Engineering Commons^™

Particle Migration In Large Cross-Section Ceramic On-Demand Extrusion Components, Austin J. Martin, Wenbin Li, Jeremy Lee Watts, Gregory E. Hilmas, Ming-Chuan Leu, Tieshu Huang

Materials Science and Engineering Faculty Research & Creative Works

Ceramic On-Demand Extrusion (CODE) is a direct ink writing process which allows for the creation of near theoretically dense ceramic components with large cross-sections due to oil-assisted drying. Yttria-stabilized zirconia (YSZ) colloidal pastes (∼d50 ≲ 1 µm) were used in CODE to produce dense (multi-road infill and ≳ 98% relative density), large continuous volume (> 1 cm3), and high fidelity (nozzle diameters ≲ 1 mm) structural ceramic components. However, many of these printed components underwent significant particle migration after forming. The reason for this particle migration defect was investigated using the coffee-ring effect for dilute solutions and rheological methods for …

Particle Migration In Large Cross-Section Ceramic On-Demand Extrusion Components, Austin J. Martin, Wenbin Li, Jeremy Lee Watts, Gregory E. Hilmas, Ming-Chuan Leu, Tieshu Huang

Mathematics and Statistics Faculty Research & Creative Works

Ceramic On-Demand Extrusion (CODE) is a direct ink writing process which allows for the creation of near theoretically dense ceramic components with large cross-sections due to oil-assisted drying. Yttria-stabilized zirconia (YSZ) colloidal pastes (∼d50 ≲ 1 µm) were used in CODE to produce dense (multi-road infill and ≳ 98% relative density), large continuous volume (> 1 cm3), and high fidelity (nozzle diameters ≲ 1 mm) structural ceramic components. However, many of these printed components underwent significant particle migration after forming. The reason for this particle migration defect was investigated using the coffee-ring effect for dilute solutions and rheological methods for …

Particle Migration In Large Cross-Section Ceramic On-Demand Extrusion Components, Austin J. Martin, Wenbin Li, Jeremy Lee Watts, Gregory E. Hilmas, Ming-Chuan Leu, Tieshu Huang

Materials Science and Engineering Faculty Research & Creative Works

Ceramic On-Demand Extrusion (CODE) is a direct ink writing process which allows for the creation of near theoretically dense ceramic components with large cross-sections due to oil-assisted drying. Yttria-stabilized zirconia (YSZ) colloidal pastes (∼d50 ≲ 1 µm) were used in CODE to produce dense (multi-road infill and ≳ 98% relative density), large continuous volume (> 1 cm3), and high fidelity (nozzle diameters ≲ 1 mm) structural ceramic components. However, many of these printed components underwent significant particle migration after forming. The reason for this particle migration defect was investigated using the coffee-ring effect for dilute solutions and rheological methods for …

Characterization Of Virgin, Re-Used, And Oxygen-Reduced Copper Powders Processed By The Plasma Spheroidization Process, M. Hossein Sehhat, David Perez-Palomino, Connor Wiedemeier, Tristan Cullom, Joseph William Newkirk

Materials Science and Engineering Faculty Research & Creative Works

Fabrication of parts with high mechanical properties heavily depend on the quality of powder deployed in the fabrication process. Copper powder in three different powder types were spheroidized using radio-frequency inductively coupled plasma (ICP) spheroidization process (TekSphero-15 system). The characterized powders include virgin powder as purchased from the powder manufacturer, powder used in electron beam powder bed fusion (EB-PBF) process, and reconditioned powder, which was used powder that underwent an oxygen-reduction treatment. The goal of spheroidizing these powder types was to evaluate the change in powder morphology, the possibility of enhancing the powder properties back to their as-received conditions, and …

Characterization Of Virgin, Re-Used, And Oxygen-Reduced Copper Powders Processed By The Plasma Spheroidization Process, M. Hossein Sehhat, David Perez-Palomino, Connor Wiedemeier, Tristan Cullom, Joseph William Newkirk

Mathematics and Statistics Faculty Research & Creative Works

Fabrication of parts with high mechanical properties heavily depend on the quality of powder deployed in the fabrication process. Copper powder in three different powder types were spheroidized using radio-frequency inductively coupled plasma (ICP) spheroidization process (TekSphero-15 system). The characterized powders include virgin powder as purchased from the powder manufacturer, powder used in electron beam powder bed fusion (EB-PBF) process, and reconditioned powder, which was used powder that underwent an oxygen-reduction treatment. The goal of spheroidizing these powder types was to evaluate the change in powder morphology, the possibility of enhancing the powder properties back to their as-received conditions, and …

Characterization Of Virgin, Re-Used, And Oxygen-Reduced Copper Powders Processed By The Plasma Spheroidization Process, M. Hossein Sehhat, David Perez-Palomino, Connor Wiedemeier, Tristan Cullom, Joseph William Newkirk

Materials Science and Engineering Faculty Research & Creative Works

Fabrication of parts with high mechanical properties heavily depend on the quality of powder deployed in the fabrication process. Copper powder in three different powder types were spheroidized using radio-frequency inductively coupled plasma (ICP) spheroidization process (TekSphero-15 system). The characterized powders include virgin powder as purchased from the powder manufacturer, powder used in electron beam powder bed fusion (EB-PBF) process, and reconditioned powder, which was used powder that underwent an oxygen-reduction treatment. The goal of spheroidizing these powder types was to evaluate the change in powder morphology, the possibility of enhancing the powder properties back to their as-received conditions, and …

Characterization And Improvement Of Powder Properties Through Plasma Spheroidization For Use In The Laser Powder Bed Fusion Process, M. Hossein Sehhat

Doctoral Dissertations

"This research was conducted to characterize the powder properties using different characterization techniques to enhance the powder behavior in the Laser Powder Bed Fusion (LPBF) process. One of the shortcomings of LPBF process is the high cost of gas-atomized powder feedstock. To overcome this downside, the cheaper water-atomized powder was characterized and used in LPBF process, and its performance was compared with those of gas-atomized powder. Also, the plasma spheroidization process was used to improve the powder characteristics; if the spheroidized powder could function as well as the virgin powder, plasma spheroidization process could be applied to the used powders …

Tini-Based Bi-Metallic Shape-Memory Alloy By Laser-Directed Energy Deposition, Yitao Chen, Cesar Ortiz Rios, Braden Mclain, Joseph William Newkirk, Frank W. Liou

Materials Science and Engineering Faculty Research & Creative Works

In this study, laser-directed energy deposition was applied to build a Ti-rich ternary Ti-Ni-Cu shape-memory alloy onto a TiNi shape-memory alloy substrate to realize the joining of the multifunctional bi-metallic shape-memory alloy structure. The cost-effective Ti, Ni, and Cu elemental powder blend was used for raw materials. Various material characterization approaches were applied to reveal different material properties in two sections. The as-fabricated Ti-Ni-Cu alloy microstructure has the TiNi phase as the matrix with Ti₂Ni secondary precipitates. The hardness shows no high values indicating that the major phase is not hard intermetallics. A bonding strength of 569.1 MPa …

Quasi-Static Multifunctional Characterization Of 3d-Printed Carbon Fiber Composites For Compressive-Electrical Properties, Ritesh Ghimire, Frank W. Liou

Mechanical and Aerospace Engineering Faculty Research & Creative Works

Multifunctional carbon fiber composites provide promising results such as high strength-to-weight ratio, thermal and electrical conductivity, high-intensity radiated field, etc. for aerospace applications. Tailoring the electrical and structural properties of 3D-printed composites is the critical step for multifunctional performance. This paper presents a novel method for evaluating the effects of the coating material system on the continuous carbon fiber strand on the multifunctional properties of 3D-printed composites and the material's microstructure. A new method was proposed for the quasi-static characterization of the Compressive-Electrical properties on the additively manufactured continuous carbon fiber solid laminate composites. In this paper, compressive and electrical …

Uncertainties Induced By Processing Parameter Variation In Selective Laser Melting Of Ti6al4v Revealed By In-Situ X-Ray Imaging, Zachary A. Young, Meelap M. Coday, Qilin Guo, Minglei Qu, S. Mohammad H. Hojjatzadeh, Luis I. Escano, Kamel Fezzaa, Tao Sun, Lianyi Chen

Mechanical and Aerospace Engineering Faculty Research & Creative Works

Selective laser melting (SLM) additive manufacturing (AM) exhibits uncertainties, where variations in build quality are present despite utilizing the same optimized processing parameters. In this work, we identify the sources of uncertainty in SLM process by in-situ characterization of SLM dynamics induced by small variations in processing parameters. We show that variations in the laser beam size, laser power, laser scan speed, and powder layer thickness result in significant variations in the depression zone, melt pool, and spatter behavior. On average, a small deviation of only ~5% from the optimized/reference laser processing parameter resulted in a ~10% or greater change …

Fabricating Tinicu Ternary Shape Memory Alloy By Directed Energy Deposition Via Elemental Metal Powders, Yitao Chen, Xinchang Zhang, Mohammad Masud Parvez, Joseph William Newkirk, Frank W. Liou

Materials Science and Engineering Faculty Research & Creative Works

In this paper, a TiNiCu shape memory alloy single-wall structure was fabricated by the directed energy deposition technique with a mixture of elemental Ti, Ni, and Cu powders following the atomic percentage of Ti50Ni45Cu5 to fully utilize the material flexibility of the additive manufacturing process to develop ternary shape memory alloys. The chemical composition, phase, and material properties at multiple locations along the build direction were studied, using scanning electron microscopy, energy-dispersive X-ray spectroscopy, X-ray diffraction, Vickers hardness test-ing, tensile testing, and differential scanning calorimetry. The location-dependent compositions of martensitic TiNi and austenitic TiNi phases, mechanical properties, and functional properties …

Absorption Of Nitrogen During Pulsed Wave L-Pbf Of 17-4 Ph Steel, Ben Brown, Joseph William Newkirk, Frank W. Liou

Materials Science and Engineering Faculty Research & Creative Works

In the fabrication of 17-4 PH by laser powder bed fusion (L-PBF) the well-documented occurrence of large amounts of retained austenite can be attributed to an elevated concentration of nitrogen present in the material. While the effects of continuous wave (CW) laser processing on in-situ nitrogen absorption characteristics have been evaluated, power modulated pulsed wave (PW) laser processing effects have not. In this study the effects of PW L-PBF processing of 17-4 PH on nitrogen absorption, phase composition, and mechanical performance are explored using commercially available PW L-PBF equipment and compared to samples produced by CW L-PBF. PW L-PBF samples …

Development Of In-Situ Radiometric Inspection Methods For Quality Assurance In Laser Powder Bed Fusion, Cody S. Lough

Doctoral Dissertations

“Laser Powder Bed Fusion (LPBF) metal Additive Manufacturing (AM) fabricates 3D metal parts layer-by-layer. The process enables production of geometrically complex parts that are difficult to inspect with traditional methods. The LPBF parts experience significant geometry driven thermal variations during manufacturing. This creates microstructure and mechanical property inhomogeneities and can stochastically cause defects. Mission critical applications require part qualification by measuring the defects non-destructively. The layer-to-layer nature of LPBF permits non-intrusive measurement of radiometric signals for a part’s entire volume. These measurements provide thermal features that correlate with the local part health. This research establishes Optical Emission Spectroscopy (OES) and …

Sources Of Quality Uncertainty In Laser Powder Bed Fusion Metal Additive Manufacturing, Zachary Young

Doctoral Dissertations

"Powder based additive manufacturing (AM) exhibits tremendous uncertainties, where variations in build quality is present despite utilizing similar build processing parameters. First, this work reports the features and formation mechanisms of five unique types of spatter during the LPBF process by in-situ high-speed, high-energy x-ray imaging. The unique physical characteristics of spatter are determined. The effect of laser scan speed and laser power on spatter formation, ejection, and mitigation are determined. Second, this work addresses the uncertainty challenge by identifying the sources of uncertainty in SLM by in-situ characterization due to variations from the additive manufacturing processing parameters needed for …

Numerical And Experimental Study Of Mechanical Properties For Laser Metal Deposition (Lmd) Process Part, Lan Li

Doctoral Dissertations

"Laser Metal Deposition (LMD), also called as, Laser Engineered Net Shaping (LENS), Directed Energy Deposition (DED), is a typical Additive Manufacturing (AM) technology, is used for advanced free-form fabrication. It creates parts by directly melting materials and depositing them on the workpiece layer by layer. In this process, the metal powder or fiber is melted within the melting pool by laser beam or electron beam and quickly solidifies to the deposited layer. LMD technology shows great advantages over traditional manufacturing on complex structure fabrication, including high building rates, easy material replacement and reduced material waste. These merits make the wide …

Hydrokinetic Turbine Composite Blades And Sandwich Structures: Damage Evaluation And Numerical Simulation, Mokhtar Fal

Doctoral Dissertations

“Composite materials are gaining interest due to their high strength to weight ratio. This study deals with both experimental and numerical approaches to cover the aspects of the failure of composite materials in hydrokinetic turbine applications. In Part I, the location and magnitude of failure in the horizontal axis water turbine carbon fiber-reinforced polymer (CFRP) composite blades with different laminate stacking sequences were investigated. Two lay-up orientations were adopted for this work ([0⁰]₄ and [0⁰/90⁰]_2s). A finite element analysis model was generated to examine the stresses along the blade. Five angles were introduced to study the effect …

Performance Evaluation Of Alsi10mg Fabricated By A Selective Laser Melting Process, David Michael Murphy

Masters Theses

“Selective laser melting is becoming a widely used additive manufacturing technique that melts metal powder in a layer by layer process in order to build a desired part or geometry. Like many additive processes, selective laser melting allows for fabrication of parts with complex geometries. In order to fabricate a fully dense part there are a number of variables to take into account including: powder characteristics, laser parameters, and environmental parameters. Each of these variables can affect the microstructure and thus the mechanical performance of an additively manufactured part. In this work, the aluminum alloy AlSi10Mg was investigated. AlSi10Mg is …

3d Printing Reinforced Concrete Structures, Bryce Tyler Tafolla

Masters Theses

"This study aims to investigate a 3D printing method to directly incorporate continuous reinforcement into concrete structures. The ability to design and produce complex structures with optimized topographical configuration can be used to reduce potential material waste while maintaining the required structural strength. Furthermore, the ability to actively incorporate reinforcement into printed members substantially reduces potential labor requirements and eliminates the need to set up formwork.

The study began its initial approach with a manual extrusion process containing reinforcement to observe the necessary constraints required to achieve a printing system with this functionality. The second stage of development was designing …

Influence Of Input Energy On Mechanical Properties Of Laser Powder Bed Fused Aisi 304l Stainless Steel, Tan Pan

Masters Theses

“Powder Bed Fusion process with selective laser melting technique is popularly adopted in additive manufacturing area on account of its layer by layer manufacturing fashion capable of fabricating components with complex internal and external geometries and structures. However, the process-property map is unique and vital for different materials and AM configurations used for fabrication. The process parameter is identified as a significant factor that heavily influences the properties and performances of the printed materials.

Current work aimed to extend the existing knowledge on Laser Powder Bed Fusion fabricated AISI 304L by accessing the influence of varying energy input on the …

A Framework For A Successful Additive Repair System, Todd E. Sparks

Doctoral Dissertations

“The goal of this research is to generate a revolutionary improvement to the usability and usefulness of additive repair technology by integrating a set of tools into a seamless work flow. Insufficient automation in the current repair process is a huge hurdle in achieving cost-effective, reliable repairs. Many opportunities have been missed due to inconsistency, quality issues and lack of robustness and flexibility. The present work addresses deficiencies in preparatory steps such as 2D and 3D geometry processing, parameter estimation, and path planning as well as on-machine execution of the path plan. The bulk of the effort is focused on …

Additive Manufacturing Of Customized Lithium-Ion Batteries: Process Fundamentals And Applications, Xiaowei Yu

Doctoral Dissertations

“In the pasting decades, considerable efforts have been spent in developing the next-generation lithium-ion batteries (LIBs), from advanced active materials to new manufacturing methods. The development of additive manufacturing (AM) has brought new opportunities to LIBs. In this work, two AM methods are introduced for fabricating electrodes of LIBs. The first method is aerosol printing, which is a solvent-based wet additive method. Whereas the second method is a solvent-free, dry printing method. The commonly used materials for current collectors and active materials (including cathodes and anodes) of LIBs are aerosol printed and the electrochemical functionalities of the printed materials are …

Development Of Lightweight Materials By Meso- And Microstructure Control, Myranda Shea Spratt

Doctoral Dissertations

”In this work, two lightweight structures – lattice structures and metal matrix syntactic foams (MMSF) – were studied. Honeycomb lattices were manufactured by powder bed selective laser melting (SLM) from 304L stainless steel. The wall thicknesses of these structures ranged from 0.2 to 0.5 mm. Surface roughness was the primary cause of dimensional mismatch between the expected and as-built structures with an average wall thickness increase of 0.12 mm. The strength of the honeycombs increased with increasing wall thickness. A feature of the SLM microstructure, the melt pool boundary, was also studied as a part of this work. 3D models …

Grain Size Effects In Selective Laser Melted Fe-Co-2v, Wesley Everhart, Joseph William Newkirk

Materials Science and Engineering Faculty Research & Creative Works

The material science of additive manufacturing (AM) has become a significant topic due to the unique way in which the material and geometry are created simultaneously. Major areas of research within inorganic materials include traditional structural materials, shape memory alloys, amorphous materials, and some new work in intermetallics. The unique thermal profiles created during selective laser melting (SLM) may provide new opportunities for processing intermetallics to improve mechanical and magnetic performance. A parameter set for the production of Fe-Co-2V material with additive manufacturing is developed and efforts are made to compare the traditional wrought alloy to the AM version of …

A Displacement Controlled Fatigue Test Method For Additively Manufactured Materials, Mohammad Masud Parvez, Yitao Chen, Sreekar Karnati, Connor Coward, Joseph William Newkirk, Frank W. Liou

Materials Science and Engineering Faculty Research & Creative Works

A novel adaptive displacement-controlled test setup was developed for fatigue testing on mini specimens. In property characterization of additive manufacturing materials, mini specimens are preferred due to the specimen preparation, and manufacturing cost but mini specimens demonstrate higher fatigue strength than standard specimens due to the lower probability of material defects resulting in fatigue. In this study, a dual gauge section Krouse type mini specimen was designed to conduct fatigue tests on additively manufactured materials. The large surface area of the specimen with a constant stress distribution and increased control volume as the gauge section may capture all different types …

A Framework For Process Inspection Of Metal Additive Manufacturing, Chih-Kun Cheng, Frank W. Liou, Yi-Chien Cheng, Sheng-Chih Shen

Mechanical and Aerospace Engineering Faculty Research & Creative Works

In this paper, we propose a process inspection framework for metal additive manufacturing (AM) processes. AM, also known as 3D printing, is the process of joining materials to make objects on the basis of 3D model data and is envisioned to play a strategic role in maintaining economic and scientific dominance. Different from conventional manufacturing methods, the AM process is a point-by-point and layer-by-layer manufacturing. Thus, there are many opportunities to generate a process error that can cause quality issues in an AM part. A systematic AM process inspection is needed to yield acceptable performance of the part. The critical …

The Influence Of Build Parameters On The Compressive Properties Of Selective Laser Melted 304l Stainless Steel, Okanmisope Fashanu, Mario F. Buchely, R. Hussein, S. Anandan, Myranda Spratt, Joseph William Newkirk, K. Chandrashekhara, H. Misak, M. A. Walker

Materials Science and Engineering Faculty Research & Creative Works

Process parameters used during Selective Laser Melting (SLM) process have significant effects on the mechanical properties of the manufactured parts. In this study, the influence of two build parameters (build orientation and hatch angle) on the compressive properties of 304L stainless steel was evaluated. SLM 304L samples were manufactured using three hatch angles, 0°, 67°,105° and two orientations, z-direction and x-direction, and tested using a compression frame according to ASTM E9-09. Bulk density was measured according to ASTM C373-17 before compression. Properties evaluated were the bulk density, yield strength, strength at 15% plastic-strain and strength at 30% plastic-strain. Results showed …

Additive Manufacturing Of Metal Functionally Graded Materials: A Review, Yitao Chen, Frank W. Liou

Mechanical and Aerospace Engineering Faculty Research & Creative Works

Functionally graded materials (FGMs) have attracted a lot of research interest due to their gradual variation in material properties that result from the non-homogeneous composition or structure. Metal FGMs have been widely researched in recent years, and additive manufacturing has become one of the most important approaches to fabricate metal FGMs. The aim of this paper is to review the research progress in metal FGMs by additive manufacturing. It will first introduce the unique properties and the advantages of FGMs. Then, typical recent findings in research and development of two major types of metal additive manufacturing methods, namely laser metal …

Design Of Lattice Structures With Graded Density Fabricated By Additive Manufacturing, Wenjin Tao, Yong Liu, Austin T. Sutton, Krishna C. R. Kolan, Ming-Chuan Leu

Mechanical and Aerospace Engineering Faculty Research & Creative Works

Lattice structures fabricated by Additive Manufacturing (AM) processes are promising for many applications, such as lightweight structures and energy absorbers. However, predicting and controlling of their mechanical behaviors is challenging due to the complexity of modeling and the uncertainties exist in the manufacturing process. In this paper, we explore the possibilities enabled by controlling the local densities. A set of lattice structures with different density gradients are designed using an implicit isosurface equation, and they are manufactured by Selective Laser Melting (SLM) process with 304L stainless steel. Finite element analysis and compression test are used to evaluate their mechanical properties. …

Development And Management Of Advanced Batteries Via Additive Manufacturing And Modeling, Jie Li

Doctoral Dissertations

"The applications of Li-ion batteries require higher energy and power densities, improved safety, and sophisticated battery management systems. To satisfy these demands, as battery performances depend on the network of constituent materials, it is necessary to optimize the electrode structure. Simultaneously, the states of the battery have to be accurately estimated and controlled to maintain a durable condition of the battery system. For those purposes, this research focused on the innovation of 3D electrode via additive manufacturing, and the development of fast and accurate physical based models to predict the battery status for control purposes. Paper I proposed a novel …

Investigation Of Additively Manufactured Polymer And Transparent Polymer Composites, Gregory Taylor

Doctoral Dissertations

"The objective of this study is an investigation of both the characterization of fused deposition modeling (FDM) of polymer thermoplastics and the manufacture of glass-reinforced transparent composites. The flexural behavior and fracture toughness of FDM parts are critical for the evaluation and optimization of both material and process. This study focuses on the performance of FDM Ultem 1010 specimens intended to be used as composite tooling due the material's high heat resistance. A three-point bend test is performed for flexure properties while a single edge notch bend test is performed for fracture toughness. For each of the tests, the build …