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Physical Sciences and Mathematics

Eurasian Journal of Physics and Functional Materials

2020

Synthesis

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Phase Composition And Thermoelectric Properties Of The Nanocomposite Alloys Naxcu2-X-Ys, M. M. Kubenova, M. Kh. Balapanov, K. A. Kuterbekov, R. Kh. Ishembetov, A. M. Kabyshev, Y. Kh. Yulaeva Mar 2020

Phase Composition And Thermoelectric Properties Of The Nanocomposite Alloys Naxcu2-X-Ys, M. M. Kubenova, M. Kh. Balapanov, K. A. Kuterbekov, R. Kh. Ishembetov, A. M. Kabyshev, Y. Kh. Yulaeva

Eurasian Journal of Physics and Functional Materials

Nanocrystalline alloys of the compositions Na 0.05 Cu 1.95 S, Na 0.075 Cu 1.925 S, Na 0.10 Cu 1.90 S, Na 0.125 Cu 1.750 S, Na 0.15 Cu 1.85 S, Na 0.17 Cu 1.80 S, Na 0.20 Cu 1.77 S were synthesized in a melt medium mixtures of hydroxides NaOH and KOH at a temperature of about 165 ◦ C. X-ray phase analysis showed that the alloys are heterophasic and consist of phases of Cu 9 S 5 digenite, CuS 2 copper disulfide, Covellite CuS, Cu 7 S 4 anilite in various combinations. The crystallite sizes range from 16 to …