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Minerva 2004, The Honors College Dec 2004

Minerva 2004, The Honors College

Minerva

This issue of Minerva includes an article on HON 350: An Introduction to Functional Genomics; an article on the creation and inaugural year of HON 180: A Cultural Odyssey; a profile on Honors alumnus, Charles Stanhope and his 2004 Distinguished Honors Graduate Lecture; and interviews with Allison Kelly, Jessica Hudec, and Jennifer Merchant on their experiences as Honors student-athletes.

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Electrochemical Behaviours Of Hemoglobin-Ddab-Modified Powder Microelectrode And The Application Of The Powder Microelectrode In Determination Of Nitric Oxide, Zhi-Mou Guo, Huan Liu, Jian Chen, Wen-Ting Zhang Nov 2004

Electrochemical Behaviours Of Hemoglobin-Ddab-Modified Powder Microelectrode And The Application Of The Powder Microelectrode In Determination Of Nitric Oxide, Zhi-Mou Guo, Huan Liu, Jian Chen, Wen-Ting Zhang

Journal of Electrochemistry

The electrochemical behaviours of DDAB-Hb-PME were studied in this paper. The (apparent) surface concentration of Hb was enhanced greatly by using the powder microelectrode (technique). NO reacts with Hb and absorbs on the surface of the modified carbon powder. Therefore, the output of the electrode was enhanced greatly by employing PME with higher reaction surface (area). The sensitivity of DDAB-Hb-PME is 3.1 mA/μmol·L~(-1)·cm~(2), which is much larger than the values obtained with the traditional electrodes. The detection limit is 9 nmol·L~(-1) and the linear response range is 9～100 nmol·L~(-1).

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Electrochemical Investigations On Pitting Susceptibility Of Iron-Based Alloy, Wei-Shan Li, Hong-Yu Chen, Zhong-Zhi Yuan, Hong Li, Qi-Ming Huang, Dong-Sheng Lv Nov 2004

Electrochemical Investigations On Pitting Susceptibility Of Iron-Based Alloy, Wei-Shan Li, Hong-Yu Chen, Zhong-Zhi Yuan, Hong Li, Qi-Ming Huang, Dong-Sheng Lv

Journal of Electrochemistry

The formation process of passive film on iron and electronic properties and pitting susceptibility of an iron-based alloy are investigated by using linear potential sweep, alternative current impedance and electrochemical nose technologies. The relationship between reciprocal square capacitance and potential following the Mott-Schottky behavior is limited at a narrow rang of low potentials. At higher potentials, linear relationship between reciprocal capacitance and potential is obtained, which is ascribed to the increasing thickness of the passive film with potential. The donor density of the passive film is influenced by the formation potential of the film, passivator and microstructure. The decrease in …

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Electrochemical Behavior Of Aluminized Steel In Seawater Environment, Cheng-Hao Liang Nov 2004

Electrochemical Behavior Of Aluminized Steel In Seawater Environment, Cheng-Hao Liang

Journal of Electrochemistry

The electrochemical behavior of aluminized steel in seawater has been studied by immersion test and electrochemical technology. The results indicate that compared with 20# steel, the aluminized steel has lower corrosion potential and stronger anodic activity in seawater. Its anodic solution will occur at low potential. The immersion test shows that the corrosion rates of aluminized steel and 20# steel are 5.80 mg/dm~2 dand 3.36 mg/dm~2 d, respectively. Through the X-ray diffraction patternanalysis, it was found that chloride ions exit in the corrosion products of aluminized steel. It proves the participation of chloride ions in the process of corrosion, which …

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Preparation And Photo-Catalyst Properties Of The Α-Fe_2o_3-Tio_2 Films On Sodium Alginate Polymer, Li-Qin Chen, Huai-Zhen Zhong, Ri-Yao Chen, Xi Zheng, Zhen Chen Nov 2004

Preparation And Photo-Catalyst Properties Of The Α-Fe_2o_3-Tio_2 Films On Sodium Alginate Polymer, Li-Qin Chen, Huai-Zhen Zhong, Ri-Yao Chen, Xi Zheng, Zhen Chen

Journal of Electrochemistry

Three new nano thin films of α-Fe_2O_(3)、TiO_2 and α-Fe_2O_(3)-TiO_2 by doping their powder with sodium alginate polymer were prepared. Surface structure and catalytic activities of the films were characterized by FTIR、XRD、PL、TEM and I-V techniques. The results of UV-visible absorption showed that the methylene blue was mineralized in aqueous of α-Fe_2O_(3)/SA、TiO_2/SA and (α-(Fe_2O_(3)))-TiO_2 /SA upon radiation with ultra violet light. α-Fe_2O_(3) enhanced their photo-decolorized-activities by doping 15% TiO_2.

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Effect Of Fe~(3+) Dopen Of Titanium Dioxide Film On Absorption Spectra And Photo Catalysis, Mei-Qun Xiao, Jia-Nian Shen, Moucheng Li, Peng-Fei Wu, Dong Liu, Yu-Juan Zhang Nov 2004

Effect Of Fe~(3+) Dopen Of Titanium Dioxide Film On Absorption Spectra And Photo Catalysis, Mei-Qun Xiao, Jia-Nian Shen, Moucheng Li, Peng-Fei Wu, Dong Liu, Yu-Juan Zhang

Journal of Electrochemistry

Photo-catalytic titanium dioxide film in nano crystalline has been prepared by electrochemical oxidation process and adding different amount of ferric ion into the electrolyte during the anodic oxidation.The effects of Fe~(3+) dopen on absorption spectra and photo-catalytic of the titanium dioxide films have been studied. It shows that the Fe~(3+) dopen caused the red shife of the absorption edge for the incoming light and exhibited the improved photocatalytic reactivity.

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Studies On The Electrochemical Preparation And Electrochemical Properties Of Conducting Polymers——Brief Introduction To The Research Work Of Electrochemistry Of Conducting Polymers In Cas Key Laboratory Of Organic Solids(I), Yong-Fange Academy Of Sciences Li Nov 2004

Studies On The Electrochemical Preparation And Electrochemical Properties Of Conducting Polymers——Brief Introduction To The Research Work Of Electrochemistry Of Conducting Polymers In Cas Key Laboratory Of Organic Solids(I), Yong-Fange Academy Of Sciences Li

Journal of Electrochemistry

Conducting polymers have drawn much attention since the discovery of conducting polyacetylene in 1977, due to the novelty and curiosity of their structure and properties as well as their promising applications in many aspects. Among the studies of conducting polymers, the electrochemical preparation and electrochemical properties of conducting polymers are of special importance, because the electropolymerization is a main method for preparing conducting polymer films and the electrochemical properties are the basis for their applications in the fields of electrode materials for batteries, electrocatalysis, electrochromic display, etc. We are one of the earliest research groups in the world to perform …

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Investigation Of Pulse Potential-Modulated Coulometry For Co_2 Detection, Hai-Chuan Wang, Bing-Liang Wu Nov 2004

Investigation Of Pulse Potential-Modulated Coulometry For Co_2 Detection, Hai-Chuan Wang, Bing-Liang Wu

Journal of Electrochemistry

A pulse potential-modulated technique was applied to measure the concentration of CO_2 in gas samples. In the first step, an anodic pulse and a consequent cathodic pulse were used to remove the organic pollutant and surface oxide on the surface of the platinized Pt gauze electrode before each experiment. As following, a given potential step was used to reduce the CO_2 into adsorbed intermediate on Pt surface, and the adsorbates produced were oxidized by a following anodic potential step. At same time the oxidation current of adsorbates were measured. A certain relation exists between the concentration of CO_2 and the …

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Electrocatalytic Performances Of Carbon Nanotube Air Electrode For Oxygen Reduction, Feng-Ming Zhao, Chun-An Ma Nov 2004

Electrocatalytic Performances Of Carbon Nanotube Air Electrode For Oxygen Reduction, Feng-Ming Zhao, Chun-An Ma

Journal of Electrochemistry

The air electrodes with different mass ratio of Pt/active carbon or carbon nanotube as catalyst layer material have been prepared. The electrocatalytic performances for oxygen reduction were evaluated by means of polarization curve and electrochemical impedance spectroscopy (EIS). The results disclosed that carbon nanotubes dealt with nitric acid in the catalyst layer had been improved obviously on the electrocatalytic activity. After the surface of carbon nanotube was oxygenated and aggraded with platinum, the catalyst had obviously effects on the electrocatalytic activity. The air electrode with the mass ratio of active carbon to Pt/carbon nanotube in 4∶1 showed better electrocatalytic activity, …

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The Investigation Of Bafesi/C Alloy Composite As Anode Materials For Li-Ion Battery, Rui-Xiang Feng, Hua Dong, Xin-Ping Ai, Han-Xi Yang Nov 2004

The Investigation Of Bafesi/C Alloy Composite As Anode Materials For Li-Ion Battery, Rui-Xiang Feng, Hua Dong, Xin-Ping Ai, Han-Xi Yang

Journal of Electrochemistry

A novel BaFeSi/C composite was prepared by mechanical ball milling, and lithium insertion reactions on the composite electrode were investigated by cyclic voltammetry ,charge-discharge measurements, XRD and XPS spectroscopy. It is demonstrated that the capacity retention with indiscernible capacity decas during charge-discharge cycling. The improved cycling ability of the composite is suggested from a cooperative action by inactive FeSi_(2 )and BaSi_2 matrix and outer graphite shell, which both buffer the volumetric changes of the active Si phase and provide a good connection for electronic and ionic conduction during lithium insertion and extraction processes.

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Lico_(X)Ni_(1-X)O_2 Cathode Materials Prepared By Electrolysis Of Co And Ni, Jin-Ping Wei, Xin Sun, Xiao-Yu Wang, Xi-Kui Bian, Jin-Ling Zhai, Yan-Jie Yan-Jie Nov 2004

Lico_(X)Ni_(1-X)O_2 Cathode Materials Prepared By Electrolysis Of Co And Ni, Jin-Ping Wei, Xin Sun, Xiao-Yu Wang, Xi-Kui Bian, Jin-Ling Zhai, Yan-Jie Yan-Jie

Journal of Electrochemistry

A new electrolytic method was developed to prepare LiCo_(x)Ni_(1-x)O_2 as a cathode material of lithium-ion battery. Contrary to the traditional method, electrolytic method is a potential method with simple process to industrialization and no pollution. Metal cobalt and nickel were electrolysed in parallel to prepare the precursor of Co_( x )Ni_(1- x )(OH)_2.Different compositional precursors could be conveniently prepared by changing electrolytic current. The LiCo_(0.3)Ni_(0.7)O_2 cathode prepared by this method was found favorable charge-discharge and cycle properties. For the LiCo_(0.3)Ni_(0.7)O_(2 )cathode material, the discharge capacities in the 1st and 50th cycles were 163 mAh/g and 140 mAh/g with charge retention …

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Study On Mass Transport In Liquid Layer Adjacent To The Electrode Through Transmission Vop-Spectroellipsometry, Wei Zhu, Yangyu-Ru Yangyu-Ru, Zong-Qing Huang Nov 2004

Study On Mass Transport In Liquid Layer Adjacent To The Electrode Through Transmission Vop-Spectroellipsometry, Wei Zhu, Yangyu-Ru Yangyu-Ru, Zong-Qing Huang

Journal of Electrochemistry

In electrochemical system, the mass transport process in liquid layer adjacent to electrode is studied through theoretical analysis only.The diffusion process can be analyzed theoretically by Fick's law for homogeneous media. Up to now, none of satisfied experimental method has been reported for studying mass transport of a whole process in liquid media yet. This paper described the experimental approach to explore mass transport in electrochemical system by transmission Vop-spectroellipsometry briefly.

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Improvement And Its Mechanism Of Storage Performance Of Ni-Mh Battery, Xiao-Feng Li Nov 2004

Improvement And Its Mechanism Of Storage Performance Of Ni-Mh Battery, Xiao-Feng Li

Journal of Electrochemistry

The storage performance of nickel-metal-hydride (Ni-MH) battery was studied by using galvanostatic charge-discharge and cyclic voltammetry. The experimental results indicated that CoOOH could not be completely restored after its being thoroughly reduced at lower potential, which might weaken electric conduction network in the positive electrode and result in fading of electrochemical properties of Ni-MH battery. Addition of nickel powder as a conductive agent into the positive electrode was beneficial to the capacity recovery after storage.

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Anodic Dissolution Of Aluminum In Koh-Ethanol Solutions, Hai-Bo Shao, Jian-Ming Wang, Xiao-Yan Wang, Yi Zheng, Jian-Qing Zhang Nov 2004

Anodic Dissolution Of Aluminum In Koh-Ethanol Solutions, Hai-Bo Shao, Jian-Ming Wang, Xiao-Yan Wang, Yi Zheng, Jian-Qing Zhang

Journal of Electrochemistry

The feasibility of employing aluminum in KOH ethanol solution as a battery anode system was discussed. Weight loss measurement showed that the corrosion rate of Al is low enough to be used in sealed batteries. Through the measurements done by anodic polarization, EIS and galvanostatic discharge, it was found that A1 is electrochemical active in a wide potential range in this system, and its discharge mechanism is similar to that of A1 in aqueous solution. The discharge potential increased rapidly after a period of time, which might be caused by the discharge products depositing on the electrode surface.

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The Inhibition Synergistic Effect Between Imidazoline Derivative And Thiourea, Jing-Mao Zhao, He-Xia Liu, Wei Di, Yu Zuo Nov 2004

The Inhibition Synergistic Effect Between Imidazoline Derivative And Thiourea, Jing-Mao Zhao, He-Xia Liu, Wei Di, Yu Zuo

Journal of Electrochemistry

The inhibition synergistic effect between imidazoline and thiourea for carbon steel in CO_2 saturated brine solution was investigated by using weight-loss method, polarization curves measureament and XPS. The results showd that the inhibition efficiency increased significantly when imidazoline derivative was added as a corrosion inhibitor in the solution together with thiourea. The N and S atoms in the inhibitor film adsorbed on the surface of carbon steel, and N atoms predominated in the film near the solution and decreased gradually with the film depth and finally S atoms were the major element in the film near the matrix. It was …

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The Electrochemical Performance Of Modified Spinel At Elevated Temperature, Zhen-Ping Cai, Xiao-Hong Chen, Shi-Gang Lu, Ming-Xun Li, Wei-Hua Jin Nov 2004

The Electrochemical Performance Of Modified Spinel At Elevated Temperature, Zhen-Ping Cai, Xiao-Hong Chen, Shi-Gang Lu, Ming-Xun Li, Wei-Hua Jin

Journal of Electrochemistry

The modified LiMn_2O_4 cathode materials for lithium ion batteries have been synthesized by solid-state reaction. The crystal structure and electrochemical performance of products have been investigated by SEM、XRD and electrochemical measurements. The XRD analysis indicated that all the synthesized products possess Fd3m spinel LiMn_2O_4 structure. Those modified LiMn_2O_4 materials showed improved cycling capacity over pure spinels at high temperature and room temperature.

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Preparation And Electrochemical Magnesium Insertion Behaviors Of Mgv_2o_6, Hua-Tang Yuan, Li-Fang Jiao, Jian-Sheng Cao, Xiu-Sheng Liu, Ming Zhao, Yong-Mei Wang Nov 2004

Preparation And Electrochemical Magnesium Insertion Behaviors Of Mgv_2o_6, Hua-Tang Yuan, Li-Fang Jiao, Jian-Sheng Cao, Xiu-Sheng Liu, Ming Zhao, Yong-Mei Wang

Journal of Electrochemistry

MgV_2O_6was synthesized by conventional solid-state reaction from MgO and V_2O_(5)as starting materials. X-Ray diffraction analysis showed that the prepared sample belongs to the monoclinic structure. Electrochemical magnesium insertion from aprotic electrolytes such as organomagnesium halides into this host was found possible and exhibited charge/discharge circulation.

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Applications Of New Activated Carbon Meterials In The Electric Double-Layer Capacitor, Jian-Jun Zhang Nov 2004

Applications Of New Activated Carbon Meterials In The Electric Double-Layer Capacitor, Jian-Jun Zhang

Journal of Electrochemistry

A new type activated carbon whose precursor was coconut shell could be obtained using specific physics-chemistry activation, and the activated carbon was applied as the material of electrode in EDLC(electrical double-layer capacitor),which had a large specific capacitance,and could charge and discharged in some large currents. Carbon dioxide and acid were used to modify carbon,and the effects of post-treatment on surface area and pore volume were investigated. A moulding method which has influence on some properties of carbon electrode with PTFE additive was researched in the paper.

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Assessing Treatment Effects In Randomized Longitudinal Two-Group Designs With Missing Observations, James Algina, H. J. Keselman Nov 2004

Assessing Treatment Effects In Randomized Longitudinal Two-Group Designs With Missing Observations, James Algina, H. J. Keselman

Journal of Modern Applied Statistical Methods

SAS’s PROC MIXED can be problematic when analyzing data from randomized longitudinal two-group designs when observations are missing over time. Overall (1996, 1999) and colleagues found a number of procedures that are effective in controlling the number of false positives (Type I errors) and are yet sensitive (powerful) to detect treatment effects. Two favorable methods incorporate time in study and baseline scores to model the missing data mechanism; one method was a single-stage PROC MIXED ANCOVA solution and the other was a two-stage endpoint analysis using the change scores as dependent scores. Because the twostage approach can lack sensitivity to …

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An Overview Of The Respondent-Generated Intervals (Rgi) Approach To Sample Surveys, S. James Press, Judith M. Tanur Nov 2004

An Overview Of The Respondent-Generated Intervals (Rgi) Approach To Sample Surveys, S. James Press, Judith M. Tanur

Journal of Modern Applied Statistical Methods

This article brings together many years of research on the Respondent-Generated Intervals (RGI) approach to recall in factual sample surveys. Additionally presented is new research on the use of RGI in opinion surveys and the use of RGI with gamma-distributed data. The research combines Bayesian hierarchical modeling with various cognitive aspects of sample surveys.

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Multivariate Contrasts For Repeated Measures Designs Under Assumption Violations, Lisa M. Lix, Aynslie M. Hinds Nov 2004

Multivariate Contrasts For Repeated Measures Designs Under Assumption Violations, Lisa M. Lix, Aynslie M. Hinds

Journal of Modern Applied Statistical Methods

Conventional and approximate degrees of freedom procedures for testing multivariate interaction contrasts in groups by trials repeated measures designs were compared under assumption violation conditions. Procedures were based on either least-squares or robust estimators. Power generally favored test procedures based on robust estimators for non-normal distributions, but was influenced by the degree of departure from non-normality, definition of power, and magnitude of the multivariate effect size.

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Modeling Incomplete Longitudinal Data, Hakan Demirtas Nov 2004

Modeling Incomplete Longitudinal Data, Hakan Demirtas

Journal of Modern Applied Statistical Methods

This article presents a review of popular parametric, semiparametric and ad-hoc approaches for analyzing incomplete longitudinal data.

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Variance Stabilizing Power Transformation For Time Series, Victor M. Guerrero, Rafael Perera Nov 2004

Variance Stabilizing Power Transformation For Time Series, Victor M. Guerrero, Rafael Perera

Journal of Modern Applied Statistical Methods

A confidence interval was derived for the index of a power transformation that stabilizes the variance of a time-series. The process starts from a model-independent procedure that minimizes a coefficient of variation to yield a point estimate of the transformation index. The confidence coefficient of the interval is calibrated through a simulation.

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Size And Power Of The Reset Test As Applied To Systems Of Equations: A Bootstrap Approach, Ghazi Shukur, Panagiotis Mantalos Nov 2004

Size And Power Of The Reset Test As Applied To Systems Of Equations: A Bootstrap Approach, Ghazi Shukur, Panagiotis Mantalos

Journal of Modern Applied Statistical Methods

The size and power of various generalization of the RESET test for functional misspecification are investigated, using the “Bootsrap critical values”, in systems ranging from one to ten equations. The properties of 8 versions of the test are studied using Monte Carlo methods. The results are then compared with another study of Shukur and Edgerton (2002), in which they used the asymptotic critical values instead and found that in general only one version of the tests works well regarding size properties. In our study, when applying the bootstrap critical values, we find that all the tests exhibits correct size even …

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Type I Error Rates For A One Factor Within-Subjects Design With Missing Values, Miguel A. Padilla, James Algina Nov 2004

Type I Error Rates For A One Factor Within-Subjects Design With Missing Values, Miguel A. Padilla, James Algina

Journal of Modern Applied Statistical Methods

Missing data are a common problem in educational research. A promising technique, that can be implemented in SAS PROC MIXED and is therefore widely available, is to use maximum likelihood to estimate model parameters and base hypothesis tests on these estimates. However, it is not clear which test statistic in PROC MIXED performs better with missing data. The performance of the Hotelling- Lawley-McKeon and Kenward-Roger omnibus test statistics on the means for a single factor withinsubject ANOVA are compared. The results indicate that the Kenward-Roger statistic performed better in terms of keeping the Type I error close to the nominal …

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Interval Estimation For The Scale Parameter Of Burr Type X Distribution Based On Grouped Data, Amjad D. Al-Nasser, Ayman Baklizi Nov 2004

Interval Estimation For The Scale Parameter Of Burr Type X Distribution Based On Grouped Data, Amjad D. Al-Nasser, Ayman Baklizi

Journal of Modern Applied Statistical Methods

The application of some bootstrap type intervals for the scale parameter of the Burr type X distribution with grouped data is proposed. The general asymptotic confidence interval procedure (Chen & Mi, 2001) is studied. The performance of these intervals is investigated and compared. Some of the bootstrap intervals give better performance for situations of small sample size and heavy censoring.

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Pseudo-Random Number Generation In R For Commonly Used Multivariate Distributions, Hakan Demirtas Nov 2004

Pseudo-Random Number Generation In R For Commonly Used Multivariate Distributions, Hakan Demirtas

Journal of Modern Applied Statistical Methods

An increasing number of practitioners and applied statisticians have started using the R programming system in recent years for their computing and data analysis needs. As far as pseudo-random number generation is concerned, the built-in generator in R does not contain multivariate distributions. In this article, R routines for widely used multivariate distributions are presented.

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An Algorithm And Code For Computing Exact Critical Values For The Kruskal-Wallis Nonparametric One-Way Anova, Sikha Bagui, Subhash Bagui Nov 2004

An Algorithm And Code For Computing Exact Critical Values For The Kruskal-Wallis Nonparametric One-Way Anova, Sikha Bagui, Subhash Bagui

Journal of Modern Applied Statistical Methods

In this article, an algorithm and code to compute exact critical values (or percentiles) for Kruskal-Wallis test on k independent treatment populations with equal or unequal sample sizes using Visual Basic (VB.NET) is provided. This program has the ability to calculate critical values for any k , sample sizes (ni ) , and significance level (α ) . An exact critical value table for k = 4 is also developed. The table will be useful to practitioners since it is not available in standard nonparametric statistics texts. The program can also be used to compute any other …

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Aligned Rank Tests As Robust Alternatives For Testing Interactions In Multiple Group Repeated Measures Designs With Heterogeneous Covariances, Xiaosheng Lei, Janet K. Holt, T. Mark Beasley Nov 2004

Aligned Rank Tests As Robust Alternatives For Testing Interactions In Multiple Group Repeated Measures Designs With Heterogeneous Covariances, Xiaosheng Lei, Janet K. Holt, T. Mark Beasley

Journal of Modern Applied Statistical Methods

Data simulation was used to investigate whether tests performed on aligned ranks (Beasley, 2002) could be used as robust alternatives to parametric methods for testing a split-plot interaction with non-normal data and heterogeneous covariance matrices. Results indicated the aligned rank method do not have any distinct advantage over parametric methods in this situation.

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Multivariate And Multistrata Nonparametric Tests: The Nonparametric Combination Method, Livio Corain, Luigi Salmaso Nov 2004

Multivariate And Multistrata Nonparametric Tests: The Nonparametric Combination Method, Livio Corain, Luigi Salmaso

Journal of Modern Applied Statistical Methods

Researchers and practitioners in many scientific disciplines and industrial fields are often faced with complex problems when dealing with comparisons between two or more groups using classical parametric methods. The data arising from real problems rarely are in agreement with stringent parametric assumptions. The NonParametric Combination (NPC) methodology frees the researcher from stringent assumptions of parametric methods and allows a more flexible analysis, both in terms of specification of multivariate hypotheses and in terms of the nature of the variables involved in the analysis. An outline of NPC methodology is given, along with case studies.

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