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Mechanical Properties And Tension-Tension Fatigue Behavior Of A Novel Additively Manufactured Polymer Matrix Composite At Room And Elevated Temperature, Grayson M. Harber
Mechanical Properties And Tension-Tension Fatigue Behavior Of A Novel Additively Manufactured Polymer Matrix Composite At Room And Elevated Temperature, Grayson M. Harber
Theses and Dissertations
The tension-tension fatigue behavior of a novel additively manufactured AM carbon fiber reinforced polymer matrix composite was studied. This novel material system consists of T1100 carbon fibers, and a UV photocured resin developed by Continuous Composites and Sartomer. Tensile properties and tension-tension fatigue were investigated for the 090 fiber orientation as well as for the ±45 fiber orientation. Specimens with 0/90 fiber orientation were tested at ambient laboratory temperature 23 °C and at elevated temperature 150 °C, while the specimens with the ±45 fiber orientation were tested only at ambient laboratory temperature. Tension-tension fatigue testing was carried out with a …
Identification And Characterization Of Point Defects In Nonlinear Optical Crystals: Barium Gallium Selenide And Lithium Triborate, Brian C. Holloway
Identification And Characterization Of Point Defects In Nonlinear Optical Crystals: Barium Gallium Selenide And Lithium Triborate, Brian C. Holloway
Theses and Dissertations
Increased interest in developing new nonlinear optical materials has led to 3rd generation materials, such as BaGa4Se7 and LiB3O5. These two nonlinear optical crystals have the potential to enable development of tunable lasers operating across the mid-wave infrared and the ultraviolet regions, respectively. Coherent light sources are used in the development of enhanced technologies with commercial and defense-based applications such as: health and environmental monitoring devices, next-generation infrared countermeasures, and ballistic missile booster exhaust plume characterization. The performance of optical materials in high-powered military applications is largely limited by the presence of defects. These defects …
Influence Of Materials And Design Parameters On Zinc Oxide Surface Acoustic Devices, Samuel B. Dewhitt
Influence Of Materials And Design Parameters On Zinc Oxide Surface Acoustic Devices, Samuel B. Dewhitt
Theses and Dissertations
This thesis presents research into Zinc Oxide (ZnO) based resonators to include Width Extensional Mode (WEM), Length Extensional Mode (LEM), and Surface Acoustic Wave (SAW) devices. The design and operation of ZnO based SAW devices are investigated further to characterize design parameters and operating modes. Their design, fabrication, and results are discussed in detail. SAW device testing in conjunction with X-Ray Diffractometry (XRD) and Atomic Force Microscopy (AFM) are utilized to characterize ZnO and its deposition parameters on a variety of different substrates and interlayers, with different deposition temperatures and annealing parameters. These substrates include silicon, silicon oxide-on-silicon, and sapphire …
Formulation And Characterization Of Fast-Curing Plastic Scintillators With High-Z Loading, Theodore W. Stephens
Formulation And Characterization Of Fast-Curing Plastic Scintillators With High-Z Loading, Theodore W. Stephens
Theses and Dissertations
Development of novel fast-curing plastic scintillators is highly advantageous due to their potential to be manufactured via 3D printing. Several formulations were developed that exhibit enhanced photon sensitivity, producing modest but discernible photopeaks at an incident gamma energy of 122 keV. The photon sensitivity is achieved via bismuth high-Z loading; however, this practice typically results in diminished light yields. Subsequent formulations, which varied the photoinitiator concentration and curing time, demonstrated successful curing with sufficient plastic hardness, reduced purple discoloration, reduced heat buildup during curing, and resulted in less cracking during the curing process, all of which were correlated with lower …
Analysis Of Microscopic Carbon Fiber Fragments, Zachary R. Scott
Analysis Of Microscopic Carbon Fiber Fragments, Zachary R. Scott
Theses and Dissertations
Carbon Fiber (CF) has different tensile strengths and transverse moduli depending on how they are fabricated. Some CF is export controlled as it can be used for weapons, spacecraft, or gas centrifuges for enriching nuclear fuel. This research project explored a new way to prepare micron sized single CF threads to measure their transverse modulus and compare the moduli of non-export controlled CF to that of an export controlled CF. Five total polyacrylonitrile (PAN) fibers were used in this project, one of which was an export controlled fiber.
Thermal Considerations For Film Cooling Materials With Anisotropic Thermal Conductivity, Carol E. Bryant
Thermal Considerations For Film Cooling Materials With Anisotropic Thermal Conductivity, Carol E. Bryant
Theses and Dissertations
Higher performance requirements and reduced core sizes are driving increases in turbine inlet temperature in gas turbine engines, surpassing the melting point of advanced materials. Newer materials, such as composites, are being introduced into the hot sections of gas turbine engines. Components in the hot section use film cooling to prevent melting. One unique aspect of some high-temperature composites is they have a bulk anisotropic thermal conductivity, therefore heat flow differs relative to traditional metallic components. Film cooling designs can be revolutionized by leveraging anisotropy in high-temperature materials. The purpose of this research is to examine thermal considerations for using …
Determination Of Nonlinear Optical Properties For Gallium Arsenide Phosphide Ternary Compounds And For Tin Thiohypodiphosphate, Peter F. Norris
Determination Of Nonlinear Optical Properties For Gallium Arsenide Phosphide Ternary Compounds And For Tin Thiohypodiphosphate, Peter F. Norris
Theses and Dissertations
The Department of Defense and the commercial sector rely on coherent light sources to emit light that transmits through the atmosphere. Nonlinear optical effects in crystalline materials can be used to generate the laser waves, but certain nonlinear effects negatively impact the performance of laser generating materials. This thesis focuses on characterizing nonlinear optical properties for gallium arsenide phosphide ternary compounds and for tin thiohypodiphosphate. The Maker Fringe experiment is used to determine the d-coefficients of the materials, which describe the magnitude of the nonlinear response of the material. The Z-Scan experiment is used to calculate the nonlinear refractive …
Manufacturing Of A Ceramic Turbine Rotor For A Compact Jet Engine, Bryan T. Leicht
Manufacturing Of A Ceramic Turbine Rotor For A Compact Jet Engine, Bryan T. Leicht
Theses and Dissertations
The primary goal of this study was to develop a low-cost, timely, scalable manufacturing method that produced a ceramic turbine that can be tested as a drop-in replacement on a JetCat P400 small scale gas turbine engine. This research compared two processes for manufacturing a ceramic turbine utilizing a pour casting method and 3D printing using stereolithography ceramic manufacturing (SLCM). The pour casting method used Silicon Nitride to create a cast turbine using a sacrificial 3D printed mold. The SLCM method evaluated producing an alumina turbine using an ADMATEC Admaflex 300 SLCM printer to directly print a ceramic turbine. This …
Potential Solution To Meet Growing Demands Of Refractory Metal: Selective Laser Melting Of Molybdenum-Tungsten Alloy, Jae Yu
Theses and Dissertations
Selective laser melting (SLM) of refractory metals has been of high interest in research due to the metals’ potential desirable characteristics in aeronautical and space applications. In particular, molybdenum and tungsten have been the focus of several studies in the search for high temperature and high strength purposes in applications like supersonic aircraft, re-entry vehicles, nuclear fission, power generation, and other space systems. However, there is still a significant knowledge gap to process defect-free alloys and making use of them in practical engineering functions. The aim of this study is to characterize the relationship between the microstructure and mechanical properties …
Creep Behavior And Deformation Mechanisms Of Spark Plasma Sintered Oxide Ceramics For Aerospace Systems At 1300˚C - 1400˚C, David D. Swanson
Creep Behavior And Deformation Mechanisms Of Spark Plasma Sintered Oxide Ceramics For Aerospace Systems At 1300˚C - 1400˚C, David D. Swanson
Theses and Dissertations
The mechanical behavior of YAG and LuAG was investigated at elevated temperatures. The specific materials investigated in this work include high-purity, polycrystalline YAG, high-purity, polycrystalline LuAG, and two doped variants of YAG: 2at% Yb-doped, polycrystalline YAG and 2at% Er-doped, polycrystalline YAG. Several billets of each material were prepared and processed by means of spark plasma sintering (SPS). Many different sintering parameters were utilized in order to obtain materials with various physical properties and to identify the effects of sintering parameters on the average grain size of the resulting materials. The compressive creep behavior of these materials was investigated at 1300°C …
Improvements To Emissive Plume And Shock Wave Diagnostics And Interpretation During Pulsed Laser Ablation Of Graphite, Timothy I. Calver
Improvements To Emissive Plume And Shock Wave Diagnostics And Interpretation During Pulsed Laser Ablation Of Graphite, Timothy I. Calver
Theses and Dissertations
This dissertation covers nanosecond pulsed laser ablation of graphite for 4-5.7 J/cm2 fluences with 248 nm and 532 nm lasers in 1-180 Torr helium, argon, nitrogen, air, and mixed gas. Three experiments were performed to improve the interpretation of common diagnostics used to characterize pulsed laser ablation, find simple but universal scaling relationships for comparing dynamics across different materials and ablation conditions, and provide a systematic analysis of graphite emissive plume and shock wave dynamics. A scaling of the Sedov-Taylor energy ratio was developed and validated for a range of studies despite differences in wavelength, pulse duration, fluence, and …
Design And Fabrication Of Zinc Oxide Optofluidic Laser Elements, Kyle T. Bodily
Design And Fabrication Of Zinc Oxide Optofluidic Laser Elements, Kyle T. Bodily
Theses and Dissertations
This thesis systematically goes through the derivation, simulation, and experimentation of Zinc Oxide optofluidic micro laser elements. Single and coupled ring resonators were simulated to show single mode transmission as well as enhanced coupling capabilities when surrounded by high refractive index liquid. Devices with diameters ranging from 100-500 µm were successfully fabricated inexpensively through standard cleanroom procedures. The devices were tested using two different pump laser systems. Testing included such factors as high pump intensity, various angles of excitation, and low temperature. In all cases PL emission was observed and recorded.
Fatigue Of Two Oxide/Oxide Ceramic Matrix Composites At 1200°C In Air And In Steam. Effect Of Diamond Drilled Effusion Holes, Anthony R. Cabri
Fatigue Of Two Oxide/Oxide Ceramic Matrix Composites At 1200°C In Air And In Steam. Effect Of Diamond Drilled Effusion Holes, Anthony R. Cabri
Theses and Dissertations
The tension-tension fatigue behavior of two oxide-oxide ceramic matrix composites (CMCs) was investigated at 1200°C in laboratory air and steam. Both composites consist of a porous oxide matrix reinforced with laminated, woven mullite/alumina (NextelTM720) fibers. The first composite had an alumina matrix, while the second had an alumina-mullite matrix. First, we assessed the effects of incorporating mullite into the matrix material on fatigue performance by studying the tension-tension fatigue behavior of alumina-mullite matrix CMC. Second, we evaluated the effects of effusion holes on the alumina matrix CMC's fatigue performance. Specimens containing an array of 17 effusion holes of 0.5-mm diameter …
Static Fatigue Of Hi-Nicalon™ S Ceramic Fiber Tows At 600°C In Air And Silicic Acid-Saturated Steam, Caleigh M. Nelson
Static Fatigue Of Hi-Nicalon™ S Ceramic Fiber Tows At 600°C In Air And Silicic Acid-Saturated Steam, Caleigh M. Nelson
Theses and Dissertations
Ceramic matrix composites (CMCs) have the potential to be utilized in applications such as hypersonic vehicles, aircraft leading edges, hot sections of engines, and rocket nozzles. Of particular interest are advanced SiC/SiC composites that can withstand the elevated temperatures and harsh oxidizing environments while maintaining their properties and structural integrity under an applied load. Steam, a major component of combustion environment, is one such aggressive oxidizing environment. As steam passes through the SiC/SiC composite, entering the composite interior through the cracks in the SiC matrix, it becomes saturated with silicic acid, Si(OH)4. Before incorporating SiC/SiC composites in the …
Static Fatigue Of Hi-Nicalon S Fiber Tows At 500°C In Air And In Silicic Acid-Saturated Steam, Richard J. Reinink
Static Fatigue Of Hi-Nicalon S Fiber Tows At 500°C In Air And In Silicic Acid-Saturated Steam, Richard J. Reinink
Theses and Dissertations
Recent developments in aerospace propulsion systems, along with emerging interest in hypersonic air vehicles has emphasized the need for materials which can withstand extreme service environments. The leading candidates for the structural components expected to operate in these environments are SiC-based ceramic matrix composites (CMCs). When a CMC component is subjected to thermomechanical loads in an aggressive environment during service, surface cracks form. As steam penetrates cracks in the SiC matrix, it becomes saturated with silicic acid, (SI(OH)4) and attacks the SiC fibers. The interaction between the Hi-Nicalon™ S SiC fibers and the (SI(OH)4)-saturated steam is …
Tension-Tension Fatigue Behavior Of Nextel™ 720/Alumina-Mullite Ceramic Composite At 1200°C In Air And In Steam, Sarah A. Witzgall
Tension-Tension Fatigue Behavior Of Nextel™ 720/Alumina-Mullite Ceramic Composite At 1200°C In Air And In Steam, Sarah A. Witzgall
Theses and Dissertations
Uniaxial tension-tension fatigue performance of an oxide-oxide continuous fiber ceramic composite was studied at 1200°C in laboratory air and in steam. The composite is reinforced with laminated, 0/90 mullite/alumina (NEXTEL™720) fibers woven in an eight-harness satin weave and has a porous alumina/mullite matrix. There is no interphase between the fiber and matrix. The composite relies on the porous matrix for crack deflection and flaw tolerance. Tension-tension fatigue was examined for maximum stresses of 45 – 136 MPa in air and in steam. To assess the effects of the steam environment on fatigue performance, experimental results obtained in air are compared …
Investigation Of Ultem 9085 For Use In Printed Orbital Structures, William R. Gallagher
Investigation Of Ultem 9085 For Use In Printed Orbital Structures, William R. Gallagher
Theses and Dissertations
Additive manufacturing is revolutionizing industries ranging from medicine to space. However, the structural characteristics of plastic parts created by these methods are not as well understood as their more established counterparts. This research explored two relevant areas: how the structural characteristics of ULTEM 9085 plastic behaved after exposure to orbital conditions and the design of the cross-sectional area of a beam to be 3-D printed in microgravity based on the expected loads from the printer. To study orbital effects, ULTEM 9085 was printed into 1/4th scale ASTM D638- 14 dogbones using a Stratasys 450mc printer. These dogbones were placed in …
Dynamic Micromechanical Fabry-Perot Cavity Sensors Fabricated By Multiphoton Absorption Onto Optical Fiber Tips, Jeremiah C. Williams
Dynamic Micromechanical Fabry-Perot Cavity Sensors Fabricated By Multiphoton Absorption Onto Optical Fiber Tips, Jeremiah C. Williams
Theses and Dissertations
This research leveraged two-photon polymerization microfabrication to integrate dynamic mechanical components with Fabry-Perot resonators onto the ends of low-loss optical fibers to prototype 3 micro-optic devices. The first device featured a multi-positional mirror that enabled thin-film deposition onto cavities of any length with mirrors of significant curvature, for refractive index sensing. The second device combined an FP cavity with a spring body featuring easily scalable stiffness for pressure sensing. The third device presented a high-speed rotating micro-anemometer for measuring a wide range of gas flows. All devices represent a significant reduction in size and weight over commercially available devices.
Wideband Metasurface Antenna, Thomas A. Lepley
Wideband Metasurface Antenna, Thomas A. Lepley
Theses and Dissertations
This effort explored design of metasurface antennas and evaluated their suitability for ultra-wideband applications (2 to 18 GHz). Six unit cell types were characterized. Eigenmode simulations produced frequency vs. phase data for the unit cells, from which impedance vs. gap size data was computed. A holographic design equation was used to generate the metasurface antenna designs. The unit cell simulations revealed that the assumption of single mode operation is a constraint for wideband designs. An 8" by 8" metasurface antenna with a Rogers 3010 dielectric and a design frequency of 10 GHz was fabricated and tested. It had a 1.5:1 …
Alternate Materials For High-Speed Projectile Casing, Andrew W. Beard
Alternate Materials For High-Speed Projectile Casing, Andrew W. Beard
Theses and Dissertations
A high-speed projectile impact is a highly complex dynamic problem that can be simplified with the use of finite element analysis solvers. Abaqus/Explicit was used to evaluate the impact of various projectiles using a plane strain setup. Using a baseline stainless steel projectile, the proposed sandwich construction design was analyzed and compared to the baseline projectile. The overall goal was to see if a new composite casing could perform similarly to the simple baseline projectile. The sandwich construction used stainless steel, tungsten, and silicon-carbide reinforce aluminum as outer and inner shell materials. The core material was created using additive manufacturing …
Solution Anneal Heat Treatments To Enhance Mechanical Performance Of Additively Manufactured Inconel 718, David J. Newell
Solution Anneal Heat Treatments To Enhance Mechanical Performance Of Additively Manufactured Inconel 718, David J. Newell
Theses and Dissertations
The nickel-based superalloy Inconel 718 (IN718) is an excellent candidate among aerospace alloys for laser powder-bed fusion (LPBF) manufacturing. As-built LPBF IN718 has a vertically aligned columnar (001) microstructure which translates into orthotropic mechanical behavior. The post-process heat treatments for IN718 were developed 60 years ago for wrought and cast processes and do not mitigate the columnar microstructure of the LPBF process. Recrystallization is required to remove the columnar microstructure, which would allow for parts to be fabricated on different machines or in different orientations but still achieve the same properties. This research investigated the microstructure of LPBF IN718 as …
Fatigue Behavior Of An Advanced Melt-Infiltrated Sic/Sic Composite With Environmental Barrier Coating At 1200°C In Air And In Steam, Thaddeus M. Williams
Fatigue Behavior Of An Advanced Melt-Infiltrated Sic/Sic Composite With Environmental Barrier Coating At 1200°C In Air And In Steam, Thaddeus M. Williams
Theses and Dissertations
Advanced aerospace applications such as aircraft turbine engine components, hypersonic flight vehicles, and spacecraft reentry thermal protection systems require structural materials that have superior long-term mechanical properties under high temperature, high pressure, and varying environmental factors, such as moisture. Because of their low density, high strength and fracture toughness at high temperatures SiC fiber-reinforced SiC matrix composites are being evaluated for aircraft engine hot-section components. In these applications the composites will be subjected to various types of mechanical loadings at elevated temperatures in oxidizing environments. Because their constituents are intrinsically oxidation-prone, the most significant problem hindering SiC/SiC composites is oxidation …
The Design Of A Continuous Wave Molecular Nitrogen Stimulated Raman Laser In The Visible Spectrum, Timothy J. Bate
The Design Of A Continuous Wave Molecular Nitrogen Stimulated Raman Laser In The Visible Spectrum, Timothy J. Bate
Theses and Dissertations
Hollow-core photonic crystal fibers (HCPCFs) shows promise as a hybrid laser with higher nonlinear process limits and small beam size over long gain lengths. This work focuses on the design of a CW molecular nitrogen (N2) stimulated Raman laser. N2 offers Raman gains scaling up to 900 amg, scaling higher than H2. The cavity experiment showed the need to include Rayleigh scattering in the high pressure required for N2 Raman lasing. Even at relatively low pressure ssuch as 1,500 psi, high conversion percentages should be found if the fiber length is chosen based on …
Cn And C2 Spectroscopy On The Pulsed Ablation Of Graphite In The Visible Spectrum, Brandon A. Pierce
Cn And C2 Spectroscopy On The Pulsed Ablation Of Graphite In The Visible Spectrum, Brandon A. Pierce
Theses and Dissertations
An experimental study was conducted on the nanosecond pulsed laser ablation of graphite using a KrF laser at a fluence of 3.8 J/cm2 in Air, Ar, He, and N2. Optical emissions spectroscopy revealed the C2 Swan sequences and the CN Violet sequences. A spectroscopic model was developed to extract the molecular rotational and vibrational temperatures of each excited species for t=0.5-10 microseconds after laser irradiation. The rovibrational temperatures were found to vary with background gas for the CN Violet; however, only the vibrational temperature varied between He and the other background gases for C2 Swan. …
Design, Development, And Testing Of A Low Cost, Additively-Manufactured, Centrifugal Compressor, Aaron P. Bauer
Design, Development, And Testing Of A Low Cost, Additively-Manufactured, Centrifugal Compressor, Aaron P. Bauer
Theses and Dissertations
The three objectives of this research were to: 1.) design, build, and test AM compressors to substitute into COTS micro-gas turbine engines, 2.) provide initial correlations between FEA and compressor failure speed, and 3.) characterize the effects of AM on compressor performance. These goals improved the design cycle cost and the design-validation time cycle. ULTEM 9085, 300-AMB, and Onyx-Kevlar temperature-dependent tensile properties were measured. FEA-predicted failure speeds of stock compressor designs led design improvements, potentially fulfilling the original compressor requirements. Physical testing of the stock and ULTEM 9085 compressors occurred. Comparing these compressors' performances demonstrated that low cost, AM materials …
Modeling Hybrid Composites Using Tsai-Wu And Hashin Failure Criterion, Candice R. Roberts
Modeling Hybrid Composites Using Tsai-Wu And Hashin Failure Criterion, Candice R. Roberts
Theses and Dissertations
Hybrid composites require further study and testing for future use in various fields. This study focuses on simulating a Hybrid Composite using IM7-977-3 laminae with steel foils in Abaqus under bolt loading by using Hashin and Tsai-Wu failure criterion. Initial simulations contain only the IM7-977-3 composite with cohesive layers. Foil samples were then tested for accurate material properties from which the simulations were then updated to include steel foils. The two models show that Tsai-Wu failure criterion, while great for anisotropic material in tension, does not prove accuracy around the hole of the composite material which is in compression. Hashin …
Nonlinear Characterizing Of A New Titanium Nitride On Aluminum Oxide Metalens, Michael A. Cumming
Nonlinear Characterizing Of A New Titanium Nitride On Aluminum Oxide Metalens, Michael A. Cumming
Theses and Dissertations
A sample metalens generated from Titanium Nitride deposited onto Aluminum Oxide was designed to focus at 10 microns with a beam centered at 800nm, and when analyzed with high intensity illumination was found to have a focal length of 9.650 ±.003µm at an intensity of 16.93[MW/cm2 ]. Analyzing this change by comparing it to a Fresnel Lens’ physics shows that for this lens, the effective nonlinear index of refraction is certainly greater than the nonlinear index of just Titanium Nitride itself, at −1.6239 × 10−15[m2/W] compared to the materials −1.3 × 10−15[m2 …
Improved Fabrication For Micromirror Arrays, Enoc Flores
Improved Fabrication For Micromirror Arrays, Enoc Flores
Theses and Dissertations
Micromirror devices which consisted of one SU-8 2050 layer, two different exposures, and a series of metal depositions were constructed and evaluated. By varying the exposure, a micromirror structure was fabricated with different thicknesses, a ratio of 1.083 µm/(mJ/cm2) was found. The initial design consisted of four layers. The pillar was made of one SU-8 layer, and the top portion had three layers in the following order: gold, SU-8, and gold. This design could not be released and did not have characteristics of a flat and conformal reflective surface. Several variations of the initial design were explored and all of …
Displacement Damage Effects In Gesn Light Emitting Diodes, Kevin K. Choe
Displacement Damage Effects In Gesn Light Emitting Diodes, Kevin K. Choe
Theses and Dissertations
Potential future use on Earth-orbiting satellites calls for investigation into the suitability of GeSn based photonic devices in high energy proton environments. The electroluminescence (EL) intensity of Ge1-xSnx (x = 0, 0.02, 0.069, and 0.094) light emitting diodes was measured before and after irradiation by 2 MeV protons at relatively high fluence levels. The results showed that GeSn devices with higher Sn content were up to 10 times more resistant against proton displacement damage than the pure Ge (x = 0) devices. As Sn concentration increased, the band gap decreased, and V-P hole trap energy level moved further from the …
Characterization Of Metal Contacts On Hydrothermally Synthesized Uranium Dioxide For Novel Semiconductor Applications, Tory E. Robinson
Characterization Of Metal Contacts On Hydrothermally Synthesized Uranium Dioxide For Novel Semiconductor Applications, Tory E. Robinson
Theses and Dissertations
This research is focused on determining which metals or combinations of metals form effective electrical contacts on hydrothermally synthesized UO2 substrates to allow for additional work in characterization of the material as well as the feasibility of its use in semiconductor devices such as solid-state neutron detectors. A methodology was established for selection of candidate metals. Target mixtures composed of Au, Ag, Pt, and Mg were chosen along with several single-metals. Thin metal films were deposited onto tungsten probe tips and hydrothermally synthesized UO2 samples to allow for analysis of mechanical and deposited contact to the substrates through I-V measurements.