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2019

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Full-Text Articles in Engineering

About Time: Visualizing Time At Burning Man, Gordon D. Hoople, Austin Choi-Fitzpatrick, Nathaniel Parde, Diane Hoffoss, Max Mellette, Rachel Nishimura, Virginia Gutman Dec 2019

About Time: Visualizing Time At Burning Man, Gordon D. Hoople, Austin Choi-Fitzpatrick, Nathaniel Parde, Diane Hoffoss, Max Mellette, Rachel Nishimura, Virginia Gutman

The STEAM Journal

About Time was a 30 foot long, 3000 pound wooden sundial that went up in flames at Burning Man 2019. The piece reflected on the role time plays in our lives. We organize our lives around time—are enslaved to time—and yet we know so little about it. Physicists and philosophers continue to grapple with deep puzzles of time—Is time a fundamental quantity, independent of human actions or observations or is it an emergent property of our perception? This installation projected time using two sundials: a horizontal dial which swept time out across the desert floor and an …


Pengembangan Training Kit Selektor Warna Barang Menggunakan Model Addie Sebagai Sarana Pembelajaran Plc, Teguh Arik Yuanto, Putu Sudira Dec 2019

Pengembangan Training Kit Selektor Warna Barang Menggunakan Model Addie Sebagai Sarana Pembelajaran Plc, Teguh Arik Yuanto, Putu Sudira

Elinvo (Electronics, Informatics, and Vocational Education)

This study aims to (1) realize the design of the item color selector training kit and (2) determine the feasibility of the item color selector training kit. The research uses the ADDIE Models reference, namely: analysis, design, development, implementation, and evaluation. Data collection techniques used were observation and questionnaires. The testing consists of product validation by experts, testing by teachers, and testing by students. The data analysis technique used is quantitative descriptive. The results consist of: (1) item color selector training kit design consisting of training and jobsheets. The training sections include boxes, conveyors, selectors and microcontroller circuits, the jobsheet …


Perangkat Penentu Kualitas Beras Ditinjau Dari Kadar Air Dan Berat Butir Menir Berbasis Arduino Uno, Mustofah Mustofah, Pipit Utami Dec 2019

Perangkat Penentu Kualitas Beras Ditinjau Dari Kadar Air Dan Berat Butir Menir Berbasis Arduino Uno, Mustofah Mustofah, Pipit Utami

Elinvo (Electronics, Informatics, and Vocational Education)

Determining the quality of rice is something that must be done to maintain the quality of rice produced by farmers. Quality determinants used for this process can be relied on for rice properly and efficiently. Determination of air content using soil moisture sensor yl-69 and determination of grain weight using a load cell sensor that emits with an Arduino UNO microcontroller as a device controller device. System making method consists of needs, analytic requirements, block diagrams, system design, manufacturing tools, testing tools and tools. The test results show that the determinant of rice quality in terms of good air and …


Sistem Cerdas Deteksi Sinyal Elektrokardiogram (Ekg) Untuk Klasifikasi Jantung Normal Dan Abnormal Menggunakan Jaringan Syaraf Tiruan (Jst), Myza Rifali, Dessy Irmawati Dec 2019

Sistem Cerdas Deteksi Sinyal Elektrokardiogram (Ekg) Untuk Klasifikasi Jantung Normal Dan Abnormal Menggunakan Jaringan Syaraf Tiruan (Jst), Myza Rifali, Dessy Irmawati

Elinvo (Electronics, Informatics, and Vocational Education)

This article aims to describe the accuracy of signal processing using neural networks. The design of this final project hardware consists of Arduino Uno, AD8232 module and electrodes. ECG signals obtained from respondents were used as test data for normal ECG signals, while for abnormal class test data the data used were obtained from the research website, namely physionet with atrial fibrillation class. The design process in this system includes the process of data acquisition, training, feature extraction, testing and classification with artificial neural networks. Based on the results of the performance of this device to record ECG signals on …


Prototipe Kursi Roda Elektrik Dengan Kendali Joystick Dan Smartphone, Andy Sadewa Junior, Fatchul Arifin Dec 2019

Prototipe Kursi Roda Elektrik Dengan Kendali Joystick Dan Smartphone, Andy Sadewa Junior, Fatchul Arifin

Elinvo (Electronics, Informatics, and Vocational Education)

Wheelchairs are one of the walking aids for people with disabilities and also for people who are unable to move from one place to another. The purpose of this research was to build hardware and software into a wheelchair prototype that can be controlled with joysticks and smartphones and to know its performance. The method in making the final project consists of the stages of need identification, requirements analysis, system design, tool making, tool testing and data collection. Based on the testing that has been done, the results are obtained that the control input from the smartphone through the application …


Kinerja Dari Prototipe Robot Visual Pengumpul Sampah Perairan Dengan Remote Control Menggunakan Telemetri, Faiz Sulistyawan, Sri Waluyanti Dec 2019

Kinerja Dari Prototipe Robot Visual Pengumpul Sampah Perairan Dengan Remote Control Menggunakan Telemetri, Faiz Sulistyawan, Sri Waluyanti

Elinvo (Electronics, Informatics, and Vocational Education)

The making of prototype robot waste water collection aims to know the performance itself. The prototype of the Aquatic Waste Collection Robot is designed to float and clean trash in remote controlled waters. The main control drives a series of DC brushless motors to drive while the MG995 servo motor drives a rudder or defender. The device is also equipped with a camera as a medium to see the condition of the robot directly or in real time which will be displayed on the monitor screen. The camera and screen are connected to a telemetry circuit consisting of a transmitter …


Pengembangan Prototype Sistem Kendali Kualitas Air Tambak Udang, Avara Ghamaliel Ty, Pramudi Utomo Dec 2019

Pengembangan Prototype Sistem Kendali Kualitas Air Tambak Udang, Avara Ghamaliel Ty, Pramudi Utomo

Elinvo (Electronics, Informatics, and Vocational Education)

The purpose of this article is to describe the analysis, design and performance of prototype shrimp water quality control systems. This tool is expected to simplify and ease the work of shrimp farmers in checking water quality regularly. In its design consists of several steps, namely designing the design of tools, making mechanical systems, programming, and the final stage of testing. The main component that is used as the main control is Arduino Nano. Salinity sensor, DS18b20, and PH-4520C as components for monitoring water quality. 12V DC water pump as a stabilizer of the pH level in the water. Based …


Analisis Kasus Pencurian Listrik Menggunakan Proses Stochastic Pada Lingkungan Terpasang Smart Metering, Arya Sony Dec 2019

Analisis Kasus Pencurian Listrik Menggunakan Proses Stochastic Pada Lingkungan Terpasang Smart Metering, Arya Sony

Elinvo (Electronics, Informatics, and Vocational Education)

Menggunakan metode deteksi yang presisi pada kasus pencurian listrik merupakan pekerjaan yang mustahil dilakukan. Hal ini disebabkan karena adanya satu variabel yang bernilai ekonomi tinggi yang diperlukan agar perhitungan mungkin untuk dilakukan, yaitu variabel jarak penghantar. Dengan memasukkan proses stokastik ke dalam persamaan deteksi pencurian listrik akan banyak mengurangi pekerjaan PLN dalam mengimplementasikan Sistem Smart Metering. Smart Metering adalah Perangkat IoT yang dapat merekam jumlah konsumsi listrik pelanggan yang terpasang pada masing-masing meteran listrik pelanggan PLN. Hasil simulasi menunjukkan bahwa dengan menggunakan proses stochastik tidak mengurangi akurasi Sistem Smart Metering dan hanya menunjukkan kesalahan rata-rata 1,19E-07%. Penemuan ini sangat …


Studi Komparasi Simulasi Sistem Kendali Pid Pada Matlab, Gnu Octave, Scilab Dan Spyder, Ardy Seto Priambodo Dec 2019

Studi Komparasi Simulasi Sistem Kendali Pid Pada Matlab, Gnu Octave, Scilab Dan Spyder, Ardy Seto Priambodo

Elinvo (Electronics, Informatics, and Vocational Education)

Dalam penelitian ini perbandingan antara perangkat lunak MATLAB, GNU Octave, Scilab dan Spyder akan diamati. Proses yang menjadi obyek dalam penelitian ini adalah sistem kendali PID yang digunakan untuk mengendalikan plant yang berupa model motor DC. Fungsi alih dari motor DC merupakan model dari motor DC yang diturunkan dari hukum newton ke-2 dan hukum kirchoff tegangan. Simulasi dilakukan pada perangkat lunak menggunakan 2 cara yaitu kode program dan block programming. Jumlah baris kode program yang terpendek adalah MATLAB dengan 17 baris dan yang terpanjang adalah Spyder dengan 20 baris kode program. Untuk block programming hanya dapat dilakukan pada MATLAB dan …


Analisa Pengujian Repeatability Timbangan Elektronik Dengan Metode Syarat Teknis Timbangan Non Otomatis Dan Metode Nmi Australia, Ponco Wali Dec 2019

Analisa Pengujian Repeatability Timbangan Elektronik Dengan Metode Syarat Teknis Timbangan Non Otomatis Dan Metode Nmi Australia, Ponco Wali

Elinvo (Electronics, Informatics, and Vocational Education)

Testing repeat electronic scales with non-automatic scales technical requirements so far is fairly long if not using a calculator or computer. The aim of this research is to compare the repeatability testing method of electronic scales using methods according to the technical requirements of non-automatic scales and the Australian NMI method, both of which refer to OIML R76 in determining the validity or cancellation of electronic scales repeatability testing. This research method is done through repeat testing on 3 samples of electronic scales, then on each electronic scale 2 test methods are performed. The conclusion is that the electronic scales …


Perancangan Sistem Pemantauan Suhu Dan Kelembaban Pada Proses Dekomposisi Pupuk Kompos Berbasis Iot, Farida Hardyanti, Pramudi Utomo Dec 2019

Perancangan Sistem Pemantauan Suhu Dan Kelembaban Pada Proses Dekomposisi Pupuk Kompos Berbasis Iot, Farida Hardyanti, Pramudi Utomo

Elinvo (Electronics, Informatics, and Vocational Education)

The problem that often occurs in making compost is the level of fertilizer maturity that is not perfect. This is caused by humidity and temperature in the unstable manufacturing process. This article aims to develop a system capable of controlling temperature and humidity as well as monitor changes in the process of compost decomposition wirelessly and describe the results of testing the system. This research uses a development method with several stages, namely: problem identification and needs analysis, design, implementation, and testing. The results show that: (1) a temperature and humidity monitoring system is realized to monitor and regulate the …


Prototype Autonomous Rover Pembersih Sampah Pantai Menggunakan Ardupilot, Adhy Febry Anto, Totok Sukardiyono Dec 2019

Prototype Autonomous Rover Pembersih Sampah Pantai Menggunakan Ardupilot, Adhy Febry Anto, Totok Sukardiyono

Elinvo (Electronics, Informatics, and Vocational Education)

Indonesia has the second longest coastline in the world. On the other hand, Indonesia is the second largest contributor to marine waste in the world. Coastal cleanliness needs to be maintained so that it becomes an attraction for tourism and to protect the marine ecosystem. This article describes the results of testing devices that can be used to clean beaches. Research carried out by the development method. An autonomous beach garbage cleaning rover is a beach trash sweeper robot equipped with GPS, compass, telemetry, ArduPilot as a navigation and communication system when the robot operates. This robot moves using 2 …


Sistem Kendali Dan Akuisisi Data Suhu Serta Kelembaban Ruang Budidaya Jamur Tiram (Pleurotus Ostreatus) Berbasis Internet Of Things (Iot), Amalia Rohmah, Satriyo Agung Dewanto Dec 2019

Sistem Kendali Dan Akuisisi Data Suhu Serta Kelembaban Ruang Budidaya Jamur Tiram (Pleurotus Ostreatus) Berbasis Internet Of Things (Iot), Amalia Rohmah, Satriyo Agung Dewanto

Elinvo (Electronics, Informatics, and Vocational Education)

This study aims to determine the performance of temperature and humidity control technology of the Internet of Things (IoT) automatic oyster mushroom cultivation space. The stages of device development consist of analysis, design, assembly and testing. The design developed combines hardware control, software, and cloud server. This tool consists of 3 main processes, namely input using DHT11 sensors, process and output, namely 220 V AC actuators. There are two tests namely technical and effectiveness. The test results that have been carried out are: (1) the performance test results obtained an average error of 1.44% and a mean humidity of 3.35%, …


Indonesia Natural Mineral For Heavy Metal Adsorption: A Review, Grandprix T. M. Kadja, Moh Mualliful Ilmi Dec 2019

Indonesia Natural Mineral For Heavy Metal Adsorption: A Review, Grandprix T. M. Kadja, Moh Mualliful Ilmi

Journal of Environmental Science and Sustainable Development

Indonesia has abundant mineral resources used as natural adsorbent materials for the absorption of heavy metal. Among these are natural zeolites, clay, and ashes. These natural materials showed high performance adsorption capacity with respects to their low cost and high availability. Several research reports had been published for studying the performance of the natural materials as adsorbent of several heavy metals i.e., Hg, Pb, Fe, Cd, Cr, Zn, Ni, and Cu by examining the effect of various factors, including pH, contact time, initial concentration, temperature, and dosage. Furthermore, to determine the adsorption rate, mechanism, and efficiency of natural materials in …


Asro (Amphibious Spy Robot): Prototipe Robot Amfibi Pengintai Dengan First Person View Dan Sistem Navigasi Berbasis Sensor Kompas, R. Amirur Rajif, Fatchul Arifin Dec 2019

Asro (Amphibious Spy Robot): Prototipe Robot Amfibi Pengintai Dengan First Person View Dan Sistem Navigasi Berbasis Sensor Kompas, R. Amirur Rajif, Fatchul Arifin

Elinvo (Electronics, Informatics, and Vocational Education)

Robots have an important role in all aspects of life, including the military field. The purpose of making this final project are building hardware and software of robot and to know the performance of robots. The method used in making the final project consists of identifying and analyzing requirements, designing and manufacturing hardware and software, and testing. The result of the performance of ASRO is that, the buoyancy force of the robot is greater than the weight of the object, namely Fa = 22,808 N and W = 15,696 N or Fa> W which makes the robot float while operate …


Electrochemical Preparation And Photocatalytic Performance Of Lanio3/Tio2 Nanotube Arrays, Cheng Gong, Ze-Yang Zhang, Si-Wan Xiang, Lan Sun, Chen-Qing Ye, Chang-Jian Lin Dec 2019

Electrochemical Preparation And Photocatalytic Performance Of Lanio3/Tio2 Nanotube Arrays, Cheng Gong, Ze-Yang Zhang, Si-Wan Xiang, Lan Sun, Chen-Qing Ye, Chang-Jian Lin

Journal of Electrochemistry

The LaNiO3/TiO2 nanotube arrays were prepared by pulse electrodeposition combined with high temperature annealing. The LaNiO3 nanoparticles modified on the TiO2 nanotube arrays had small particle size (< 10 nm), uniform distribution and controllable loading. Some LaNiO3 nanoparticles were deposited inside the TiO2 nanotubes. The UV-visible absorption spectra displayed that the absorption band edge of LaNiO3/TiO2 nanotube arrays was obviously red-shifted as compared with that of TiO2 nanotube arrays, and the visible light absorption was enhanced significantly. The photocatalytic degradation results of rhodamine B (RhB) under visible light showed that the LaNiO3/TiO2 nanotube arrays prepared by pulse electrodeposition for 500 cycles had …


Electrochemical Cycling Stability Of Polyaniline Films In Different Color Ranges, Kun Xu, Kai-Ling Zhou, Hao Wang, Jing-Bing Liu, Hui Yan Dec 2019

Electrochemical Cycling Stability Of Polyaniline Films In Different Color Ranges, Kun Xu, Kai-Ling Zhou, Hao Wang, Jing-Bing Liu, Hui Yan

Journal of Electrochemistry

The electrochromic behaviors of polyaniline films were investigated by potential step and cyclic voltammetry coupled with UV viscosity photometer. The polyaniline films show colorful changes from pale yellow to green and then to blue. Electrochromic stability, electrochemical behavior, coloring performance, optical properties and surface formations of the produced films were studied in detail. The working electrode was the flexible PANI electrode, and the counter electrode and the reference electrode were a platinum sheet and Ag/AgCl, respectively. The in situ optical transmittance of the PANI film at 650 nm was measured using an ultraviolet-visible-near-infrared spectrophotometer (Shimadzu UV-3101PC) combining with a square …


Transient Electrochemical Surface-Enhanced Raman Spectroscopic Study In Electrochemical Reduction Of P-Nitrothiophenol, Yun Ling, Jing Tang, Guo-Kun Liu, Cheng Zong Dec 2019

Transient Electrochemical Surface-Enhanced Raman Spectroscopic Study In Electrochemical Reduction Of P-Nitrothiophenol, Yun Ling, Jing Tang, Guo-Kun Liu, Cheng Zong

Journal of Electrochemistry

P-nitrothiophenol (PNTP) is one of the most common probe molecules studied by surface-enhanced Raman spectroscopy (SERS). The research in electrochemical reduction behavior of PNTP will help understanding the mechanism for the nitrobenzene reduction. In this paper, we used transient electrochemical surface-enhanced Raman spectroscopy (TEC-SERS) to study the SERS of PNTP with cyclic voltammetry and chronoamperometry on gold electrodes. The results show that the TEC-SERS provide a time resolution that equals the transient electrochemical methods, and we concluded that the reaction was so quick that we did not observe the spectral information of intermediate species described in the literatures with a …


Quantitative Detection Of Levofloxacin Hydrochloride By Differential Pulse Stripping Voltammetry With Electrodeposited Bismuth Film Electrodes, Zi-Ying Guo, Zuo-Peng Li, Jiang Li, Jian-Guo Zhao, Feng Feng Dec 2019

Quantitative Detection Of Levofloxacin Hydrochloride By Differential Pulse Stripping Voltammetry With Electrodeposited Bismuth Film Electrodes, Zi-Ying Guo, Zuo-Peng Li, Jiang Li, Jian-Guo Zhao, Feng Feng

Journal of Electrochemistry

In this study, differential pulse stripping voltammetry was developed for the quantitative detection of levofloxacin hydrochloride indirectly. Levofloxacin hydrochloride contains organic amine, which can be precipitated upon interaction with Zn(SCN)42-. By means of differential pulse stripping voltammetry, the concentration of Zn2+ can be determined using an in-situ formed bismuth film electrode, which allows determining indirectly the amount of levofloxacine hydrochloride. The linearity equation, I = 1.1401c - 0.5309 with the correlative coefficient R = 0.9979, was presented in the experiment. The results showed that this approach is very sensitive, having a limitation of detection of 3.18 …


Calculation Of Heat Exchange Intensity At Gas-Liquid Flow Washing Tube-Lattice Nozzles, Elbek Tulkinovich Mavlonov, Zakirova Nafisa Sanatovna, Kudratilla Fuadovich Karimov, Khabibulla Sagdullaevich Nurmukhamedov Dec 2019

Calculation Of Heat Exchange Intensity At Gas-Liquid Flow Washing Tube-Lattice Nozzles, Elbek Tulkinovich Mavlonov, Zakirova Nafisa Sanatovna, Kudratilla Fuadovich Karimov, Khabibulla Sagdullaevich Nurmukhamedov

Chemical Technology, Control and Management

Several experiments were conducted on removing the heat of reaction upon contact of carbon dioxide with purified brine. Pipes with a developed heat exchange surface formed by spiral grooves on the outside and similar protrusions inside the pipes are used for effective conduction. The experiments were carried out on two and four pipes with different pitch and depth of grooves,i.e. h / S = 0.017-0.095. Studies on the intensification of convective heat exchange when washing a bundle of spiral-rolled pipes with a gas-liquid flow have found an increase in heat transfer by 1.8-2.7 times compared to a smooth pipe. Such …


Development Of Structures Of Intellectual Information Protection System, Tulkun Fayzievich Bekmuratov, Fayzullajon Bakhtiyorovich Botirov Dec 2019

Development Of Structures Of Intellectual Information Protection System, Tulkun Fayzievich Bekmuratov, Fayzullajon Bakhtiyorovich Botirov

Chemical Technology, Control and Management

The structures of intelligent information protection systems are considered. The tree of tasks for protecting information of the information system of enterprise is presented. Information security management systems without automation of management processes and automated information security management systems are considered. The functional capabilities of multi-agent information protection systems are investigated and possible risks are analyzed. The proposed schemes of automated and automated information security management systems are described. The proposed technology for constructing a software package for an enterprise information security management system is considered, based on the concept of multi-agent systems as the basic technology for software implementation …


Algebraic Correction Of Algorithms For Recognition And Identification Of Biological Objects In Data Mining Problems, Mirzoyan Kamilov, Mirzaakbar Hudayberdiev Dec 2019

Algebraic Correction Of Algorithms For Recognition And Identification Of Biological Objects In Data Mining Problems, Mirzoyan Kamilov, Mirzaakbar Hudayberdiev

Chemical Technology, Control and Management

The integration of information technologies with biology is considered, enabling specialists to further study the subject area. The object of the study is the identification of the information structure and parameters of Insects Orthoptera of Uzbekistan. For this purpose, an information and identification software complex were created and the analysis of the variety of orthoptera having a certain internal structure and, accordingly, the formed structure of the relational database of the Insecta Orthoptera species was carried out. At the same time, attention will also be paid to the study of a number of scientific issues, one way or another related …


Polyaniline Coated Hollow Sulfur Prepared Using Sublimate 2,4,6-Tri(Propan-2-Yl)-1,3,5-Trioxane As Template For Sulfur Electrode, Zhang-Feng Li, Xiao-Rui Wang, Wen-Sheng Tian, Jin-Ze Yang, Ping Zhang, Li-Ping Ma, Yang Chen, Xiao-Li Cui, Zhi-Yu Jiang Dec 2019

Polyaniline Coated Hollow Sulfur Prepared Using Sublimate 2,4,6-Tri(Propan-2-Yl)-1,3,5-Trioxane As Template For Sulfur Electrode, Zhang-Feng Li, Xiao-Rui Wang, Wen-Sheng Tian, Jin-Ze Yang, Ping Zhang, Li-Ping Ma, Yang Chen, Xiao-Li Cui, Zhi-Yu Jiang

Journal of Electrochemistry

An advance method for preparing polyaniline-coated hollow sulfur material using sublimate material ADD(2,4,6-tri(propan-2-yl)-1,3,5-trioxane) as a template was developed for lithium-sulfur battery. At first, the smashed ADD particles were coated by a sulfur layer through the reaction of Na2S2O3 with diluted HCl. Then polyaniline layer was coated again on the surface of sulfur layer through the reaction of aniline with (NH4)2S2O8. After being dried at 60 oC for 12 h, the ADD in such a composite evaporated totally, and resulted in the formation of polyaniline-coated hollow sulfur …


Electrochemical Determination Of Trace Copper Ions In Drinking Water Source, Jing-Ji Peng, Hong Zheng, Yi-Song Zou, Guo-Kun Liu, Dong-Xing Yuan Dec 2019

Electrochemical Determination Of Trace Copper Ions In Drinking Water Source, Jing-Ji Peng, Hong Zheng, Yi-Song Zou, Guo-Kun Liu, Dong-Xing Yuan

Journal of Electrochemistry

Aiming at the on-site and quick safety evaluation of the dissolved trace copper ions (Cu2+) in drinking water source, an electrochemical detection platform was developed on the basis of the square wave anodic stripping voltammetry using the gold nanoparticles (Au NPs) modified glassy carbon electrode, where Au NPs were deposited via electrochemical cyclic voltammetry. The proposed method displayed the limit of detection as low as 1.3 μg·L-1 in the linear range of 2 ~ 50 μg·L-1. The proposed method was applied to the determination of Cu2+ in the midstream of Minjiang River, one of …


Bipolar-Membrane Electrodialysis Method To Treat Industrial High Saline Perfume Wastewater, Jian Zhang, Dong-Fang Niu, Shuo-Zhen Hu, Xin-Sheng Zhang Dec 2019

Bipolar-Membrane Electrodialysis Method To Treat Industrial High Saline Perfume Wastewater, Jian Zhang, Dong-Fang Niu, Shuo-Zhen Hu, Xin-Sheng Zhang

Journal of Electrochemistry

Large amount of organic saline wastewater is generated from various chemical industries. The contents of organic saline wastewater are more and more complicated as they are created from different types of industries. Directly discharging the organic saline wastewater without pre-treatment can generate severe environmental problem and waste useful resources. It is necessary to use an economical method to treat the organic saline wastewater and recover the salt into useful materials to achieve resource reuse. Bipolar-membrane electrodialysis (BMED) is one of the methods that can remove salt from the wastewater and convert it into certain acid and base with higher value …


Electrochemical Behaviors Of Azopurine On Gold Electrodes, Ming-Xue Li, Hang Shi, Jia Liu, Meng Zhang, Jian-Zhang Zhou, De-Yin Wu, Zhong-Qun Tian Dec 2019

Electrochemical Behaviors Of Azopurine On Gold Electrodes, Ming-Xue Li, Hang Shi, Jia Liu, Meng Zhang, Jian-Zhang Zhou, De-Yin Wu, Zhong-Qun Tian

Journal of Electrochemistry

In this paper, we studied the electrochemical behaviors of azopurine on polished gold electrodes with cyclic voltammetry (CV). On the basis of analyzing scan rate and peak current, it was supposed that the redox process belonged to a reversible process controlled by adsorption in 0.2 mol·L-1 PBS (pH = 4.0 ~ 10.0) solutions. The potentials of redox peaks moved more negatively with increasing pH value. This proved that the H+ proton has participcted in the electrochemical reaction. The further data analysis and the calculation of surface adsorption excess demonstrated that the reaction was a two-proton and two-electron process. …


Study On Electro-Sorption Of Heavy Metals And Sulfamethoxazole On Activated Carbon Fibers, Wen-Jun Zhao, Bing-Xin Jia, Ya-Nan Zhang, Jiu-Nian Guan, Jiao Qu, Ying Lu Dec 2019

Study On Electro-Sorption Of Heavy Metals And Sulfamethoxazole On Activated Carbon Fibers, Wen-Jun Zhao, Bing-Xin Jia, Ya-Nan Zhang, Jiu-Nian Guan, Jiao Qu, Ying Lu

Journal of Electrochemistry

To study the optimal removal condition, adsorption mechanism and comparative analysis of the three typical cationic pollutants, i.e., Zn(II), anionic pollutant Cr(VI) and molecular pollutant sulfamethoxazole (SMX), using self-made upflowed electro-sorption device for adsorptions of above three pollutants by modified activated carbon fiber were researched. The activated carbon fiber (ACF) was modified by hydrochloric acid. The ACF morphology and structure before and after modification were characterized by SEM, BET and FTIR. The characterization results show that the modified ACF had fewer surface impurities than the modified surface and the gully is more obvious, the specific surface area was increased by …


Electrochemical Sensor Based On Magnetic Electrode Modified With Magnetic Molecularly Imprinted Nanoparticles Immobilized Hemoglobin For Determination Of Hydrogen Peroxide, Yang Yuan, Jia-Xin Wang, Yu-Hua Cao Dec 2019

Electrochemical Sensor Based On Magnetic Electrode Modified With Magnetic Molecularly Imprinted Nanoparticles Immobilized Hemoglobin For Determination Of Hydrogen Peroxide, Yang Yuan, Jia-Xin Wang, Yu-Hua Cao

Journal of Electrochemistry

In this work, the surface-imprinted technique was used to prepare magnetic hemoglobin (Hb) imprinted nanoparticles, using Fe3O4@SiO2 NPs as the carrier, Hb as the template molecule, and tetraethyl orthosilicate (TEOS) as the imprinted polymer monomer. The nanoparticles had a core-shell structure, with magnetic Fe3O4 NPs as the core and Hb imprinted polymers as the shell. Therefore, Hb could be concentrated and fixed on the surface of the magnetic imprinted nanoparticles (MMIPs NPs). Furthermore, MMIPs NPs were immobilized with chitosan (CS) on the surface of a magnetic electrode to constitute Hb enzyme-like biosensor …


Ionic Liquid Assisted Synthesis Of Porous Carbons From Rice Husk For Supercapacitors, Han-Fang Zhang, Feng Wei, Jian Sun, Meng-Ying Jing, Xiao-Jun He Dec 2019

Ionic Liquid Assisted Synthesis Of Porous Carbons From Rice Husk For Supercapacitors, Han-Fang Zhang, Feng Wei, Jian Sun, Meng-Ying Jing, Xiao-Jun He

Journal of Electrochemistry

It is still a challenge to prepare carbon materials with high specific surface area at low cost from renewable resources. Herein, the authors report an efficient approach to synthesize porous carbons (PCs) from rice husk with ionic liquid (1-butyl-3-methylimidazolium hexafluorophosphate (BMIMPF6)) as a template and an activation agent. The as-made PCs featured the high specific surface area up to 1438 m2·g-1. As electrodes for supercapacitors, PCs showed a high specific capacitance of 256 F·g-1 at 0.05 A·g-1 in 6 mol·L-1 KOH aqueous electrolyte and a good rate performance of 211 F·g …


An Aptasensor Based On Aunps/Pani/Tnts Nanocomposite For Electrochemical Detection Of Tobramycin, Yong-Ling Nong, Ni-Na Qiao, Ying Liang Dec 2019

An Aptasensor Based On Aunps/Pani/Tnts Nanocomposite For Electrochemical Detection Of Tobramycin, Yong-Ling Nong, Ni-Na Qiao, Ying Liang

Journal of Electrochemistry

A novel well-constructed electrochemical aptamer-based sensor for the detection of tobramycin was presented, using differential pulse voltammetry (DPV) as a detection technique and methylene blue(MB) as an electrochemical indicator. A glassy carbon electrode modified with a nanocomposite of Au nanoparticles/polyaniline/titania nanotubes (AuNPs/PANI/TNTs) was constructed as the electrode scaffold. The nanocomposite was characterized by transmission electron microscopy and X-ray photoelectron spectroscopy in detail. The results of cyclic voltammetry and electrochemical impedance measurements demonstrated that the AuNPs/PANI/TNTs nanocomposites can improve greatly the electron transfer on the interface. For the detection of tobramycin, the DPV results showed a linear relationship between the current …