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Mechanical Engineering Faculty Research

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Electrospinning

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Morphology Control Of One-Dimensional Gallium Nitride Nanostructures By Modulating The Crystallinity Of Sacrificial Gallium Oxide Templates, Yun Taek Ko, Mijeong Park, Jingyeong Park, Jaeyun Moon, Yong Ho Choa, Young In Lee Jan 2021

Morphology Control Of One-Dimensional Gallium Nitride Nanostructures By Modulating The Crystallinity Of Sacrificial Gallium Oxide Templates, Yun Taek Ko, Mijeong Park, Jingyeong Park, Jaeyun Moon, Yong Ho Choa, Young In Lee

Mechanical Engineering Faculty Research

In this study, we demonstrated a method of controllably synthesizing one-dimensional nanostructures having a dense or a hollow structure using fibrous sacrificial templates with tunable crystallinity. The fibrous ga2o3 templates were prepared by calcining the polymer/gallium precursor nanofiber synthesized by an electrospinning process, and their crystallinity was varied by controlling the calcination temperature from 500oC to 900oC. gaN nanostructures were transformed by nitriding the ga2o3 nanofibers using NH3 gas. All of the transformed gaN nanostructures maintained a one-dimensional structure well and exhibited a diameter of about 50 nm, but their morphology was clearly distinguished according to the crystallinity of the …


Measurement Of Adhesion Energy Of Electrospun Polymer Membranes Using A Shaft-Loaded Blister Test, Shing Chung Josh Wong, Haining Na, Pei Chen Jun 2013

Measurement Of Adhesion Energy Of Electrospun Polymer Membranes Using A Shaft-Loaded Blister Test, Shing Chung Josh Wong, Haining Na, Pei Chen

Mechanical Engineering Faculty Research

This study aims to examine the adhesion work of electrospun polymer nano- and micro-fibers. The adhesion energy at the interface of electrospun membrane and a rigid substrate is characterized by a shaft-loaded blister test (SLBT). By controlling the processing parameters, polyvinylidene fluoride (PVDF) fibrous membranes are prepared with fiber diameters ranging from 201 ± 86 nm to 2,724 ± 587 nm. The adhesion energy between electrospun membrane and rigid substrate increases from 8.1 ± 0.7 mJ/m2 to 258.8 ± 43.5 mJ/m2 by use of smaller fiber diameters. Adhesion energies between electrospun PVDF membranes and SiC substrates made of different grain …