesting little effect from boron on yield strength. The hardness was relatively insensitive to the experimental conditions, except for heat treatment at 1500° and 1800°F where significant softening occurred with transformation of the microstructure to Pd …