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Grain Size Effects On Viscoelastic Relaxation Of Sub-Micron Thickness Fcc Metallic Films, Jeffrey Smyth Aug 2018

Grain Size Effects On Viscoelastic Relaxation Of Sub-Micron Thickness Fcc Metallic Films, Jeffrey Smyth

Theses and Dissertations

Sub-micron thickness metallic thin films are known to exhibit mechanical size effects, where the thin film mechanical behavior can differ significantly from that of a bulk version of the same material. One such mechanical behavior, and the focus of this work, is the unique thin film viscoelastic deformation response to sub-yield, low-strain stimuli in near-ambient temperature environments. In engineering components using bulk materials, strains within the elastic regime are generally considered instantaneous. It is only at higher operating temperatures that temporal deformation processes, such as creep, are considered in bulk component design. However, in Micro-Electro-Mechanical Systems (MEMS), specifically Radio Frequency ...


Development Of Microdialysis Probes In Series Approach Toward Eliminating Microdialysis Sampling Calibration: Miniaturization Into A Pdms Microfluidic Device, Randy Espinal Cabrera May 2018

Development Of Microdialysis Probes In Series Approach Toward Eliminating Microdialysis Sampling Calibration: Miniaturization Into A Pdms Microfluidic Device, Randy Espinal Cabrera

Theses and Dissertations

A new microdialysis sampling method and microfluidic device were developed in vitro. The method consisted of using up to four microdialysis sampling probes connected in series to evaluate the relative recovery (RR) of different model solutes methyl orange, fluorescein isothiocyanate (FITC)-dextran average mol. wt. 4,000 (FITC-4), FITC-10, FITC-20, and FITC-40. Different flow rates (0.8, 1.0, and 1.5 µL/min) were used to compare experimentally observed relative recoveries with theoretical estimations. With increasing the number of probes in series, the relative recovery increases and ~100% (99.7% ± 0.9%) relative recovery for methyl orange was obtained ...