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Ceria-Zirconia Oxide High Temperature Desulfurization Sorbent, Kwang Bok Yi
Ceria-Zirconia Oxide High Temperature Desulfurization Sorbent, Kwang Bok Yi
LSU Doctoral Dissertations
High temperature desulfurization of highly reducing coal-derived gases using ceria and ceria-zirconia sorbents is the primary object of this dissertation research. If H2S concentration is reduced to less than 1 ppmv the product gas may be used with fuel cells and downstream catalytic process. CeO2 is reduced to a non-stoichiometric oxide, which is superior to CeO2 in removing H2S. Moreover, ZrO2 addition to CeO2 to form a solid solution, Ce1-xZrxO2, increases the reducibility of CeO2. This should also result in improved desulfurization performance. Pure CeO2 and sorbents, both commercially available and prepared at LSU, were tested. XRD analysis indicated that …
Chemical Production Complex Optimization, Pollution Reduction And Sustainable Development, Aimin Xu
Chemical Production Complex Optimization, Pollution Reduction And Sustainable Development, Aimin Xu
LSU Doctoral Dissertations
The objective of this research is to propose, develop and demonstrate chemical production complex optimization to determine the optimal configuration of chemical plants in a superstructure of possible plants. The Chemical Complex Analysis System is a new methodology that has been developed to determine the best configuration of plants in a chemical production complex based on the AIChE Total Cost Assessment (TCA) for economic, energy, environmental and sustainable costs. All new, energy-efficient, and environmentally acceptable plants using greenhouse gases that can produce potentially commercial products designed with HYSYS were integrated into the chemical complex using the System. The optimum configuration …
Turbine Blade Tip Cooling And Heat Transfer, Hasan Nasir
Turbine Blade Tip Cooling And Heat Transfer, Hasan Nasir
LSU Doctoral Dissertations
Turbine blade tip leakage flow from blade pressure side to suction side over the tip surface increases the thermal loading to the blade tip, leading to a high local temperature and thus, is considered one of the primary sources of blade failure. Leakage flow can be reduced by using a recessed or squealer tip blade or by cooling the blade tip to incorporate film cooling. The performance of different recessed tip geometries were investigated and compared with plane tip performance. A transient liquid crystal technique was employed to measure detailed heat transfer coefficient distributions. Coolant injection from holes located on …
Numerical Methods For The Unsteady Incompressible Navier-Stokes Equations And Their Application To The Direct Numerical Simulation Of Turbulent Flows, Frank Herbert Muldoon
Numerical Methods For The Unsteady Incompressible Navier-Stokes Equations And Their Application To The Direct Numerical Simulation Of Turbulent Flows, Frank Herbert Muldoon
LSU Doctoral Dissertations
Two new methods for the efficient parallel computation of the unsteady incompressible Navier-Stokes equations are presented. Such efficient methods are desired for large scale parallel computations of unsteady turbulent flows such as Direct Numerical Simulations (DNS). The performance of the new methods has a distinct advantage over the artificial compressibility method, in that the methods exhibit robust convergence for a variety of flow problems without extensive need for tuning computational parameters. These methods and others have been implemented in a computer program designed for massively parallel computer architectures, written by the author and used to obtain all results in this …
Development Of Dynamic Travel Demand Models For Hurricane Evacuation, Haoqiang Fu
Development Of Dynamic Travel Demand Models For Hurricane Evacuation, Haoqiang Fu
LSU Doctoral Dissertations
Little attention has been given to estimating dynamic travel demand in transportation planning in the past. However, when factors influencing travel are changing significantly over time – such as with an approaching hurricane - dynamic demand and the resulting variation in traffic flow on the network become important. In this study, dynamic travel demand models for hurricane evacuation were developed with two methodologies: survival analysis and sequential choice model. Using survival analysis, the time before evacuation from a pending hurricane is modeled with those that do not evacuate considered as censored observations. A Cox proportional hazards regression model with time-dependent …
Modeling The Hydrologic And Particulate Loadings From Paved Urban Surfaces, Chad Michael Cristina
Modeling The Hydrologic And Particulate Loadings From Paved Urban Surfaces, Chad Michael Cristina
LSU Doctoral Dissertations
This dissertation details the results of recent investigations concerning non-colloidal particulate matter found in urban rainfall-runoff and urban snowmelt. Three forms of the power law model (PLM) were used to model particle number density. It was found that significant model error could be introduced into PLMs when the median diameter particle was used to estimate the number of particles per interval, but the SSE of continuous PLMs could be significantly reduced through the use of correction factors when the sieve interval was large (P<0.05). Additionally, a multiple PLM analysis may be more appropriate than a single PLM analysis when changes in particle population occur within a single gradation. PLMs were also used to model the relationship between cumulative granulometric mass and cumulative particulate-bound metal mass. The use of such calibrated PLMs provided considerable cost reduction when compared to conventional direct measurements of particulate-bound metal mass. A first flush analysis indicated that only events with average volumetric flow rates approaching 1 L/min/m of drainage width exhibit a rapid depletion of particulate matter consistent with the concentration-based definition of the first flush. An analysis of particle separation mechanisms indicated that 90% of these particles, by mass, could be removed from the discharge with detention times of 30 min and 120 min for snowmelt and rainfall-runoff, respectively, in a typical roadside drainage system. It was also found that the kinematic wave model could accurately model significant aspects of rainfall-runoff events in traffic-impacted watersheds provided that abstractions were incorporated into the modeling process. For this watershed the source of abstraction was attributable to vehicular traffic. For high-intensity events with more than 10 vehicles per runoff volume (VPV) the runoff coefficient varied between 0.6 and 0.9 while for low-intensity events with fewer than 10 VPV the coefficient ranged between 0.2 and 0.4.
Morphological Evolution And Instabilities Of Solid Thin Films And Wires, Wanxi Kan
Morphological Evolution And Instabilities Of Solid Thin Films And Wires, Wanxi Kan
LSU Doctoral Dissertations
This dissertation can be divided into four parts. In part I (Chapter 2), the diffusion controlled growth of multiple compound phases is studied with the nonlinear Kirkendall effect included. This part analyzes the growth of N compound phases. The method of finding intrinsic diffusion coefficients from only the positions of interfaces is found for two layers. In addition, the asymptotic analysis valid for small concentration gradients is applied to the “multi-foil” method of measuring intrinsic diffusion coefficients and yields an analytic solution for the displacement curve. A bounded solid film on a substrate can breakup from the edge into islands …
Innovative Cooling Configurations For Low Emission Gas Turbine Combustors, Ryan Thomas Hebert
Innovative Cooling Configurations For Low Emission Gas Turbine Combustors, Ryan Thomas Hebert
LSU Master's Theses
Presently, effective cooling of modern low NOx combustor liners is achieved through combinations of innovative impingement configurations and other heat transfer enhancement methods. An inherent characteristic of conventional impingement configurations is the occurrence of downstream heat transfer degradation due to increased crossflow effects. In the present study, two different impingement configurations are studied. Both impingement configurations examined in this study aim to increase heat transfer effectiveness by reducing the detrimental effects of spent air crossflow. In Part I, a combination technique wherein impingement is combined with ribs placed in between impingement rows is studied. Three configurations with increased rib placements …
Testing A Cmos Operational Amplifier Circuit Using A Combination Of Oscillation And Iddq Test Methods, Pavan K. Alli
Testing A Cmos Operational Amplifier Circuit Using A Combination Of Oscillation And Iddq Test Methods, Pavan K. Alli
LSU Master's Theses
This work presents a case study, which attempts to improve the fault diagnosis and testability of the oscillation testing methodology applied to a typical two-stage CMOS operational amplifier. The proposed test method takes the advantage of good fault coverage through the use of a simple oscillation based test technique, which needs no test signal generation and combines it with quiescent supply current (IDDQ) testing to provide a fault confirmation. A built in current sensor (BICS), which introduces insignificant performance degradation of the circuit-under-test (CUT), has been utilized to monitor the power supply quiescent current changes in the CUT. The testability …
Trajectory And Window Width Predictions For A Cased Hole Sidetrack Using A Whipstock, Harshad Prakash Patil
Trajectory And Window Width Predictions For A Cased Hole Sidetrack Using A Whipstock, Harshad Prakash Patil
LSU Master's Theses
The Trackmaster system manufactured by Smith Services consists of a multi-ramped whipstock and a trimill assembly used to perform a sidetrack from a cased well. Smith Services has observed evidence that the trimill assembly may prematurely leave the face of the whipstock and build excess inclination and dogleg severity or may fall into the original well immediately after leaving the end of the whipstock ramp thus creating a need to predict the borehole trajectory for sidetracking operations. The goal of this project was to predict the borehole trajectory and the window profile cut in the casing by the sidetracking equipment …
Numerical And Experimental Investigation Of Transport Processes In Biological Systems, Yimeng He
Numerical And Experimental Investigation Of Transport Processes In Biological Systems, Yimeng He
LSU Master's Theses
This thesis focuses on optimization techniques for transport process during the cryopreservation of biological systems. In the first part of this thesis, a well established shape independent Differential Scanning Calorimeter (DSC) technique was used to measure the dehydration response during freezing of Pacific oyster sperm cells. Volumetric shrinkage during freezing of diploid and tetraploid pacific oyster sperm cell suspensions was obtained at cooling rates of 5 and 20 ˚C/min in the presence of extracellular ice and CPAs. By fitting a model of water transport to the experimentally obtained volumetric shrinkage data the best fit membrane permeability parameters (Lpg and …
Development Of A True Triaxial Apparatus For Soil Testing, Heath Stuart Williams
Development Of A True Triaxial Apparatus For Soil Testing, Heath Stuart Williams
LSU Master's Theses
This thesis presents the development of a True Triaxial Testing TTT Apparatus. The TTT apparatus developed has the capabilities of applying the three principal stresses to a rectangular prismoidal specimen independently. The minor principal stress is provided by the cell pressure. The major principal stress is provided by a load actuator traveling at a constant velocity. A LabView software program instantaneously reads instrumentation, makes calculations, and commands a second load actuator to induce an intermediate principal stress that maintains a constant b-value; where b-value is equal to the intermediate principal stress minus the minor principal stress divided by the major …
A Re-Evaluation Of Geopressured-Geothermal Aquifers As An Energy Resource, Jeremy Scott Griggs
A Re-Evaluation Of Geopressured-Geothermal Aquifers As An Energy Resource, Jeremy Scott Griggs
LSU Master's Theses
The search for more efficient and economical forms of energy generation is a continual process. Natural gas production and electricity generation from geopressured-geothermal aquifers is an unconventional hydrocarbon source that has long been unproductive due to its marginal economics and lack of technological certainty. This thesis demonstrates that, based on modern technological competencies and economic constraints, geopressured-geothermal energy now maintains a viable future as an alternative domestic energy source.
Online Heat Transfer Measurement And Analysis For Sugar Mill Evaporators, David Timothy Solberg
Online Heat Transfer Measurement And Analysis For Sugar Mill Evaporators, David Timothy Solberg
LSU Master's Theses
Fouling and scaling in evaporators has been an area of great interest to raw sugar mills for a number of years and many of the mechanisms causing the scale and the rates of scaling are unknown. In an attempt to quantify the scaling rates and measure the scaling, an online model has been developed to model a system of evaporators. Monitoring the heat transfer coefficient as a function of time enabled measurement of the scaling rate by monitoring the heat transfer coefficient as it decreased with time. It is assumed that the scaling on the juice side of the evaporators …
Color, Texture And Rehydration Characteristics Of Ohmically Treated Sweet Potatoes, Sireesha Bhattiprolu
Color, Texture And Rehydration Characteristics Of Ohmically Treated Sweet Potatoes, Sireesha Bhattiprolu
LSU Master's Theses
Ohmic heating has been shown to affect the drying rate and texture of foods. This research was designed to determine the effect of ohmic heating on rehydration, color and texture properties of sweet potatoes. Three combinations: 60Hz, 40V, 60Hz, 60V and 1Hz, 40V were applied to ohmically heat sweet potato cubes. The ohmic treated cubes and untreated cubes or controls were stored for six days in four different %relative humidities of 11.15%, 32.73%, 57.70% and 75.32%. Results showed that there was no significant difference in the rehydration properties of ohmic treated samples and control samples. The % moisture gain varied …
Numerical Modeling Of Strain Localization In Granular Materials Using Cosserat Theory Enhanced With Microfabric Properties, Mustafa Alsaleh
Numerical Modeling Of Strain Localization In Granular Materials Using Cosserat Theory Enhanced With Microfabric Properties, Mustafa Alsaleh
LSU Doctoral Dissertations
Finite element solution in the updated Lagrangian frame is used to investigate the strain localization phenomenon "shear bands" in granular materials. The micro-polar theory was used as the mathematical foundation for the continuum formulations. A laboratory testing results are used for verification and comparison with the numerical simulation. Silica sand and glass beads with different shape indices, size and surface roughness were tested under biaxial and triaxial loading conditions to investigate the physics of the problem. The shape non-uniformity and the irregular surface roughness of the grains were studied carefully to evaluate their effect on shear band characteristics. To this …
Material Length Scales In Gradient-Dependent Plasticity/Damage And Size Effects: Theory And Computation, Rashid Kamel Abu Al-Rub
Material Length Scales In Gradient-Dependent Plasticity/Damage And Size Effects: Theory And Computation, Rashid Kamel Abu Al-Rub
LSU Doctoral Dissertations
Structural materials display a strong size-dependence when deformed non-uniformly into the inelastic range: smaller is stronger. This effect has important implications for an increasing number of applications in structural failure, electronics, functional coatings, composites, micro-electro-mechanical systems (MEMS), nanostructured materials, micro/nanometer fabrication technologies, etc. The mechanical behavior of these applications cannot be characterized by classical (local) continuum theories because they incorporate no ‘material length scales’ and consequently predict no size effects. On the other hand, it is still not possible to perform quantum and atomistic simulations on realistic time and structures. It is therefore necessary to develop a scale-dependent continuum theory …
Modeling Of Cane Sugar Colorant Removal In Packed-Bed Ion Exchange Columns And An Investigation Into Pretreatment Methods, Bruce Malcolm Ellis
Modeling Of Cane Sugar Colorant Removal In Packed-Bed Ion Exchange Columns And An Investigation Into Pretreatment Methods, Bruce Malcolm Ellis
LSU Master's Theses
Cane sugar colorants have been extensively researched but still little is known about their exact compositions. Rather than distinct compounds, they are a mixture of many compounds. Some it is assumed can be classified into the pseudo components that have been defined using gel permeation chromatography, based on molecular weight. The defining of these components has allowed the colorants to be modeled independently, instead of as one lumped color parameter. The measured colored components were modeled using a linear driving force adsorption model, which could be applied in the design process for optimizing the decolorizing capacity of the resins. The …
Photo-Control Of Dna Oligonucleotides With Cage Compounds, Bilal Ghosn
Photo-Control Of Dna Oligonucleotides With Cage Compounds, Bilal Ghosn
LSU Master's Theses
Many biochemical processes in which DNA and other nucleic acids participate are central to functions in both living cells and in molecular biology assays. While many compounds have been used to regulate the activity of DNA, these strategies are limited to the aqueous-based diffusion of the activator to the target DNA molecule. An improvement to the induction of DNA bioactivity is to move to a light-based modulation. This research demonstrates a light-based technique using a photo-cleavable cage compound to transiently inactivate DNA hybridization. Function can be restored with exposure to near-UV light, allowing for temporal control of DNA oligonucleotide (ODN) …
An Evaluation Of Methods Used To Obtain The Railroad Preemption Queue Clearance Time, Deeangela Renee Kenon
An Evaluation Of Methods Used To Obtain The Railroad Preemption Queue Clearance Time, Deeangela Renee Kenon
LSU Master's Theses
Because of the potential for serious train-vehicle accidents at or near railroad-highway grade crossings, preemption of traffic signals is a very important supplement to an active warning system. Preemption is the transfer of normal signal phasing to a special control mode with the purpose of clearing any vehicles that are queued within the dynamic envelope as the train approaches, and prohibiting signal phases that would allow additional vehicles in the track area while the train is present. The focus of this research was the determination of the Clear Track Green Interval (or the Queue Clearance Time). The clear track green …
Analysis And Evaluation Of A Bioengineered Submerged Breakwater, Matthew Dwain Campbell
Analysis And Evaluation Of A Bioengineered Submerged Breakwater, Matthew Dwain Campbell
LSU Master's Theses
Louisiana's coastline has received national attention due to rapid erosion rates estimated from approximately 60 to 100 square kilometers per year. The disappearance of coastal areas jeopardizes public and private infrastructure, property values, aquatic ecosystems, and standards of living. In order to resolve the erosion problem, innovative solutions have been explored that may improve effectiveness and cost efficiency. This research involves a technology, termed an "oysterbreak," which is a bioengineered submerged breakwater. This structure promotes oysters to form a dense structure that dissipates wave energy. Since the structure is biologically dominated, initial material use is modest. The oysterbreak was evaluated …
A Bio-Mems Device For Separation Of Breast Cancer Cells From Peripheral Whole Blood, Juan Feng
A Bio-Mems Device For Separation Of Breast Cancer Cells From Peripheral Whole Blood, Juan Feng
LSU Master's Theses
This work demonstrates the application of Bio-Micro Electro Mechanical System (Bio-MEMS) technology for early breast cancer detection and diagnosis. Early breast cancer detection and diagnosis typically uses conventional mammogram screening followed by biopsy, which can be problematic since mammography can only detect highly calcified tumors greater than 1 cm in size. A micro-device was developed to identify and specifically collect tumor cells of low abundance (1 tumor cell among 107 normal blood cells) from circulating whole blood. By immobilizing anti-EpCAM (Epithelial Cell Adhesion Molecule) antibodies on polymer micro-channel walls by the chemical surface modification of PMMA, breast cancer cells …
Route Planning Of Automated Guided Vehicles For Container Logistics, Sanjay Shankarrao Gurav
Route Planning Of Automated Guided Vehicles For Container Logistics, Sanjay Shankarrao Gurav
LSU Master's Theses
Automated guided vehicles (AGVs) are widely used in container terminals for the movement of material from shipping to the yard area and vice versa. Research in this area is directed toward the development of a path layout design and routing algorithms for container movement. The problem is to design a path layout and a routing algorithm that will route the AGVs along the bi-directional path so that the distance traveled will be minimized. This thesis presents a bi-directional path flow layout and a routing algorithm that guarantee conflict-free, shortest time routes for AGVs. Based on the path layout, a routing …
Biological Treatment Of Industrial Wastewater Containing High Concentrations Of Linear Alkylbenzene Sulfonate (Las), Luis Alberto Espinoza
Biological Treatment Of Industrial Wastewater Containing High Concentrations Of Linear Alkylbenzene Sulfonate (Las), Luis Alberto Espinoza
LSU Master's Theses
Lauryl Alkylbenzene Sulfonate (LAS) is the major anionic surfactant used worldwide in detergent and household cleaning product formulations. Its biodegradation and removal has been extensively studied in wastewater treatment facilities and laboratory-scale tests at low concentrations (<10 mg/L) typical of those encountered in municipal wastewater treatment plants. Less effort, however, has been expended investigating degradation of higher concentrations of LAS representative of those expected in wastewater generated at LAS manufacturing operations. The research described in this thesis was conducted to study biological processes for treating wastewaters containing high concentrations (e.g., 400 mg/L) of LAS. Initial experiments were carried out using a respirometry technique, and subsequently, three different laboratory-scale bioreactor systems. The three systems studied were a Sequencing Batch Reactor (SBR), a Sequencing Batch Biofilm Reactor (SBBR), and an Intermittent Cycle Extension Aeration System (ICEAS). The SBR and ICEAS were operated on a five-day cycle basis with a hydraulic retention time of four days. The SBBR was operated mainly in a two-day cycle having a hydraulic retention time of ten days as well, and polyurethane foam cubes were used as a support medium for attached biomass growth. The three systems were compared on their ability to remove LAS measured in terms of total organic carbon (TOC) and methylene blue active substances (MBAS). The reactors were also compared on the basis of foam production. The ICEAS showed the best performance in terms of controllable foam production while exhibiting a capacity for effectively dealing with transient periods of elevated loading. When a short Fill period was used, the SBR and SBBR had the disadvantage of producing excessive foaming, and an intermittent aeration strategy was required avoid overflow.
Design, Fabrication And Thermomechanical Testing Of A Vertical Bimorph Sensor In The Wafer Plane, Madhulika Sathe
Design, Fabrication And Thermomechanical Testing Of A Vertical Bimorph Sensor In The Wafer Plane, Madhulika Sathe
LSU Master's Theses
A bimetallic recurve device was designed, fabricated and tested as a temperature sensor. The device is to be used for sensing temperatures up to 300 C inside oil wells for downhole condition monitoring. Continuous downhole measurements at high temperatures and pressures are required to monitor conditions downhole instruments are exposed to during use. Currently mercury thermometers and resistive temperature detectors (RTD) are used for downhole temperature measurements. Microsensors have potential application downhole, due to their small size and inherent robustness. The principle of a bimetallic beam was used to measure temperature. A bimetallic beam deflects with changes in temperature due …
Study Of Characteristics Of Plasma Nitriding And Oxidation Of Superalloy In738lc, Mary Shanti Pampana
Study Of Characteristics Of Plasma Nitriding And Oxidation Of Superalloy In738lc, Mary Shanti Pampana
LSU Master's Theses
IN738LC is a nickel base superalloy, widely used in various applications in turbine engines at high temperatures. Its oxidation and nitriding characteristics were focused in this study. Oxidation kinetics of IN738LC in dry air was studied at selected temperatures, specially chosen depending on the chemical dynamics of the alloy at such high temperatures during annealing. Isothermal oxidation in dry air was carried out at 1000°C, 1090°C, 1140°C and 1190°C. XRD results indicated an interesting onset of preferred orientation in the ã’ depleted layer in all the samples. The XPS and XRD analyses revealed the main oxide phases present in the …
Iddq Testing Of A Cmos First Order Sigma-Delta Modulator Of An 8-Bit Oversampling Adc, Anand K. Chamakura
Iddq Testing Of A Cmos First Order Sigma-Delta Modulator Of An 8-Bit Oversampling Adc, Anand K. Chamakura
LSU Master's Theses
This work presents IDDQ testing of a CMOS first order sigma-delta modulator of an 8-bit oversampling analog-to-digital converter using a built-in current sensor [BICS]. Gate-drain, source-drain, gate-source and gate-substrate bridging faults are injected using fault injection transistors. All the four faults cause varying fault currents and are successfully detected by the BICS at a good operation speed. The BICS have a negligible impact on the performance of the modulator and an external pin is provided to completely cut-off the BICS from the modulator. The modulator was designed and fabricated in 1.5 μm n-well CMOS process. The decimator was designed on …
Effects Of Automobile Seating Posture On Trunk Muscle Activity, Milton Maada-Gormoh Saidu
Effects Of Automobile Seating Posture On Trunk Muscle Activity, Milton Maada-Gormoh Saidu
LSU Master's Theses
Reports for adult population indicate that almost 80% of the adult population has reported some form of lower back aches. Each year American workers suffer more than 300,000 lost-time injuries involving musculoskeletal disorders of the back, with the costs that run into billions of dollars. Sedentary tasks are known to be major contributing factors of back pain. Prior studies have indicated that the myoelectric activity of the lumbar region decreases when the back rest inclination of a seat increased. An increase in seat pan inclination so that it increases pressure on the leg muscles is also a cause for back …
Development And Integration Of New Processes Consuming Carbon Dioxide In Multi-Plant Chemical Production Complexes, Sudheer Indala
Development And Integration Of New Processes Consuming Carbon Dioxide In Multi-Plant Chemical Production Complexes, Sudheer Indala
LSU Master's Theses
New, energy-efficient and environmentally acceptable, catalytic processes have been identified that can use excess high purity CO2 as a raw material from the sources available in a chemical production complex. The chemical complex in the lower Mississippi River Corridor has been used to show how these new plants can be integrated into this existing infrastructure using the Chemical Complex and Cogeneration Analysis System. Eighty six published articles of laboratory and pilot plant experiments were reviewed that describe new methods and catalysts to use CO2 for producing commercially important products. Reactions have been categorized as hydrogenation reactions; hydrocarbon synthesis …
Watermarking Using Decimal Sequences, Navneet Kumar Mandhani
Watermarking Using Decimal Sequences, Navneet Kumar Mandhani
LSU Master's Theses
This thesis introduces the use of decimal sequences in watermarking to hide information for authentication. The underlying system is based on code division multiple access (CDMA), which is a form of spread spectrum communication. Different algorithms for the use of decimal sequences have been formulated for use in black and white images. The watermark is spread across the carrier image by using the d- sequences of optimal period and retrieval is made by the use of correlation. Matlab version 6.5 was used to implement the algorithms discussed in this thesis. The advantage of using d-sequences over PN sequences is that …