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Biomedical Engineering and Bioengineering Commons

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Journal

X-ray microanalysis

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Full-Text Articles in Biomedical Engineering and Bioengineering

Corrosion Of Metal Hip Arthroplasties And Its Possible Role In Loosening, H. K. Koerten, J. J. A. M. Van Raay, J. J. M. Onderwater, F. P. Bernoski, P. M. Rozing Jan 1997

Corrosion Of Metal Hip Arthroplasties And Its Possible Role In Loosening, H. K. Koerten, J. J. A. M. Van Raay, J. J. M. Onderwater, F. P. Bernoski, P. M. Rozing

Cells and Materials

Tissue removed with human hip arthroplasties during revision surgery of 45 patients was evaluated by transmission electron microscopy and X -ray microanalysis (XRMA). The results show that microscopic and submicroscopic particles are abundantly present in the tissue at the tissue/implant interface. XRMA of individual particles shows that the chemical composition of a portion of the particles was in agreement with that of the retrieved implants. Regularly, particulates with a dissimilar chemical composition were found. Sometimes, these particles could be recognized as filler particles of the cements used. Other particles could partly or completely be composed of the chemical elements that …


Some Observations On The Structure Of Encrusting Biofilms Of Proteus Mirabilis On Urethral Catheters, C. Winters, D. J. Stickler, N. S. Howe, T. J. Williams, N. Wilkinson, C. J. Buckley Jan 1995

Some Observations On The Structure Of Encrusting Biofilms Of Proteus Mirabilis On Urethral Catheters, C. Winters, D. J. Stickler, N. S. Howe, T. J. Williams, N. Wilkinson, C. J. Buckley

Cells and Materials

A physical model of the bladder has been used to study the process of urinary catheter encrustation. Techniques have been devised for the preparation of sections through these encrustations in situ on the luminal surfaces of catheters and for mapping the distribution of calcium and magnesium in the biofilms. Transmission electron microscopy on these sections showed struvite-like crystals lying in the matrix and in direct contact with the catheter surface. Calcium phosphate ("bioapatite") was distributed throughout the film and many of these amorphous particles appear to have cells at their cores. Freeze-substituted sections of biofilms also showed electron dense materials …


In Vitro Studies Of Encrustations On Catheters, A Model Of Infection Stone Formation, W. Schmitz, A. Nolde, G. Marklein, A. Hesse Jan 1993

In Vitro Studies Of Encrustations On Catheters, A Model Of Infection Stone Formation, W. Schmitz, A. Nolde, G. Marklein, A. Hesse

Cells and Materials

Deposition of infection-induced stone material on urinary catheters is a common problem in urological patients. Therefore, a crystallization model was developed in order to form this material in a reproducible manner. Furthermore, the dissolving potency of two solutions (Suby-G® and Solution-R®) was investigated with this model. The encrustations were examined by infrared (IR) spectroscopy, chemical encrustation analysis , scanning electron microscopy (SEM) and X-ray microanalysis. In addition, the encrustations were calculated from the results of the urine analysis, before and after each experiment, as contents remaining in each artificial bladder. The model conditions changed during the experiment and led to …


Pulpal Response To Calcium Phosphate Materials. In Vivo Study Of Calcium Phosphate Materials In Endodontics, A. H. Jean, J. A. Pouezat, G. Daculsi Jan 1993

Pulpal Response To Calcium Phosphate Materials. In Vivo Study Of Calcium Phosphate Materials In Endodontics, A. H. Jean, J. A. Pouezat, G. Daculsi

Cells and Materials

The aim of this study was to determine if calcium phosphate (CaP) materials could be used to substitute for calcium hydroxide (CH) as a pulp capping agent. Especially prepared and characterized CaP materials with CH as the reference or control material were used for pulpcapping teeth of pigs, rats, and dogs. The CaP materials included: DCPD (dicalcium phosphate dihydrate), OCP (octacalcium phosphate), ß-TCP ({3-tricalcium phosphate), BCP (biphasic calcium phosphate mixture of 50150 HA and ß-TCP), and HA (hydroxyapatite) which were used in particle sizes of < 5 μm or < 150 μm. The animals were sacrificed after 21 days to …


In-Vivo Reactions In Some Bioactive Glasses And Glass-Ceramics Granules, A. M. Gatti, T. Yamamuro, L. L. Hench, O. H. Andersson Jan 1993

In-Vivo Reactions In Some Bioactive Glasses And Glass-Ceramics Granules, A. M. Gatti, T. Yamamuro, L. L. Hench, O. H. Andersson

Cells and Materials

Two different bioactive glasses and one glass-ceramic were implanted as granules for 2 months in rabbit muscle and for 5 months in sheep jaw in order to study the influence of the biological surroundings on the reactions of the materials.

Scanning electron microscope and energy dispersive X-ray microanalysis showed that a calcium and phosphorous-rich (CaP) surface layer (adjacent to a silicon rich-layer) forms on both glasses in both implantation sites. The glass-ceramic developed only a CaP layer. A chemical process of degradation was more evident in muscle, even though the implantation time was shorter than that in bone. For all …