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Application Of Accuracy And Precision Evaluations Based On The Current United States And Indonesian Pharmacopoeias: A Critical Review, Gunawan Indrayanto

Makara Journal of Science

New methods for the evaluation of accuracy and precision are mentioned in the latest edition of the United States Pharmacopoeia (USP), whereas other validation parameters, that is, selectivity, linearity, range, and robustness, remained relatively unchanged. In obtaining reliable data from any chemical/pharmaceutical analysis, the analytical procedure must be validated or verified in accordance with the latest edition of the pharmacopoeia. Some review articles on the general validation methods have been published by the author. This present review will focus on the implementation and discussion of the accuracy and precision evaluation based on the current USP and Indonesian pharmacopoeia. Some examples …

Variation Sources Analysis And Monitoring Of Measurement System Of Food Packaging Paper Based On Hs Gc/Ms, Zhao Hai-Juan, Li Wen-Wei, Wagn Hui, Du Shan-Tao, Wang Hai-Yu, Li Chun-Yang

Food and Machinery

Objective: To improve the accuracy and validity of the measurement data of solvent residues in food packaging paper. Methods: Taking the HS GC-MS measurement system as the research object, variation sources in the measurement process was separated by using the measurement system analysis, and the traditional control chart and EWMA control chart of repeatability and reproducibility were established respectively to effectively monitor the detection error of the measurement system. Results: ① HS GC/MS had high measurement accuracy, with GRR of about 9.76%, and the gauging ability of the measurement system was relatively good. ② Through the combination …

Freely Chosen Cadence Is Increased During Repeated Bouts Of Submaximal Ergometer Pedalling, Andreas Schmidt, Jonas G. Madsen, Magnus K. Hyttel, Ernst A. Hansen

International Journal of Exercise Science

International Journal of Exercise Science 15(1): 1142-1155, 2022. It was investigated whether the phenomenon of repeated bout rate enhancement occurs during submaximal ergometer cycling. Repeated bout rate enhancement is defined as an increase of the freely, or spontaneously, chosen cadence during repeated bouts of pedalling and has previously been reported for finger tapping. This is relevant to study since cadence can affect biomechanical and physiological responses. Recreationally active individuals (n=27) performed five consecutive 5-min bouts of cycling at 100 W using freely chosen cadence. All bouts were separated by 10-min rest. Cadence, pedal force profile characteristics, heart rate, …

Long-Term Winter-Site Fidelity In Song Sparrows (Melospiza Melodia), Tosha R. Kelly, Keith A. Hobson, Garth @. Casbourn, Elizabeth A. Macdougall-Shackleton, Scott A. Macdougall-Shackleton

Biology Publications

In migratory animals, the degree to which individuals return to the same wintering sites across multiple years can affect fitness and population dynamics, and thus has important implications for conservation. Despite this, long-term evaluations of wintering-site fidelity are rare for migratory birds: many populations are intensively studied on their breeding grounds but tracking the migratory movements of small birds once they leave the breeding grounds is challenging. To evaluate patterns of overwintering location and fidelity, we collected winter-grown claw tissue from 301 Song Sparrows (Melospiza melodia; 449 samples) captured in spring at their breeding grounds over six consecutive …

Irreproducibility In Searches Of Scientific Literature: A Comparative Analysis, Gábor Pozsgai, Gábor L. Lövei, Liette Vasseur, Geoff Gurr, Péter Batáry, János Korponai, Nick A. Littlewood, Jian Liu, Arnold Móra, John J. Obrycki, Olivia Reynolds, Jenni A. Stockan, Heather Vanvolkenburg, Jie Zhang, Wenwu Zhou, Minsheng You

Entomology Faculty Publications

1. Repeatability is the cornerstone of science, and it is particularly important for systematic reviews. However, little is known on how researchers’ choice of database, and search platform influence the repeatability of systematic reviews. Here, we aim to unveil how the computer environment and the location where the search was initiated from influence hit results.
2. We present a comparative analysis of time-synchronized searches at different institutional locations in the world and evaluate the consistency of hits obtained within each of the search terms using different search platforms.
3. We revealed a large variation among search platforms and showed that PubMed and Scopus …

A Migratory Sparrow Has Personality In Winter That Is Independent Of Other Traits, Theadora A. Block, Rachel Star, Daizaburo Shizuka, Alexis S. Chaine, Bruce E. Lyon

Papers in Behavior in Biological Sciences

Small birds in winter face trade-offs between predation risk and foraging, and alternate life-history strategies may arise from these trade-offs. Animal personality shows similarities with alternative life-history strategies, and using a life-history context to understand personality can provide valuable insights. Golden-crowned sparrows, Zonotrichia atricapilla, a small migratory bird, have a complex winter social system with high site-fidelity, long-term social associations between individuals and competition mediated by badges of status. We asked whether golden-crowned sparrows show personalities during winter, whether these personalities were consistent over 3 years and whether they correlated with social and morphological traits. We found that …

Most Published Selection Gradients Are Underestimated: Why This Is And How To Fix It, Niels Jeroen Dingemanse, Yimen G. Araya-Ajoy, David F. Westneat

Biology Faculty Publications

Ecologists and evolutionary biologists routinely estimate selection gradients. Most researchers seek to quantify selection on individual phenotypes, regardless of whether fixed or repeatedly expressed traits are studied. Selection gradients estimated to address such questions are attenuated unless analyses account for measurement error and biological sources of within-individual variation. Estimates of standardized selection gradients published in Evolution between 2010 and 2019 were primarily based on traits measured once (59% of 325 estimates). We show that those are attenuated: bias increases with decreasing repeatability but differently for linear versus nonlinear gradients. Others derived individual-mean trait values prior to analyses (41%), typically using …

Repeatability Of Foraging Behavior Following A Simulated Predation Attempt Depends On Color Morph, Sex, And Foraging Metric In Red-Backed Salamanders (Plethodon Cinereus), Brian P. Waldron*, Marissa C. Ganzfried*, Cari-Ann M. Hickerson, Carl D. Anthony

2021 Faculty Bibliography

Behavioral repeatability greatly affects the capacity of an individual to respond to varying environments. When multiple behaviors within individuals are repeatable and correlated across time or across contexts, it is termed a behavioral syndrome. However, not all behaviors exhibit the same level of repeatability, and relatively few studies have examined repeatability in amphibians. We examined the repeatability of foraging behavior in the Eastern Red-backed salamander (Plethodon cinereus), a color-polymorphic terrestrial salamander, following a simulated predation attempt. We tested several hypotheses: (1) Simulated predation would negatively affect foraging, increasing latency to feed and decreasing the number of prey items eaten in …

Character Displacement In The Midst Of Substantial Background Evolution In Anolis Lizard Island Populations, Ambika Kamath, Nicholas C. Herrmann, Kiyoko M. Gotanda, Kum C. Shim, Jacob Lafond, Gannon Cottone, Heather Falkner, Todd S. Campbell, Yoel E. Stuart

Biology: Faculty Publications and Other Works

Negative interactions between species can generate divergent selection that causes character displacement. However, other processes cause similar divergence. We use spatial and temporal replication across island populations of Anolis lizards to assess the importance of negative interactions in driving trait shifts. Previous work showed that the establishment of Anolis sagrei on islands drove resident Anolis carolinensis to perch higher and evolve larger toepads. To further test the interaction's causality and predictability, we resurveyed a subset of islands nine years later. Anolis sagrei had established on one island between surveys. We found that A. carolinensis on this island now perch higher …

Large Variability In Feeding Behavior Among Crossbred Growing Cattle, David N. Kelly, Roy D. Sleator, Craig P. Murphy, Stephen B. Conroy, Michelle M. Judge, Donagh P. Berry

Department of Biological Sciences Publications

The purpose of this study was to define an extensive suite of feeding behavior traits in growing crossbred cattle and to investigate their phenotypic inter-relationships as well as relationships with other performance and efficiency traits. Time-series feeding behavior data, as well as feed intake and liveweight records, were available for 624 growing crossbred cattle, of which 445 were steers and 179 were heifers. Feeding behavior repeatability estimates were calculated using linear mixed models. Additionally, partial Spearman correlations were estimated among 14 feeding behavior traits, as well as between feeding behavior with both performance and feed efficiency traits, using residuals retained …

Lamb Wool Shedding Is A Good Predictor Of Ewe Wool Shedding, Napoleón Vargas Jurado, Larry Kuehn, Ronald M. Lewis

Department of Animal Science: Faculty Publications

Interest in reducing labour costs due to shearing has led to development of breed types that shed their wool naturally. Selection at young ages can facilitate response. Reliability of predictions of adult from lamb wool shedding (WS) is thus key in the design of breeding programmes to increase shedding. Our objectives were to estimate heritabilities and genetic relationships between WS measured once in lambs and repeatedly in ewes and to assess the accuracy of lamb WS EBV to predict ewe WS EBV based on a multi‐trait threshold or a repeatability model. Data were 4,971 lamb and 3,335 ewe WS records …

Acclimation, Long-Term Repeatability, And Phenotypic Correlations Of Aerobic Metabolic Traits In The Gulf Killifish, Fundulus Grandis, Jessica E. Reemeyer

University of New Orleans Theses and Dissertations

This research examined the effects of acclimation to lowered salinity, elevated temperature, and hypoxia on aerobic metabolism of the Gulf killifish, Fundulus grandis, a common estuarine resident of the Gulf of Mexico. Standard metabolic rate (SMR), maximum metabolic rate (MMR), absolute aerobic scope (AAS), and critical oxygen tension (P_crit) were each influenced by one or more acclimation treatments. Assessing the consistency of these traits measured in the same individuals over time, all were found to be significantly repeatable with no indication that the repeatability of any traits was affected by acclimation conditions. Significant correlations were found between …

Sensitive And Reliable Measures Of Driver Performance In Simulated Motor-Racing, Christopher Irwin, Jamie Mollica, Ben Desbrow

International Journal of Exercise Science

International Journal of Exercise Science 12(6): 971-978, 2019. Motor racing is a physically and mentally demanding sport, associated with a high degree of risk for drivers. Hence, driving simulation provides a safe alternative to explore the impact acute physiological perturbations (e.g. heat stress or dehydration) on a driver’s performance. This study aimed to determine sensitive and reliable simulated driving performance parameters that could be employed in future driving performance studies. Thirty-six healthy males (age: 26.5 ± 8.1 y, body mass: 75.6 ± 12.2 kg, mean ± SD) completed a single experimental trial involving four simulated motor-racing drives (2 initial drives …

Fifty Years Of Cave Arthropod Sampling: Techniques And Best Practices, J. Judson Wynne, Francis G. Howarth, Stefan Sommer, Brett G. Dickson

International Journal of Speleology

Ever-increasing human pressures on cave biodiversity have amplified the need for systematic, repeatable, and intensive surveys of cave-dwelling arthropods to formulate evidence-based management decisions. We examined 110 papers (from 1967 to 2018) to: (i) understand how cave-dwelling invertebrates have been sampled; (ii) provide a summary of techniques most commonly applied and appropriateness of these techniques, and; (iii) make recommendations for sampling design improvement. Of the studies reviewed, over half (56) were biological inventories, 43 ecologically focused, seven were techniques papers, and four were conservation studies. Nearly one-half (48) of the papers applied systematic techniques. Few papers (24) provided enough information …

Parental Habituation To Human Disturbance Over Time Reduces Fear Of Humans In Coyote Offspring, Christopher J. Schell, Julie K. Young, Elizabeth V. Lonsdorf, Rachel M. Santymire, Jill M. Mateo

Wildland Resources Faculty Publications

A fundamental tenet of maternal effects assumes that maternal variance over time should have discordant consequences for offspring traits across litters. Yet, seldom are parents observed across multiple reproductive bouts, with few studies consider‐ ing anthropogenic disturbances as an ecological driver of maternal effects. We ob‐ served captive coyote (Canis latrans) pairs over two successive litters to determine whether among‐litter differences in behavior (i.e., risk‐taking) and hormones (i.e., cortisol and testosterone) corresponded with parental plasticity in habituation. Thus, we explicitly test the hypothesis that accumulating experiences of anthropogenic disturbance reduces parental fear across reproductive bouts, which should have disparate phenotypic …

It Takes Two: Evidence For Reduced Sexual Conflict Over Parental Care In A Biparental Canid, Christopher J. Schell, Julie K. Young, Elizabeth V. Lonsdorf, Jill M. Mateo, Rachel M. Santymire

USDA Wildlife Services: Staff Publications

In biparental systems, sexual conflict over parental investment predicts that the parent providing care experiences greater reproductive costs. This inequality in parental contribution is reduced when offspring survival is dependent on biparental care. However, this idea has received little empirical attention. Here, we determined whether mothers and fathers differed in their contribution to care in a captive population of coyotes (Canis latrans). We performed parental care assays on 8 (n = 8 males, 8 females) mated pairs repeatedly over a 10-week period (i.e., 5–15 weeks of litter age) when pairs were first-time breeders (2011), and again as experienced …

Consistent Individual Behavior: Evidence Of Personality In Black Bears, Patrick J. Myers, Julie K. Young

USDA Wildlife Services: Staff Publications

Personality is defined as consistency in individual differences in organismal behavior across time or context, a phenomenon of interest within behavioral and evolutionary ecology. Empirical data have revealed an ever-increasing number and diversity of taxa that display these phenotypic patterns in both wild and captive settings. Moreover, these behavioral traits are frequently linked to wild behavior, life history strategies, and measures of individual fitness. Understanding personality is of particular importance for some animals, such as large carnivores, which may express maladaptive behavior that can lead to conflict with humans. To date, few studies of personality exist on large carnivores and …

Parental Habituation To Human Disturbance Over Time Reduces Fear Of Humans In Coyote Offspring, Christopher J. Schell, Julie K. Young, Elizabeth V. Lonsdorf, Rachel M. Santymire, Jill M. Mateo

USDA Wildlife Services: Staff Publications

A fundamental tenet of maternal effects assumes that maternal variance over time should have discordant consequences for offspring traits across litters. Yet, seldom are parents observed across multiple reproductive bouts, with few studies considering anthropogenic disturbances as an ecological driver of maternal effects. We observed captive coyote (Canis latrans) pairs over two successive litters to determine whether among‐litter differences in behavior (i.e., risk‐taking) and hormones (i.e., cortisol and testosterone) corresponded with parental plasticity in habituation. Thus, we explicitly test the hypothesis that accumulating experiences of anthropogenic disturbance reduces parental fear across reproductive bouts, which should have disparate phenotypic …

Individual Variation In Avian Avoidance Behaviours In Response To Repeated, Simulated Vehicle Approach, Travis L. Devault, T. W. Seamans, B. F. Blackwell, S. L. Lima, E. Fernandez-Juricic

USDA Wildlife Services: Staff Publications

Birds exhibit variation in alert and flight behaviours in response to vehicles within and between species, but it is unclear how properties inherent to individuals influence variation in avoidance responses over time. We examined individual variation in avoidance behaviours of Brown-headed Cowbirds (Molothrus ater (Boddaert, 1783)) in response to repeated presentation of a simulated vehicle approach in a video playback scenario. Wemodeled temporal alert and flight behaviours to determine whether overall behavioural variation resulted primarily from variation within individuals (i.e., intraindividual variation) or between individuals (i.e., interindividual variation). We examined reaction norms (individual × treatment day) and whether birds …

Employing Individual Measures Of Baseline Glucocorticoids As Population-Level Conservation Biomarkers: Considering Within-Individual Variation In A Breeding Passerine, Christine L. Madliger, Oliver P. Love

Great Lakes Institute for Environmental Research Publications

Labile physiological variables, such as stress hormones [i.e. glucocorticoids (GCs)], allow individuals to react to perturbations in their environment and may therefore reflect the effect of disturbances or positive conservation initiatives in advance of population-level demographic measures. Although the application of GCs as conservation biomarkers has been of extensive interest, few studies have explicitly investigated whether baseline GC concentrations respond to disturbances consistently across individuals. However, confirmation of consistent responses is of paramount importance to assessing the ease of use of GCs in natural systems and to making valid interpretations regarding population-level change (or lack of change) in GC concentrations. …

Temporal Overlap And Repeatability Of Feather Corticosterone Levels: Practical Considerations For Use As A Biomarker, Christopher M. Harris, Christine L. Madliger, Oliver P. Love

Great Lakes Institute for Environmental Research Publications

The measurement of corticosterone (CORT) levels in feathers has recently become an appealing tool for the conservation toolbox, potentially providing a non-invasive, integrated measure of stress activity throughout the time of feather growth. However, because the mechanism of CORT deposition, storage and stability in feathers is not fully understood, it is unclear how reliable this measure may be, especially when there is an extended interval between growth and feather collection. We compared CORT levels of naturally grown feathers from tree swallows (Tachycineta bicolor) that were moulted and regrown concurrently and therefore expected to have similar CORT levels. Specifically, we compared …

Employing Individual Measures Of Baseline Glucocorticoids As Population-Level Conservation Biomarkers: Considering Within-Individual Variation In A Breeding Passerine, Christine L. Madliger, Oliver P. Love

Integrative Biology Publications

Labile physiological variables, such as stress hormones [i.e. glucocorticoids (GCs)], allow individuals to react to perturbations in their environment and may therefore reflect the effect of disturbances or positive conservation initiatives in advance of population-level demographic measures. Although the application of GCs as conservation biomarkers has been of extensive interest, few studies have explicitly investigated whether baseline GC concentrations respond to disturbances consistently across individuals. However, confirmation of consistent responses is of paramount importance to assessing the ease of use of GCs in natural systems and to making valid interpretations regarding population-level change (or lack of change) in GC concentrations. …

Olfactory Attractants And Parity Affect Prenatal Androgens And Territoriality Of Coyote Breeding Pairs, Christopher J. Schell, Julie K. Young, Elizabeth V. Lonsdorf, Jill M. Mateo, Rachel M. Santymire

USDA Wildlife Services: Staff Publications

Hormones are fundamental mediators of personality traits intimately linked with reproductive success. Hence, alterations to endocrine factors may dramatically affect individual behavior that has subsequent fitness consequences. Yet it is unclear how hormonal or behavioral traits change with environmental stressors or over multiple reproductive opportunities, particularly for biparental fauna. To simulate an environmental stressor, we exposed captive coyote (Canis latrans) pairs to novel coyote odor attractants (i.e. commercial scent lures) midgestation to influence territorial behaviors, fecal glucocorticoid (FGMs) and fecal androgen metabolites (FAMs). In addition, we observed coyote pairs as first-time and experienced breeders to assess the influence …

Temporal Overlap And Repeatability Of Feather Corticosterone Levels: Practical Considerations For Use As A Biomarker, Christopher M. Harris, Christine L. Madliger, Oliver P. Love

Integrative Biology Publications

The measurement of corticosterone (CORT) levels in feathers has recently become an appealing tool for the conservation toolbox, potentially providing a non-invasive, integrated measure of stress activity throughout the time of feather growth. However, because the mechanism of CORT deposition, storage and stability in feathers is not fully understood, it is unclear how reliable this measure may be, especially when there is an extended interval between growth and feather collection. We compared CORT levels of naturally grown feathers from tree swallows (Tachycineta bicolor) that were moulted and regrown concurrently and therefore expected to have similar CORT levels. Specifically, we compared …

Animal Personality As A Cause And Consequence Of Contest Behaviour, Mark Briffa, Lynne U. Sneddon, Alistair J. Wilson

Lynne Sneddon, PhD

We review the evidence for a link between consistent among-individual variation in behaviour (animal personality) and the ability to win contests over limited resources. Explorative and bold behaviours often covary with contest behaviour and outcome, although there is evidence that the structure of these ‘behavioural syndromes’ can change across situations. Aggression itself is typically repeatable, but also subject to high within-individual variation as a consequence of plastic responses to previous fight outcomes and opponent traits. Common proximate mechanisms (gene expression, endocrine control and metabolic rates) may underpin variation in both contest behaviour and general personality traits. Given the theoretical links …

Animal Personality As A Cause And Consequence Of Contest Behaviour, Mark Briffa, Lynne U. Sneddon, Alistair J. Wilson

Sentience Collection

We review the evidence for a link between consistent among-individual variation in behaviour (animal personality) and the ability to win contests over limited resources. Explorative and bold behaviours often covary with contest behaviour and outcome, although there is evidence that the structure of these ‘behavioural syndromes’ can change across situations. Aggression itself is typically repeatable, but also subject to high within-individual variation as a consequence of plastic responses to previous fight outcomes and opponent traits. Common proximate mechanisms (gene expression, endocrine control and metabolic rates) may underpin variation in both contest behaviour and general personality traits. Given the theoretical links …

Computerized Dietary Assessments Compare Well With Interviewer Administered Diet Histories For Patients With Type 2 Diabetes Mellitus In The Primary Healthcare Setting, Y. C. Probst, S. Faraji, M. Batterham, D. G. Steel, Linda C. Tapsell

Dr Marijka Batterham

Using a context-based case-control trial, 41 adults with type 2 diabetes mellitus were randomized into four groups to complete dietary assessments (computerized or interviewer administered) at 0, 2 and 8 weeks and food records at 0 and 2 weeks. Repeatability of reported energy, total fat, saturated, polyunsaturated and monounsaturated fatty acids between the computerized and interviewer administered methods were assessed using repeated measures ANOVA. Paired t-tests and Pearson's correlations determined relative validity of the assessments.

Computerized Dietary Assessments Compare Well With Interviewer Administered Diet Histories For Patients With Type 2 Diabetes Mellitus In The Primary Healthcare Setting, Y. C. Probst, S. Faraji, M. Batterham, D. G. Steel, Linda C. Tapsell

L. C. Tapsell

Using a context-based case-control trial, 41 adults with type 2 diabetes mellitus were randomized into four groups to complete dietary assessments (computerized or interviewer administered) at 0, 2 and 8 weeks and food records at 0 and 2 weeks. Repeatability of reported energy, total fat, saturated, polyunsaturated and monounsaturated fatty acids between the computerized and interviewer administered methods were assessed using repeated measures ANOVA. Paired t-tests and Pearson's correlations determined relative validity of the assessments.

Analysis Of A Kinetic Multi-Segment Foot Model. Part I: Model Repeatability And Kinematic Validity, Dustin A. Bruening, Kevin M. Cooney, Frank L. Buczek

Faculty Publications

Kinematic multi-segment foot models are still evolving, but have seen increased use in clinical and research settings. The addition of kinetics may increase knowledge of foot and ankle function as well as influence multi-segment foot model evolution; however, previous kinetic models are too complex for clinical use. In this study we present a three-segment kinetic foot model and thorough evaluation of model performance during normal gait. In this first of two companion papers, model reference frames and joint centers are analyzed for repeatability, joint translations are measured, segment rigidity characterized, and sample joint angles presented. Within-tester and between-tester repeatability were …

Computerized Dietary Assessments Compare Well With Interviewer Administered Diet Histories For Patients With Type 2 Diabetes Mellitus In The Primary Healthcare Setting, Y. C. Probst, S. Faraji, M. Batterham, D. G. Steel, Linda C. Tapsell

Faculty of Health and Behavioural Sciences - Papers (Archive)

Using a context-based case-control trial, 41 adults with type 2 diabetes mellitus were randomized into four groups to complete dietary assessments (computerized or interviewer administered) at 0, 2 and 8 weeks and food records at 0 and 2 weeks. Repeatability of reported energy, total fat, saturated, polyunsaturated and monounsaturated fatty acids between the computerized and interviewer administered methods were assessed using repeated measures ANOVA. Paired t-tests and Pearson's correlations determined relative validity of the assessments.