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Materials Science and Engineering

University of Central Florida

Theses/Dissertations

2004

Nanocomposites

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Processing, Microstructural And Mechanical Characterization Of Mechanically Alloyed Al-Al2o3 Nanocomposites, Pushkar Katiyar Jan 2004

Processing, Microstructural And Mechanical Characterization Of Mechanically Alloyed Al-Al2o3 Nanocomposites, Pushkar Katiyar

Electronic Theses and Dissertations

Aluminum-alumina nanocomposites were synthesized using mechanical alloying of blended component powders of pure constituents. This study was performed on various powder mixtures with aluminum as the matrix and alumina as the reinforcement with volume fractions of 20, 30, and 50 % and Al2O3 particle sizes of 50 nm, 150 nm, and 5 µm. X-ray diffraction (XRD) and scanning electron microscopy (SEM) techniques were used for the crystal structure and microstructural characterization of the powders at different stages of milling. Al2O3 powders with 50 nm and 150 nm particle size were predominantly of γ-type, while Al2O3 of 5 µm size was …