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Stainless-Steel Column For Robust High Temperature Microchip Gas Chromatography, Abhijit Ghosh, Austin R. Foster, Jacob C. Johnson, Carlos R. Vilorio, Luke T. Tolley, Brian D. Iverson, Aaron R. Hawkins, H. Dennis Tolley, Milton L. Lee Dec 2019

Stainless-Steel Column For Robust High Temperature Microchip Gas Chromatography, Abhijit Ghosh, Austin R. Foster, Jacob C. Johnson, Carlos R. Vilorio, Luke T. Tolley, Brian D. Iverson, Aaron R. Hawkins, H. Dennis Tolley, Milton L. Lee

Faculty Publications

This paper reports the first results of a robust, high performance, stainless-steel microchip gas chromatography (GC) column that is capable of analyzing complex real world mixtures as well as operating at very high temperatures. Using a serpentine design, a 10 m column with an approximately semicircular cross section with a 52 µm hydraulic diameter (Dh) was produced in a 17 cm x 6.3 cm x 0.1 cm rectangular steel chip. The channels were produced using a multilayer chemical etch and diffusion bonding process, and metal nuts were brazed onto the inlet and outlet ports allowing for column ...


Towards Overcoming The Curse Of Dimensionality: The Third-Order Adjoint Method For Sensitivity Analysis Of Response-Coupled Linear Forward/Adjoint Systems, Uncertainty Quantification And Predictive Modeling With Applications To Nuclear Energy Systems, Dan Gabriel Cacuci Nov 2019

Towards Overcoming The Curse Of Dimensionality: The Third-Order Adjoint Method For Sensitivity Analysis Of Response-Coupled Linear Forward/Adjoint Systems, Uncertainty Quantification And Predictive Modeling With Applications To Nuclear Energy Systems, Dan Gabriel Cacuci

Faculty Publications

This work presents the Third-Order Adjoint Sensitivity Analysis Methodology (3rd-ASAM) for response-coupled forward and adjoint linear systems. The 3rd-ASAM enables the efficient computation of the exact expressions of the 3rd-order functional derivatives (“sensitivities”) of a general system response, which depends on both the forward and adjoint state functions, with respect to all of the parameters underlying the respective forward and adjoint systems. Such responses are often encountered when representing mathematically detector responses and reaction rates in reactor physics problems. The 3rd-ASAM extends the 2nd-ASAM in the quest to overcome the “curse of dimensionality” in sensitivity analysis, uncertainty quantification and predictive ...


Ligaos Is A Fast Li-Ion Conductor: A First-Principles Prediction, Xueling Lei, Wenjun Wu, Bo Xu, Chuying Ouyang, Kevin Huang Oct 2019

Ligaos Is A Fast Li-Ion Conductor: A First-Principles Prediction, Xueling Lei, Wenjun Wu, Bo Xu, Chuying Ouyang, Kevin Huang

Faculty Publications

Solid Li-ion conducting electrolytes are highly sought for all solid-state Li-batteries, which are considered the next-generation safe batteries. Here a systematic computational study on the intrinsic transport properties of lithium gallium oxysulfide, LiGaOS (S. G. Pmc21), as a potential solid-state Li-ion electrolyte have been reported. The phonon dispersion spectrum analysis indicates that LiGaOS crystal structure is dynamically stable. The energy band structure and density of states calculations suggest that LiGaOS is an insulator with a wide indirect band gap of ∼5.44 eV. The CI-NEB calculations reveal that the “kick-off” collective migration via Li-interstitials is the dominant conduction mechanism ...


The Influence Of Temperature On Dispersion Of Particles On Liquid Surfaces, Sathish Kumar Gurupatham, Valmiki Sooklal, A. Hensen, M. Conner Sep 2019

The Influence Of Temperature On Dispersion Of Particles On Liquid Surfaces, Sathish Kumar Gurupatham, Valmiki Sooklal, A. Hensen, M. Conner

Faculty Publications

It was shown recently that small particles and powders spontaneously disperse on liquid surfaces when they come in contact with the interface for the first time (Figure 2). This happens due to the combined effect of the capillary force, buoyant weight of the particle and the viscous drag that the particles experience when they encounter the liquid surface. The particles undergo oscillations normal to the interface before they come to the equilibrium position on the interface. These oscillations, in turn, induce a flow on the interface which disperses the particles radially outward. This phenomenon has a significant role in the ...


Takeoff And Performance Tradeoffs Of Retrofit Distributed Electric Propulsion For Urban Transport, Kevin Moore, Andrew Ning Aug 2019

Takeoff And Performance Tradeoffs Of Retrofit Distributed Electric Propulsion For Urban Transport, Kevin Moore, Andrew Ning

Faculty Publications

While vertical takeoff and landing aircraft have shown promise for urban air transport, distributed electric propulsion on existing aircraft may offer immediately implementable alternatives. Distributed electric propulsion could potentially decrease takeoff distances enough to enable thousands of potential inter-city runways. This conceptual study explores the effects of a retrofit of open-bladed electric propulsion units. To model and explore the design space we use blade element momentum method, vortex lattice method, linear-beam finite element analysis, classical laminate theory, composite failure, empirically-based blade noise modeling, motor and motor-controller mass models, and gradient-based optimization. With liftoff time of seconds and the safe total ...


Transverse Vibration Of Clamped-Pinned-Free Beam With Mass At Free End, Jonathan Hong, Jacob Dodson, Simon Laflamme, Austin Downey Jul 2019

Transverse Vibration Of Clamped-Pinned-Free Beam With Mass At Free End, Jonathan Hong, Jacob Dodson, Simon Laflamme, Austin Downey

Faculty Publications

Engineering systems undergoing extreme and harsh environments can often times experience rapid damaging effects. In order to minimize loss of economic investment and human lives, structural health monitoring (SHM) of these high-rate systems is being researched. An experimental testbed has been developed to validate SHM methods in a controllable and repeatable laboratory environment. This study applies the Euler-Bernoulli beam theory to this testbed to develop analytical solutions of the system. The transverse vibration of a clamped-pinned-free beam with a point mass at the free end is discussed in detail. Results are derived for varying pin locations and mass values. Eigenvalue ...


Concrete Crack Detection And Monitoring Using A Capacitive Dense Sensor Array, Jin Yan, Austin Downey, Alessandro Cancelli, Simon Laflamme, An Chen, Jian Li, Filippo Ubertini Apr 2019

Concrete Crack Detection And Monitoring Using A Capacitive Dense Sensor Array, Jin Yan, Austin Downey, Alessandro Cancelli, Simon Laflamme, An Chen, Jian Li, Filippo Ubertini

Faculty Publications

Cracks in concrete structures can be indicators of important damage and may significantly affect durability. Their timely identification can be used to ensure structural safety and guide on-time maintenance operations. Structural health monitoring solutions, such as strain gauges and fiber optics systems, have been proposed for the automatic monitoring of such cracks. However, these solutions become economically difficult to deploy when the surface under investigation is very large. This paper proposes to leverage a novel sensing skin for monitoring cracks in concrete structures. This sensing skin is constituted of a flexible electronic termed soft elastomeric capacitor, which detects a change ...


Vibration-Based In-Situ Detection And Quantification Of Delamination In Composite Plates, Hanfei Mei, Asaad Migot, Mohammad Faisal Haider, Roshan Joseph, Md Yeasin Bhuiyan, Victor Giurgiutiu Apr 2019

Vibration-Based In-Situ Detection And Quantification Of Delamination In Composite Plates, Hanfei Mei, Asaad Migot, Mohammad Faisal Haider, Roshan Joseph, Md Yeasin Bhuiyan, Victor Giurgiutiu

Faculty Publications

This paper presents a new methodology for detecting and quantifying delamination in composite plates based on the high-frequency local vibration under the excitation of piezoelectric wafer active sensors. Finite-element-method-based numerical simulations and experimental measurements were performed to quantify the size, shape, and depth of the delaminations. Two composite plates with purpose-built delaminations of different sizes and depths were analyzed. In the experiments, ultrasonic C-scan was applied to visualize the simulated delaminations. In this methodology, piezoelectric wafer active sensors were used for the high-frequency excitation with a linear sine wave chirp from 1 to 500 kHz and a scanning laser Doppler ...


Controlling The Oxygen Electrocatalysis On Perovskite And Layered Oxide Thin Films For Solid Oxide Fuel Cell Cathodes, Gene Yang, Wonsang Jung, Sung-Jin Ahn, Dongkyu Lee Mar 2019

Controlling The Oxygen Electrocatalysis On Perovskite And Layered Oxide Thin Films For Solid Oxide Fuel Cell Cathodes, Gene Yang, Wonsang Jung, Sung-Jin Ahn, Dongkyu Lee

Faculty Publications

Achieving the fast oxygen reduction reaction (ORR) kinetics at the cathode of solid oxide fuel cells (SOFCs) is indispensable to enhance the efficiency of SOFCs at intermediate temperatures. Mixed ionic and electronic conducting (MIEC) oxides such as ABO3 perovskites and Ruddlesden-Popper (RP) oxides (A2BO4) have been widely used as promising cathode materials owing to their attractive physicochemical properties. In particular, oxides in forms of thin films and heterostructures have enabled significant enhancement in the ORR activity. Therefore, we aim to give a comprehensive overview on the recent development of thin film cathodes of SOFCs. We discuss ...


Influence Of Micro-Structured Superhydrophobic Surfaces On Nucleation And Natural Convection In A Heated Pool, Adam Cowley, Daniel Maynes, Julie Crockett, Brian D. Iverson Feb 2019

Influence Of Micro-Structured Superhydrophobic Surfaces On Nucleation And Natural Convection In A Heated Pool, Adam Cowley, Daniel Maynes, Julie Crockett, Brian D. Iverson

Faculty Publications

This word experimentally explores sub-boiling pool nucleation on micro-structured superhydrophobic surfaces. All surfaces tested were submerged in a 20 mm deep pool of water and heated from below to maintain a constant surface temperature, while the side walls of the pool were insulated, and the top was covered. Three thermocouples positioned in the pool obtain the average pool temperature. A heat flux sensor is placed directly beneath the surface to measure the heat flux supplied to the pool. Free convection heat transfer coefficients are obtained for the sub-boiling temperature range of 40 – 90 ºC. Six surface types are studied: smooth ...


Recent Advances In Piezoelectric Wafer Active Sensors For Structural Health Monitoring Applications, Hanfei Mei, Mohammad Faisal Haider, Roshan Joseph, Asaad Migot, Victor Giurgiutiu Jan 2019

Recent Advances In Piezoelectric Wafer Active Sensors For Structural Health Monitoring Applications, Hanfei Mei, Mohammad Faisal Haider, Roshan Joseph, Asaad Migot, Victor Giurgiutiu

Faculty Publications

In this paper, some recent piezoelectric wafer active sensors (PWAS) progress achieved in our laboratory for active materials and smart structures (LAMSS) at the University of South Carolina: http: //www.me.sc.edu/research/lamss/ group is presented. First, the characterization of the PWAS materials shows that no significant change in the microstructure after exposure to high temperature and nuclear radiation, and the PWAS transducer can be used in harsh environments for structural health monitoring (SHM) applications. Next, PWAS active sensing of various damage types in aluminum and composite structures are explored. PWAS transducers can successfully detect the simulated crack ...


Propagating, Evanescent, And Complex Wavenumber Guided Waves In High-Performance Composites, Victor Giurgiutiu, Mohammad Faisal Haider Jan 2019

Propagating, Evanescent, And Complex Wavenumber Guided Waves In High-Performance Composites, Victor Giurgiutiu, Mohammad Faisal Haider

Faculty Publications

The study of propagating, evanescent and complex wavenumbers of guided waves (GWs) in high-performance composites using a stable and robust semi-analytical finite element (SAFE) method is presented. To facilitate understanding of the wavenumber trajectories, an incremental material change study is performed moving gradually from isotropic aluminum alloy to carbon fiber reinforced polymer (CFRP) composites. The SAFE results for an isotropic aluminum alloy plate are compared with the exact analytical solutions, which shows that N = 20 SAFE elements across the thickness provides <0.5% error in the highest evanescent wavenumber for the given frequency-wavenumber range. The material change study reveals that reducing the transverse and shear moduli moves the wavenumber solution towards one similar to composite material. The comparison of the propagating, evanescent and complex wavenumber trajectories between composites and aluminum alloy show that antisymmetric imaginary Lamb wave modes always exist in composites although they may not exist in isotropic aluminum alloy at some frequencies. The wavenumber trajectories for a unidirectional CFRP plate show that the range of real wavenumber is much smaller than in the isotropic aluminum alloy. For laminated CFRP composite plates (e.g., unidirectional, off-axis, transverse, cross-ply and quasi-isotropic laminates), the quasi Lamb wave and shear horizontal (SH) wave trajectories are also identified and discussed. The imaginary SH wave trajectories in laminated composites are distorted due to the presence of ±45 plies. The convergence study of the SAFE method in various CFRP laminates indicates that sufficient accuracy can always be achieved by increasing the number of SAFE elements. Future work will address the stress-continuity between composite layers.


Optimization Of Turbine Design In Wind Farms With Multiple Hub Heights, Using Exact Analytic Gradients And Structural Constraints, Andrew P.J. Stanley, Andrew Ning, Katherine Dykes Jan 2019

Optimization Of Turbine Design In Wind Farms With Multiple Hub Heights, Using Exact Analytic Gradients And Structural Constraints, Andrew P.J. Stanley, Andrew Ning, Katherine Dykes

Faculty Publications

Wind farms are generally designed with turbines of all the same hub height. If wind farms were designed with turbines of different hub heights, wake interference between turbines could be reduced, lowering the cost of energy (COE). This paper demonstrates a method to optimize onshore wind farms with two different hub heights using exact, analytic gradients. Gradient-based optimization with exact gradients scales well with large problems and is preferable in this application over gradient-free methods. Our model consisted of the following: a version of the FLOw Redirection and Induction in Steady-State wake model that accommodated three- dimensional wakes and calculated ...