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Fracture Toughness Improvement Of ����� Ceramics By Grain Size Control And Ductile Phase Reinforcement, Kesong Wang
Fracture Toughness Improvement Of ����� Ceramics By Grain Size Control And Ductile Phase Reinforcement, Kesong Wang
McKelvey School of Engineering Theses & Dissertations
This study used grain size control and ductile phase reinforcement to improve fracture toughness of ����� ceramics. Alpha alumina particles of 100 nm, 0.5-1 micrometers, and 10 micrometers were coated with 1-5 nm nickel by electroless nickel plating (ENP). The coated powders were consolidated at 1200℃-1500℃ by spark plasma sintering (SPS). The sintered samples were annealed at 1100 oC for 1.5 hours and 10 hours to determine the effect of post sintering annealing on hardness and fracture toughness. Density of the samples were measured by the standard Archimedes method using a 5 mL pycnometer. Hardness values were determined by Vickers …