Engineering Commons^™

Optimization Of The Hot Embossing Parameters And Sintering Characterization For Alumina/Berea Sandstone Sintering, Justin F. Robbins

LSU Master's Theses

The purpose of this study is to investigate the process of hot embossing on alumina based ceramics as a cost-efficient procedure for manufacturing microfluidic testing components. Alumina ceramics were used as an exploratory phase for the final objective of the project, manufacturing of Berea sandstone based ceramic samples. Previous research has shown potential in using hot embossing on Alumina based ceramics; however, complications with extrusion and micro-structure quality were observed. For this reason, the research performed aimed to produce Berea Sandstone based components by first improving upon the embossing quality of alumina ceramics.

The thesis first investigates changes in the …

Biomass Catalytic Upconversion With A Metallic Catalyst Bed Under Radio Frequency Induction Heating, Mohammad Abu-Laban

LSU Master's Theses

This study investigated the thermal performances of platinum particles when coupled on a steel support, under the application of a radio frequency (RF) field. Platinum nanoparticles were reduced on the surfaces of type-316 stainless steel balls, based on published methods of Pt reduction from chloroplatinic acid. Alternatively, 1wt. % Pt/Al2O3 commercial catalyst pellets were mixed with stainless steel balls and investigated for hydro-deoxygenation of pyrolysis oil from pine sawdust biomass. The catalysts were placed inside an electric insulator tube suspended within a looping copper coil connected to the induction heater, and heated at different power levels. An infrared camera was …

Pool Boiling Enhancement Via Micro Ratchets, Lance Austin Brumfield

LSU Master's Theses

Nucleate boiling is an attractive method for achieving high heat flux at low superheat temperatures. It is frequently used for industrial applications such as heat exchangers and is being considered to cool advanced central processing units (CPU) which produce heat fluxes on the order of 1 MW/m2 and are becoming increasing less efficient to cool via forced conduction of air. The issues with implementing nucleate boiling as a cooling mechanism lies in the difficulty of quantifying the complex and numerous mechanisms which control the process. A comprehensive nucleate boiling model has yet to be formulated and will required in order …

The Design And Modification Of A Sputter System For Dc Reactive Sputtering Of Alumina And Zirconia Thin Films, Diane Van Ho

LSU Master's Theses

Yttria-stabilized zirconia (7% YSZ) is the most used material for thermal barrier coatings (TBCs) to reduce the conductive heat transfer on turbine blades, but it is not resistant to infrared radiation. In order to reduce radiation heat transfer, alternating materials, such as alumina and zirconia, can be used to fabricate multi-layer coatings in which each layer is optimized to reflect a targeted range of wavelength. This research aims to fabricate these multi-layer coatings by reactive magnetron sputtering. Reactive magnetron sputtering is the sputtering of an elemental target in the presence of a reactive gas that will react with the target …

Zeolite And Metal Oxide Catalysts For The Production Of Dimethyl Sulfide And Methanethiol, Craig Plaisance

LSU Master's Theses

Metal oxide and zeolite catalysts were examined to determine their suitability for the production of methanethiol and dimethyl sulfide from the condensation of methanol and hydrogen sulfide. Fixed bed reactor experiments were used to test the catalysts in these processes. The acid sites of these catalysts were characterized by investigating the thermal desorption of 1-propanamine from these sites. It was found that WO3/ZrO2, La2O3/Al2O3, g-Al2O3, and HZSM-5 catalysts were active and selective in the production of dimethyl sulfide. On these four catalysts, the reaction converting methanol to dimethyl ether and the methanethiol disproportionation reaction were fast and close to equilibrium. …