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Effect Of Sintering On Microstructure And Properties Of Hydroxyapatite Produced By Different Synthesizing Methods, N Monmaturapoj, C Yatongchai
Effect Of Sintering On Microstructure And Properties Of Hydroxyapatite Produced By Different Synthesizing Methods, N Monmaturapoj, C Yatongchai
Journal of Metals, Materials and Minerals
The aim of this study is to investigate the effect of the sintering schedule on microstructure and properties of hydroxyapatite which is produced by different synthesizing methods. Hence, wet-chemical precipitation and solid-state reaction were performed to prepare nano-sized hydroxyapatite (HA) powders. Powders were then uniaxially pressed and sintered by varying temperatures and times. XRD and SEM were used to identify phases and morphology. Density and porosity of the sintered sample were determined using the Archimedes technique. Flexural strength was measured by a universal testing machine. The results show that density and strength could be improved by increasing the sintering temperature …
Optimizing The Mechanical Properties Of Partially Yttria Stabilized Zirconia With Alumina Additions, Ramanaganapathy Kandaswamy
Optimizing The Mechanical Properties Of Partially Yttria Stabilized Zirconia With Alumina Additions, Ramanaganapathy Kandaswamy
All Theses
Zirconia is one of the extensively studied solid oxide ceramics with respect to its use in various industrial applications like electrolyte in fuel cells, sensors, refractories and exhaust chamber in automobile industry. It can be found from the literature 1-4 that are contradictory results on the mechanical properties when alumina is added. There are several factors like microstructure, phase composition and method of processing that affects the mechanical properties of the material. The focus of this research is to examine how hardness, tensile strength and other properties varies with alumina content and deduce the optimal amount of alumina that is …
Freeze Extrusion Fabrication Of 13-93 Bioactive Glass Scaffolds For Bone Repair, Tieshu Huang, Nikhil D. Doiphode, M. N. Rahaman, Ming-Chuan Leu, B. Sonny Bal, D. E. Day
Freeze Extrusion Fabrication Of 13-93 Bioactive Glass Scaffolds For Bone Repair, Tieshu Huang, Nikhil D. Doiphode, M. N. Rahaman, Ming-Chuan Leu, B. Sonny Bal, D. E. Day
Materials Science and Engineering Faculty Research & Creative Works
There is an increasing demand for synthetic scaffolds with the requisite biocompatibility, internal architecture, and mechanical properties for the bone repair and regeneration. In this work, scaffolds of a silicate bioactive glass (13-93) were prepared by a freeze extrusion fabrication (FEF) method and evaluated in vitro for potential applications in bone repair and regeneration. The process parameters for FEF production of scaffolds with the requisite microstructural characteristics, as well as the mechanical and cell culture response of the scaffolds were evaluated. After binder burnout and sintering (60 min at 700°C), the scaffolds consisted of a dense glass network with interpenetrating …
Performance Of Nevada’S Aggregates In Alkali-Aggregate Reactivity Of Portland Cement Concrete, Mohammad Shahidul Islam
Performance Of Nevada’S Aggregates In Alkali-Aggregate Reactivity Of Portland Cement Concrete, Mohammad Shahidul Islam
UNLV Theses, Dissertations, Professional Papers, and Capstones
Alkali-aggregate reaction (AAR) is a form of distress that occurs in concrete and results in serviceability problems, cracks, spalling, and other deterioration mechanisms. There are two categories of AAR, namely, alkali-silica reaction (ASR) and alkali-carbonate reaction (ACR). Alkali-silica reaction is one of the most recognized deleterious phenomena in concrete, and has been a major concern since its discovery in the 1940s. The reaction which occurs between reactive silica or silicates present in some aggregates and alkalis of Portland cement produces an alkali-silica gel that expands in the presence of moisture resulting in concrete cracks. ACR is also a chemical reaction …