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Identification Of Cave Minerals By Raman Spectroscopy: New Technology For Non-Destructive Analysis, William B. White
Identification Of Cave Minerals By Raman Spectroscopy: New Technology For Non-Destructive Analysis, William B. White
International Journal of Speleology
The identification of minerals from caves generally requires that samples be removed from the cave for analysis in the laboratory. The usual tools are X-ray powder diffraction, the optical microscope, and the scanning electron microscope. X-ray diffraction gives a definitive fingerprint by which the mineral can be identified by comparison with a catalog of reference patterns. However, samples must be ground to powder and unstable hydrated minerals may decompose before analysis is complete. Raman spectroscopy also provides a fingerprint useful for mineral identification but with the additional advantage that some a-priori interpretation of the spectra is possible (distinguishing carbonates from …
Vashegyite From Gaura Cu Muscă Cave (Locvei Mountains, Romania): A New And Rare Phosphate Occurrence, Bogdan P. Onac, Luminiţa Zaharia, Joe Kearns, Daniel Veres
Vashegyite From Gaura Cu Muscă Cave (Locvei Mountains, Romania): A New And Rare Phosphate Occurrence, Bogdan P. Onac, Luminiţa Zaharia, Joe Kearns, Daniel Veres
International Journal of Speleology
This study investigated the occurrence of vashegyite from a guano-rich deposit located in the Gaura cu Muscă Cave, Romania. Analytical methods used include optical microscopy, X-ray powder diffraction (XRD), scanning electron-microscopy (SEM), inductively coupled plasma-atomic emission spectrometry (ICP-AES), thermal investigations and Fourier-transform infrared (FT-IR) analyses. Vashegyite occurs as friable, chalky white, irregular nodules of up to 2.5 cm in diameter, within a 15 cm thick sequence of organic and minerogenic sediments. The chemical structural formula is: (Al10.91Fe3+0.06Na0.1Ca0.02Mg0.08)Σ=11.17[(PO4)8.78(SiO4)0.056]Σ=8.83(OH) …