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Carbon Removal And Optoelectronic Property Tuning In Copper Arsenic Sulfide Thin Films Through Ligand Exchange And Alloying, Louis R. Schroeder, Scott McClary, Rakesh Agrawal 2017 Purdue University

Carbon Removal And Optoelectronic Property Tuning In Copper Arsenic Sulfide Thin Films Through Ligand Exchange And Alloying, Louis R. Schroeder, Scott Mcclary, Rakesh Agrawal

The Summer Undergraduate Research Fellowship (SURF) Symposium

Solution processed thin film solar cells are attractive alternatives to conventional energy sources due to low waste generation, flexibility in substrate choice, and scalability. The novel semiconductor Cu3AsS4 in the enargite phase has a near ideal band gap of 1.4 eV and has earth abundant constituent elements; yet single-junction solar cells have yielded low efficiencies due to a secondary carbonaceous phase present, among other issues. This carbonaceous phase may be eliminated by exchanging the carbonaceous ligands with molecular metal chalcogenides. To characterize the ligand exchanged particles, UV-Vis-NIR spectroscopy, Raman spectroscopy, X-ray diffraction, scanning electron microscopy, energy dispersive X-ray spectroscopy ...


Improving Methods Of Doping On Black Phosphorus, Yuqin Duan, Adam Charnas, Jingkai Qin, Peide Ye 2017 Electrocal and Computer Engineering

Improving Methods Of Doping On Black Phosphorus, Yuqin Duan, Adam Charnas, Jingkai Qin, Peide Ye

The Summer Undergraduate Research Fellowship (SURF) Symposium

Black phosphorus (BP) is a 2D semiconducting material with high carrier mobility. It is usually p-type due to oxidation states near its valence band. Although achieved through other growth methods, n-type doping has not yet been accomplished through the modern chemical vapor transport (CVT) growth method. To address this issue, small amounts of tellurium were added to Red Phosphorus to act as a dopant during the CVT growth process in addition to tin(Sn) and tin(IV) iodide, which facilitate growth. The chemicals are heated up to 600°C and precisely cooled in a 21-hour process, during which BP crystals ...


Laser-Assisted Metal Organic Chemical Vapor Deposition Of Gallium Nitride, Hossein Rabiee Golgir 2017 University of Nebraska-Lincoln

Laser-Assisted Metal Organic Chemical Vapor Deposition Of Gallium Nitride, Hossein Rabiee Golgir

Theses, Dissertations, and Student Research from Electrical & Computer Engineering

Due to its unique properties, gallium nitride is of great interest in industry applications including optoelectronics (LEDs, diode laser, detector), high power electronics, and RF and wirelss communication devices. The inherent shortcomings of current conventional deposition methods and the ever-increasing demand for gallium nitride urge extended efforts for further enhancement of gallium nitride deposition. The processes of conventional methods for gallium nitride deposition, which rely on thermal heating, are inefficient energy coupling routes to drive gas reactions. A high deposition temperature (1000-1100 °C) is generally required to overcome the energy barriers to precursor adsorption and surface adatom migration. However, there ...


Broadband Measurement Of Rate-Dependent Viscoelasticity At Nanoscale Using Scanning Probe Microscope: Poly(Dimethylsiloxane) Example, Zhonghua Xu, Kyongsoo Kim, Qingze Zou, Pranav Shrotriya 2017 Iowa State University

Broadband Measurement Of Rate-Dependent Viscoelasticity At Nanoscale Using Scanning Probe Microscope: Poly(Dimethylsiloxane) Example, Zhonghua Xu, Kyongsoo Kim, Qingze Zou, Pranav Shrotriya

Pranav Shrotriya

A control approach to achieve nanoscale broadband viscoelasticmeasurement using scanning probe microscope(SPM) is reported. Current SPM-based force measurement is too slow to measure rate-dependent phenomena, and large (temporal) measurement errors can be generated when the sample itself changes rapidly. The recently developed model-less inversion-based iterative control technique is used to eliminate the dynamics and hysteresis effects of the SPM hardware on the measurements, enabling rapid excitation and measurement of rate-dependent material properties. The approach is illustrated by the mechanical characterization of poly(dimethylsiloxane) over a broad frequency range of three orders of magnitude (∼1 Hz to 4.5 KHz).


Dynamic Characterization Of A Soft Elastomeric Capacitor For Structural Health Monitoring, Simon Laflamme, Filippo Ubertini, Hussam Saleem, Antonella D'Alessandro, Austin R.J. Downey, Halil Ceylan, Annibale L. Materazzi 2017 Iowa State University

Dynamic Characterization Of A Soft Elastomeric Capacitor For Structural Health Monitoring, Simon Laflamme, Filippo Ubertini, Hussam Saleem, Antonella D'Alessandro, Austin R.J. Downey, Halil Ceylan, Annibale L. Materazzi

Halil Ceylan

Structural health monitoring of civil infrastructures is a difficult task, often impeded by the geometrical size of the monitored systems. Recent advances in conducting polymers enabled the fabrication of flexible sensors capable of covering large areas, a possible solution to the monitoring challenge of mesoscale systems. The authors have previously proposed a novel sensor consisting of a soft elastomeric capacitor (SEC) acting as a strain gauge. Arranged in a network configuration, the SECs have the potential to cover very large surfaces. In this paper, understanding of the proposed sensor is furthered by evaluating its performance at vibration-based monitoring of large-scale ...


Studies In Mesoscopics And Quantum Microscopies, Zhenghao Ding, Gabriel C. Spalding 2017 Illinois Wesleyan University

Studies In Mesoscopics And Quantum Microscopies, Zhenghao Ding, Gabriel C. Spalding

Honors Projects

This thesis begins with a foundational section on quantum optics. The single-photon detectors used in the first chapter were obtained through the Advanced Laboratory Physics Association (ALPhA), which brokered reduced cost for educational use, and the aim of the single-photon work presented in Chapter 1 is to develop modules for use in Illinois Wesleyan's instructional labs beyond the first year of university. Along with the American Association of Physics Teachers, ALPhA encourages capstone-level work, such as Chapter 1 of this honors thesis, which is explicitly designed to play the role of passing on, to a next generation of physics ...


Optimization Of Reduced Graphene Oxide Deposition For Hydrogen Sensing Technologies, Matthew Pocta 2017 University of Arkansas, Fayetteville

Optimization Of Reduced Graphene Oxide Deposition For Hydrogen Sensing Technologies, Matthew Pocta

Mechanical Engineering Undergraduate Honors Theses

Graphene is known to be a key material for improving the performance of hydrogen sensors. High electrical conductivity, maximum possible surface area with respect to volume, and high carrier mobility are a few of the properties that make graphene ideal for hydrogen sensing applications. The problem with utilizing graphene is the difficulty in depositing uniform, thin layers onto substrate surfaces. This study examines a new method of optimizing graphene deposition by utilizing an airbrush to deposit both graphene oxide (GO) and reduced graphene oxide (rGO) onto glass substrates. The number of depositions were varied among samples to study the effect ...


Compositionally Graded Indium Gallium Nitride Solar Cells, Christopher Matthews 2017 University of Arkansas, Fayetteville

Compositionally Graded Indium Gallium Nitride Solar Cells, Christopher Matthews

Electrical Engineering Undergraduate Honors Theses

For the past several decades, methods to harvest solar energy have been investigated intensively. A majority of the work done in this field has been on solar cells made with silicon – the most mature semiconductor material. Recent developments in material fabrication and processing techniques have enabled other semiconductor materials to attract practical interest and research effort as well. Indium gallium nitride (InGaN) is one such material. The material properties of InGaN indicate that solar cells made with it have the potential to achieve much higher power density than a standard silicon solar cell. High power density InGaN solar cells could ...


Development Of Intermediate Band Solar Cell Through Ingan Quantum Well Structures, Kelly McKenzie 2017 University of Arkansas, Fayetteville

Development Of Intermediate Band Solar Cell Through Ingan Quantum Well Structures, Kelly Mckenzie

Electrical Engineering Undergraduate Honors Theses

In the search for high-efficiency solar cells, InxGa1-xN has come under scrutiny as a unique material with high potential. This is due to characteristics including an easily tunable bandgap, large range of potential bandgap values, and high heat resistance. However, one factor limiting its adaptation is the high density of crystal defects. In this thesis, the qualities of InGaN are discussed and the intermediate band solar cell structure is introduced. Additionally, the growth and characterization of two sets of InGaN-based solar cell devices are reported and evaluated.


Tunable, Room Temperature Thz Emitters Based On Nonlinear Photonics, Raju Sinha 2017 Florida International University

Tunable, Room Temperature Thz Emitters Based On Nonlinear Photonics, Raju Sinha

FIU Electronic Theses and Dissertations

The Terahertz (1012 Hz) region of the electromagnetic spectrum covers the frequency range from roughly 300 GHz to 10 THz, which is in between the microwave and infrared regimes. The increasing interest in the development of ultra-compact, tunable room temperature Terahertz (THz) emitters with wide-range tunability has stimulated in-depth studies of different mechanisms of THz generation in the past decade due to its various potential applications such as biomedical diagnosis, security screening, chemical identification, life sciences and very high speed wireless communication. Despite the tremendous research and development efforts, all the available state-of-the-art THz emitters suffer from either being ...


A Finite Element Approach To Self-Consistent Field Theory Calculations Of Multiblock Polymers, David M. Ackerman, Kris Delaney, Glenn H. Fredrickson, Baskar Ganapathysubramanian 2017 Iowa State University

A Finite Element Approach To Self-Consistent Field Theory Calculations Of Multiblock Polymers, David M. Ackerman, Kris Delaney, Glenn H. Fredrickson, Baskar Ganapathysubramanian

Mechanical Engineering Publications

Self-consistent field theory (SCFT) has proven to be a powerful tool for modeling equilibrium microstructures of soft materials, particularly for multiblock polymers. A very successful approach to numerically solving the SCFT set of equations is based on using a spectral approach. While widely successful, this approach has limitations especially in the context of current technologically relevant applications. These limitations include non-trivial approaches for modeling complex geometries, difficulties in extending to non-periodic domains, as well as non-trivial extensions for spatial adaptivity. As a viable alternative to spectral schemes, we develop a finite element formulation of the SCFT paradigm for calculating equilibrium ...


Low-Temperature Fabrication Process For Integrated High-Aspect Ratio Metal Oxide Nanostructure Semiconductor Gas Sensors, William Paul Clavijo 2017 Virginia Commonwealth University

Low-Temperature Fabrication Process For Integrated High-Aspect Ratio Metal Oxide Nanostructure Semiconductor Gas Sensors, William Paul Clavijo

Theses and Dissertations

This work presents a new low-temperature fabrication process of metal oxide nanostructures that allows high-aspect ratio zinc oxide (ZnO) and titanium dioxide (TiO2) nanowires and nanotubes to be readily integrated with microelectronic devices for sensor applications. This process relies on a new method of forming a close-packed array of self-assembled high-aspect-ratio nanopores in an anodized aluminum oxide (AAO) template in a thin (2.5 µm) aluminum film deposited on a silicon and lithium niobate substrate (LiNbO3). This technique is in sharp contrast to traditional free-standing thick film methods and the use of an integrated thin aluminum film greatly ...


Quantifying Gauche Defects And Phase Evolution In Self-Assembled Monolayers Through Sessile Drops, Jiahao Chen, Boyce Chang, Stephanie Oyola-Reynoso, Zhengjia Wang, Martin M. Thuo 2017 Iowa State University

Quantifying Gauche Defects And Phase Evolution In Self-Assembled Monolayers Through Sessile Drops, Jiahao Chen, Boyce Chang, Stephanie Oyola-Reynoso, Zhengjia Wang, Martin M. Thuo

Materials Science and Engineering Publications

Self-assembled monolayers (SAMs) are widely used in surface modifications, specifically in tuning the surface chemistry of materials. The structure and properties of SAMs have been extensively studied often with sophisticated tools, even for the simplest n-alkanethiolate SAMs. In SAMs, especially in linear n-alkanethiolates, the properties are dependent on the chain length, which is best manifested in the so-called odd–even effect, a simple yet not fully understood phenomenon. One main challenge is fully delineating the origin of length-dependent properties, which can be due to the structure (ideal SAMs), defect evolution, or substrate-molecule effects. This study demonstrates that utilizing ...


Rapid And Label-Free Detection Of Interferon Gamma Via An Electrochemical Aptasensor Comprising A Ternary Surface Monolayer On A Gold Interdigitated Electrode Array, Shaowei Ding, Curtis L. Mosher, Xian Y. Lee, Suprem R. Das, Allison A. Cargill, Xiaohui Tang, Bolin Chen, Eric S. McLamore, Carmen Gomes, Jesse M. Hostetter, Jonathan C. Claussen 2017 Iowa State University

Rapid And Label-Free Detection Of Interferon Gamma Via An Electrochemical Aptasensor Comprising A Ternary Surface Monolayer On A Gold Interdigitated Electrode Array, Shaowei Ding, Curtis L. Mosher, Xian Y. Lee, Suprem R. Das, Allison A. Cargill, Xiaohui Tang, Bolin Chen, Eric S. Mclamore, Carmen Gomes, Jesse M. Hostetter, Jonathan C. Claussen

Mechanical Engineering Publications

A label-free electrochemical impedance spectroscopy (EIS) aptasensor for rapid detection (<35 min) of interferon-gamma (IFN-γ) was fabricated by immobilizing a RNA aptamer capture probe (ACP), selective to IFN-γ, on a gold interdigitated electrode array (Au IDE). The ACP was modified with a thiol group at the 5′ terminal end and subsequently co-immobilized with 1,6-hexanedithiol (HDT) and 6-mercapto-1-hexanolphosphate (MCH) to the gold surface through thiol–gold interactions. This ACP/HDT-MCH ternary surface monolayer facilitates efficient hybridization with IFN-γ and displays high resistance to nonspecific adsorption of nontarget proteins [i.e., fetal bovine serum (FBS) and bovine serum albumin (BSA)]. The Au IDE functionalized with ACP/HDT-MCH was able to measure IFN-γ in actual FBS solution with a linear sensing range from 22.22 pM to 0.11 nM (1–5 ng/mL) and a detection limit of 11.56 pM. The ability to rapidly sense IFN-γ within this sensing range makes the developed electrochemical platform conducive toward in-field disease detection of a variety of diseases including paratuberculosis (i.e., Johne’s Disease). Furthermore, experimental results were numerically validated with an equivalent circuit model that elucidated the effects of the sensing process and the influence of the immobilized ternary monolayer on signal output. This is the first time that ternary surface monolayers have been used to selectively capture/detect IFN-γ on Au IDEs.


Dynamic Characterization Of A Soft Elastomeric Capacitor For Structural Health Monitoring, Simon Laflamme, Filippo Ubertini, Hussam Saleem, Antonella D'Alessandro, Austin R.J. Downey, Halil Ceylan, Annibale L. Materazzi 2016 Iowa State University

Dynamic Characterization Of A Soft Elastomeric Capacitor For Structural Health Monitoring, Simon Laflamme, Filippo Ubertini, Hussam Saleem, Antonella D'Alessandro, Austin R.J. Downey, Halil Ceylan, Annibale L. Materazzi

Simon Laflamme

Structural health monitoring of civil infrastructures is a difficult task, often impeded by the geometrical size of the monitored systems. Recent advances in conducting polymers enabled the fabrication of flexible sensors capable of covering large areas, a possible solution to the monitoring challenge of mesoscale systems. The authors have previously proposed a novel sensor consisting of a soft elastomeric capacitor (SEC) acting as a strain gauge. Arranged in a network configuration, the SECs have the potential to cover very large surfaces. In this paper, understanding of the proposed sensor is furthered by evaluating its performance at vibration-based monitoring of large-scale ...


A Multi-Channel 3d-Printed Bioreactor For Evaluation Of Growth And Production In The Microalga Dunaliella Sp, Cristian A. Cox 2016 University of Maine

A Multi-Channel 3d-Printed Bioreactor For Evaluation Of Growth And Production In The Microalga Dunaliella Sp, Cristian A. Cox

Electronic Theses and Dissertations

We explored the capabilities of additive manufacturing using a photo-cured jetted material 3D printer to manufacture a milli-microfluidic device with direct application in microalgae Dunaliella sp growth and intracellular compounds biosynthesis tests. A continuous microbioreactor for microalgae culture was CAD designed and successfully built in 1 hour and 49 minutes using black photopolymer cured by UV and a support material. The microreactor was made up of 2 parts including the bioreactor itself and a microchannel network for culture media fluids and microalgae. Both parts were assembled to form a single unit. Additional optical and auxiliar components were added. An external ...


Strategies And Techniques For Fabricating Mems Bistable Thermal Actuators., Dilan Ratnayake 2016 University of Louisville

Strategies And Techniques For Fabricating Mems Bistable Thermal Actuators., Dilan Ratnayake

Electronic Theses and Dissertations

Bistable elements are beginning to appear in the field of MEMS as they allow engineers to design sensors and actuators which require no electrical power and possess mechanical memory. This research focuses on the development of novel strategies and techniques for fabricating MEMS bistable structures to serve as no electrical power thermal actuators. Two parallel strategies were explored for the design and fabrication of the critical bistable element. Both strategies involved an extensive material study on candidate thin film materials to determine their temperature coefficient of expansion and as-deposited internal stress properties. Materials investigated included titanium tungsten, Invar, silicon nitride ...


Nanostructured Morphologies In Glassy Polymer Networks, Brian Greenhoe 2016 University of Southern Mississippi

Nanostructured Morphologies In Glassy Polymer Networks, Brian Greenhoe

Dissertations

The body of this work describes a novel approach for the dispersion of multi-walled carbon nanotubes in a high Tg epoxy prepolymer matrix using a twin screw high-shear continuous reactor. The method demonstrated improves on previous dispersion methods in several ways. It offers increased efficiency through excellent heat transfer, while being solvent-less, scale-able, and tailorable to drive dispersion states to judiciously chosen dispersion states. Furthermore, it was shown that dispersion state and agglomerate morphology can be directed, in several ways, through processing conditions and also by controlling the matrix viscosity profile through cure. Broadband dielectric spectroscopy, optical hot-stage microscopy ...


Fabrication Of Infrared Photodetectors Utilizing Lead Selenide Nanocrystals, Justin Anthony Hill 2016 University of Arkansas, Fayetteville

Fabrication Of Infrared Photodetectors Utilizing Lead Selenide Nanocrystals, Justin Anthony Hill

Theses and Dissertations

Colloidal lead selenide and lead selenide / lead sulfide core/shell nanocrystals were grown using a wet chemical synthesis procedure. Absorbance and photoluminescence measurements were made to verify the quality of the produced nanocrystals. Absorbance spectra were measured at room temperature, while photoluminescence spectra were measured at 77 K. Organic ligands were exchanged for shorter ligands in order to increase the conductivity of the nanocrystals. Absorption and PL spectra for both core and core/shell nanocrystals were compared. Interdigital photodetector devices with varying channel widths were fabricated by depositing gold onto a glass substrate. Lead selenide nanocrystals were deposited onto these ...


Dispersion Of Particles In Liquid Metal Using Contactless Electromagnetic Stirring, Koulis A. Pericleous, Valdis Bojarevics, Georgi S. Djambazov 2016 University of Greenwich

Dispersion Of Particles In Liquid Metal Using Contactless Electromagnetic Stirring, Koulis A. Pericleous, Valdis Bojarevics, Georgi S. Djambazov

The 8th International Conference on Physical and Numerical Simulation of Materials Processing

No abstract provided.


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