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- Scanning electron microscopy (7)
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Articles 1 - 13 of 13
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The Wear Behavior Of Cross-Linked Uhmwpe Under Dry And Bovine Calf Serum-Lubricated Conditions
The Wear Behavior Of Cross-Linked Uhmwpe Under Dry And Bovine Calf Serum-Lubricated Conditions
A.S. Md Abdul Haseeb
The present study was performed to investigate the effects of gamma radiation on the wear behavior of unirradiated and irradiated ultra-high-molecular-weight polyethylene (UHMWPE) against Ti-6Al-4V under dry and lubricated conditions at different applied loads. The UHMWPE specimens were exposed directly to nominal doses of 0, 25, 40, 50, and 100 kGy. Scanning electron microscope (SEM) analysis of the worn surface of UHMWPE and Ti-6Al-4V was performed to understand the mechanism of wear involved between the contact surfaces during wear testing. From the wear test results, there were significant differences between the wear of unirradiated UHMWPE and UHMWPE irradiated at 25, …
Effects Of Addition Of Copper Particles Of Different Size To Sn-3.5ag Solder
Effects Of Addition Of Copper Particles Of Different Size To Sn-3.5ag Solder
A.S. Md Abdul Haseeb
No abstract provided.
Gas Sensors Based On One Dimensional Nanostructured Metal-Oxides: A Review
Gas Sensors Based On One Dimensional Nanostructured Metal-Oxides: A Review
A.S. Md Abdul Haseeb
Recently one dimensional (1-D) nanostructured metal-oxides have attracted much attention because of their potential applications in gas sensors. 1-D nanostructured metal-oxides provide high surface to volume ratio, while maintaining good chemical and thermal stabilities with minimal power consumption and low weight. In recent years, various processing routes have been developed for the synthesis of 1-D nanostructured metal-oxides such as hydrothermal, ultrasonic irradiation, electrospinning, anodization, sol-gel, molten-salt, carbothermal reduction, solid-state chemical reaction, thermal evaporation, vapor-phase transport, aerosol, RF sputtering, molecular beam epitaxy, chemical vapor deposition, gas-phase assisted nanocarving, UV lithography and dry plasma etching. A variety of sensor fabrication processing routes …
Effect Of Temperature On The Corrosion Behavior Of Mild Steel Upon Exposure To Palm Biodiesel
Effect Of Temperature On The Corrosion Behavior Of Mild Steel Upon Exposure To Palm Biodiesel
A.S. Md Abdul Haseeb
Recently biodiesel, as an alternative fuel is getting more significance to replace diesel fuel completely or partially. However, corrosion of automotive materials in biodiesel is a major concern as this can reduce engine life. This study aims to investigate the corrosion behavior of mild steel at three different temperatures such as room temperature, 50 and 80 °C. Static immersion tests in B0 (diesel), B50 (50% biodiesel in diesel), B100 (biodiesel) were carried out for 1200 h. At the end of the tests, corrosion characteristic was investigated by weight loss measurements and changes of the exposed metal surface. Fuels were analyzed …
Failure Analysis Of Retrieved Uhmwpe Tibial Insert In Total Knee Replacement
Failure Analysis Of Retrieved Uhmwpe Tibial Insert In Total Knee Replacement
A.S. Md Abdul Haseeb
This study involves the failure analysis of an ultra high molecular polyethylene (UHMWPE) tibial insert from Apollo® Total Knee System, which was removed after 10. years of service from 70. years old female patient. The tibial insert was investigated by using a stereoscope, scanning electron microscope (SEM), infinite focus microscope (IFM) and energy disperse spectroscopy (EDS) to characterize the morphology and composition of the bearing surface. Differential scanning calorimetry (DSC) and Fourier transform spectroscopy (FTIR) were employed to characterize the degradation and crystallinity of the component. Gel-permeation chromatography (GPC) was used to measure the polyethylene tibial insert molecular weight. Results …
Structural And Mechanical Properties Of Nanostructured Tio2 Thin Films Deposited By Rf Sputtering
Structural And Mechanical Properties Of Nanostructured Tio2 Thin Films Deposited By Rf Sputtering
A.S. Md Abdul Haseeb
This study mainly aims to evaluate the effects of substrate temperatures on the mechanical properties of TiO2 thin films deposited on glass substrates by radio-frequency (RF) magnetron sputtering. All titania films possess anatase structure having a nodular morphology. AES results reveal that Si and Na ions from glass diffuse into TiO2 films at higher substrate temperatures. Micro-scratch and wear tests were conducted to evaluate their mechanical and tribological properties. The adhesion critical loads of TiO2 films deposited at room temperature, 200 and 300°C are found to be 1.51, 1.54 and 1.08N, respectively. Scratch hardness also increases from 11.5 to 13.6GPa …
Effects Of Annealing Treatment On Optical Properties Of Anatase Tio 2 Thin Films
Effects Of Annealing Treatment On Optical Properties Of Anatase Tio 2 Thin Films
A.S. Md Abdul Haseeb
In this investigation, anatase TiO 2 thin films were grown by radio frequency magnetron sputtering on glass substrates at a high sputtering pressure and room temperature. The anatase films were then annealed at 300-600 °C in air for a period of 1 hour. To examine the structure and morphology of the films, X-ray diffraction (XRD) and atomic force microscopy (AFM) methods were used respectively. From X-ray diffraction patterns of the TiO 2 films, it was found that the as-deposited film showed some differences compared with the annealed films and the intensities of the peaks of the crystalline phase increased with …
Production And Purification Of Zircon Opacifier From Zircon Found In The Coastal Area Of Bangladesh
Production And Purification Of Zircon Opacifier From Zircon Found In The Coastal Area Of Bangladesh
A.S. Md Abdul Haseeb
In this study the potentiality of Bangladesh zircon as a raw material for opacifier was examined. Preparation of zircon flour was done by both wet and dry ball milling. Wet milling of zircon was found to be much efficient than dry milling. Zircon flour of peak size 8 μm obtained by wet milling was purified by leaching in concentrated H2SO4 acid. Leaching time was varied from 2 to 20 h and sulphuric acid concentration ranged from 10 to 80 ml/l. Both un-purified and purified Bangladesh zircon flour were tested for their performance as opacifier in a couple of local ceramic …
Tribo-Surface Characteristics Of Al-B4c And Al-Sic Composites Worn Under Different Contact Pressures
Tribo-Surface Characteristics Of Al-B4c And Al-Sic Composites Worn Under Different Contact Pressures
A.S. Md Abdul Haseeb
Tribo-surface characteristics of two aluminium metal matrix composites (Al-MMC) of compositions Al-13 vol%B4C and Al-13 vol%SiC sliding against a commercial phenolic brake pad have been investigated under dry conditions. The wear tests were carried out using a pin-on-disc type apparatus at a linear speed of 1.62 m s-1 under contact pressures ranging from 0.75 to 3.00 MPa. The coefficient of friction was recorded on line. Wear rates were calculated from mass loss measurements. Scanning electron microscope equipped with energy dispersive X-ray spectroscopy was used to examine the tribo-surface. It is found that wear rate of both composites increases with increasing …
Modeling Of The Effects Of Athermal Flow Strength And Activation Energy For Dislocation Glide On The Nanoindentation Creep Of Nickel Thin Film At Room Temperature
A.S. Md Abdul Haseeb
Nanoindentation creep behaviour of nickel at room temperature has been modeled based on the obstacle-controlled dislocation glide mechanism. Using the model, the effects of two important materials parameters viz. the activation free energy required by dislocation to overcome an obstacle without any aid from external stress, ΔF and the athermal flow strength, τ0, which is the flow strength of solids at 0 K are systematically studied. It has been found that ΔF plays a dominant role in room temperature creep properties of nickel. The role of ΔF is particularly dominant in determining the time dependent deformation. On the other hand, …
Velocity Effects On The Wear, Friction And Tribochemistry Of Aluminum Mmc Sliding Against Phenolic Brake Pad
A.S. Md Abdul Haseeb
Two aluminum metal matrix composites (MMC) reinforced with 13 vol.% of SiC or B4C particles were made by stir casting followed by hot extrusion. Effects of sliding velocity on the wear, friction and tribochemistry of the worn surfaces of both composites sliding against a commercial phenolic brake pad have been investigated under dry condition. The wear tests were carried out using a pin-on-disc type apparatus at two linear sliding speeds: 1.62 and 4.17 m s-1 under a constant contact pressure of 0.75 MPa for a sliding distance of 5832 m. The coefficient of friction was recorded and wear rate of …
On The Nature Of The Electrochemically Synthesized Hard Fe-0.96 Mass Pct C Alloy Film
On The Nature Of The Electrochemically Synthesized Hard Fe-0.96 Mass Pct C Alloy Film
A.S. Md Abdul Haseeb
A hard Fe-0.96 mass pet C alloy with a hardness value of 810 HV has been electrochemically synthesized from a ferrous sulfate bath containing a small amount of citric acid and L-ascorbic acid. The nature of the alloy has been investigated by a number of techniques, including X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), scanning electron microscopy (SEM), transmission electron microscopy (TEM), Mössbauer spectroscopy, differential scanning calorimetry (DSC), and magnetic measurements. The decomposition behavior of the alloy is also studied and compared with that of thermally prepared martensite. It has been found that the electrochemically deposited Fe-C alloy exists in …
Study Of The Wear Behaviour Of Al-4.5% Cu-3.4% Fe In Situ Composite: Effect Of Thermal And Mechanical Processing
A.S. Md Abdul Haseeb
Wear behaviour of as-cast and heat-treated spheroidal graphite (SG) cast iron has been studied under dry sliding conditions using a pin-on-disc type apparatus. Wear tests were carried out at a linear sliding speed of 0.88 m s -1, under a constant load of 1.5 kg. All tests were performed in ambient air at room temperature. Extent of wear damage and wear mechanisms were investigated by means of weight loss measurement, optical microscopy, microhardness measurement and X-ray diffractometry on wear debris. The wear rate measured after 9500 m of sliding is found to be about three times higher in the as-cast …