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Stainless-Steel Column For Robust High Temperature Microchip Gas Chromatography, Abhijit Ghosh, Austin R. Foster, Jacob C. Johnson, Carlos R. Vilorio, Luke T. Tolley, Brian D. Iverson, Aaron R. Hawkins, H. Dennis Tolley, Milton L. Lee
Stainless-Steel Column For Robust High Temperature Microchip Gas Chromatography, Abhijit Ghosh, Austin R. Foster, Jacob C. Johnson, Carlos R. Vilorio, Luke T. Tolley, Brian D. Iverson, Aaron R. Hawkins, H. Dennis Tolley, Milton L. Lee
Faculty Publications
This paper reports the first results of a robust, high performance, stainless-steel microchip gas chromatography (GC) column that is capable of analyzing complex real world mixtures as well as operating at very high temperatures. Using a serpentine design, a 10 m column with an approximately semicircular cross section with a 52 µm hydraulic diameter (Dh) was produced in a 17 cm x 6.3 cm x 0.1 cm rectangular steel chip. The channels were produced using a multilayer chemical etch and diffusion bonding process, and metal nuts were brazed onto the inlet and outlet ports allowing for column interfacing …