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Theses/Dissertations

2006

University of Central Florida

Materials Science and Engineering

Sol-gel

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Alumina-Aluminum Titanate-Titania Nanocomposite: Synthesis, Sintering Studies, Assessment Of Bioactivity And Its Mechanical And Electrical Properties, Vikas Somani Jan 2006

Alumina-Aluminum Titanate-Titania Nanocomposite: Synthesis, Sintering Studies, Assessment Of Bioactivity And Its Mechanical And Electrical Properties, Vikas Somani

Electronic Theses and Dissertations

This thesis reports the development, synthesis and characterization of a ceramic-ceramic nanocomposite system for its possible application as structural and electronic biomaterial in the biomedical industry. The study selected and synthesized alumina-aluminum titanate-titania (Al2O3-Al2TiO5-TiO2) nanoceramic composite using a simple Sol-Gel technique, which can be easily reproduced. Aluminum propoxide and titanium propoxide were used as precursor chemicals. Propanol and 2- methoxy ethanol were used as solvent and stabilizer, respectively. Thermal analyses were performed for a systematic understanding of phase evolution from the synthesized gel. X-Ray diffraction technique was used to confirm the phase evolution, phase purity, crystallite size and crystal structure(s) …


Synthesis, Processing And Characterization Of Nanocrystalline Titanium Dioxide, Shipeng Qiu Jan 2006

Synthesis, Processing And Characterization Of Nanocrystalline Titanium Dioxide, Shipeng Qiu

Electronic Theses and Dissertations

Titanium dioxide (TiO2), one of the basic ceramic materials, has found a variety of applications in industry and in our daily life. It has been shown that particle size reduction in this system, especially to nano regime, has the great potential to offer remarkable improvement in physical, mechanical, optical, biological and electrical properties. This thesis reports on the synthesis and characterization of the nanocrystalline TiO2 ceramic in details. The study selected a simple sol-gel synthesis process, which can be easily controlled and reproduced. Titanium tetraisopropoxide, isopropanol and deionized water were used as starting materials. By careful control of relative proportion …